CN208449314U - A kind of amion acetic acid production ammonification synthesis reactor - Google Patents
A kind of amion acetic acid production ammonification synthesis reactor Download PDFInfo
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- CN208449314U CN208449314U CN201821064136.9U CN201821064136U CN208449314U CN 208449314 U CN208449314 U CN 208449314U CN 201821064136 U CN201821064136 U CN 201821064136U CN 208449314 U CN208449314 U CN 208449314U
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- fixed frame
- shaft
- acetic acid
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- electrode slice
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Abstract
The utility model relates to reaction kettle devices, a kind of amion acetic acid production ammonification synthesis reactor is provided, autoclave body and kettle cover including reaction kettle, the inside of autoclave body is equipped with shaft, the top of kettle cover is equipped with the driving device of drive shaft rotation, shaft circumference direction is equipped with several linking arms, and fixed frame, the fixed several groups heating sheet in the inside of fixed frame are fixedly connected on the outside of linking arm；The upper outer of shaft is equipped at intervals with annular electro pole piece, and electrode slice is separately connected the positive and negative anodes of heating sheet, and the outside of electrode slice is equipped with the fixed brush being electrically connected with electrode slice, and fixed brush is fixedly connected with fixing seat and is electrically connected with extraneous power supply unit.The utility model can heat reaction process in the way of paddle heating, while paddle also can be carried out the stirring of material, and paddle can follow kettle cover to carry out disassembly, cleaning, considerably increase maintainability.
Description
Technical field
The utility model relates to reaction kettle devices, and in particular to a kind of amion acetic acid production ammonification synthesis reactor.
Background technique
The production method of amion acetic acid mainly uses monoxone ammoniation process, first all puts into methenamine in reaction kettle,
Then ammonium hydroxide is added, then monoxone is added dropwise, is reacted at 50-60 DEG C, keeps the temperature 3 hours at 72~78 DEG C, then analyse through alcohol,
Obtain product.Including 1, chloride process, chlorine is passed through in the reaction kettle of acetic acid, under sulfur catalyst, heating is reacted,
It is produced into monoxone and hydrogen chloride gas.2, ammonification process: monoxone is passed through in ammonia reaction kettle, generates amion acetic acid and chlorination
Ammonium.
Therefore, in the synthesis process, both need to heat medical fluid, it is carried out being sufficiently mixed reaction again, it is existing
It is mostly heated using water in technology, heating efficiency is low, and the inner wall that water circulation pipe is in addition used for a long time is easy to appear knot wall object, clearly
Reason is difficult.Electric heating has the advantages that heating efficiency is high, and disassembly is inconvenient, and later maintenance is also highly difficult.
Summary of the invention
The utility model is to solve water circulating-heating in the prior art easily to occur tying wall phenomenon, and electric heating is difficult in maintenance to be lacked
It falls into, a kind of ammonification synthesis reactor that can be heated while agitating is provided.
The utility model is implemented with the following technical solutions, a kind of amion acetic acid production ammonification synthesis reactor, including reaction
The autoclave body and kettle cover of kettle, the inside of autoclave body are equipped with shaft, and the top of kettle cover is equipped with the driving device of drive shaft rotation, shaft circle
Circumferential direction is equipped with several linking arms, and fixed frame, the fixed several groups heating sheet in the inside of fixed frame are fixedly connected on the outside of linking arm；
The upper outer of shaft is equipped at intervals with annular electro pole piece, and electrode slice is separately connected the positive and negative anodes of heating sheet, sets on the outside of electrode slice
There is the fixed brush being electrically connected with electrode slice, fixed brush is fixedly connected with fixing seat and is electrically connected with extraneous power supply unit.
Preferably, the electrode slice is located above kettle cover, and the brush is mounted on the inside of the brush carrier block of annular.
Preferably, the fixed frame is rectangular configuration, and heating sheet connects along the length direction parallel connection of fixed frame in fixed frame
It connects.
Preferably, the fixed frame is fixedly connected with axes of rotation skew.
Further, interval is equipped between institute's heating sheet.
The utility model is beneficial in that, can be heated in the way of paddle heating to reaction process,
Paddle also can be carried out the stirring of material simultaneously, and paddle can follow kettle cover to carry out disassembly, cleaning, and considerably increasing can safeguard
Property.
Detailed description of the invention
Fig. 1 the utility model overall structure diagram；
Fig. 2 the utility model fixed rack structure schematic diagram；
Fig. 3 the utility model electrode slice attachment structure schematic diagram；
1. kettle cover in figure, 11. driving motors, 12. fixing seats, 2. autoclave bodies, 3. shafts, 31. linking arms, 4. fixed frames, 5.
Heating sheet, 51. heating sheet conducting wire I, 52. heating sheet conducting wire II, 6. electrode slice I, 61. fixed brush I, 62. power supply lines, 7. electrodes
Piece II, 71. fixed brush II.
Specific embodiment
The utility model is described in further detail with reference to the accompanying drawing.
Embodiment one
As shown in Figure 1, the utility model provides a kind of amion acetic acid production ammonification synthesis reactor, the autoclave body including reaction kettle
2 and kettle cover 1, kettle cover and autoclave body are separable, and wherein the inner vertical of autoclave body is equipped with shaft 3, are equipped with driving above shaft and kettle cover
The driving device of shaft rotation, is equipped with bearing, driven by the driving device, shaft can be in autoclave body between shaft and kettle cover
Portion's rotation.Wherein shaft circumference direction is equipped with several linking arms 31, and one end and the shaft of linking arm are fixed, the other end of linking arm
It is fixedly connected with fixed frame 4, fixed frame is tower structure, and the fixed several groups heating sheet 5 in inside, heating sheet is preferably using pottery
Porcelain heating sheet.It when shaft rotates, is able to drive linking arm and fixed frame rotates together, heating sheet realizes heating, shaft after being powered
Drive heating sheet rotary heating.
As shown in Figures 2 and 3, in order to realize the rotary heating of heating sheet, the upper outer fixed electrode film I6 of shaft and
Electrode slice II7, is spaced setting between two arrays of electrodes piece, and the inside of shaft is equipped with conducting wire, electrode slice respectively by conducting wire connection plus
The positive and negative anodes of backing, and the outside of electrode slice is equipped with the fixed brush being electrically connected with electrode slice, fixed brush passes through fixing seat 12
It is fixedly connected, fixed brush I61 and fixed brush II71 respectively correspond electrode slice I6 and electrode slice II7, fixed brush I61 and solid
Stable electric brush II71 passes through power supply line 62 respectively and is electrically connected with extraneous power supply unit, and fixed brush is fixed on the inside of fixing seat.
In the present embodiment, since the intracorporal operating condition of kettle is more severe, electrode slice is arranged above kettle cover, driving motor 11
Drive shaft to pass through kettle cover, power supply realized by electrode slice and brush, such brush be mounted on the inside of the brush carrier block of annular with
Electrical connection is realized in electrode slice contact, and the upper and lower sides of fixing seat are connect with rotating shaft sealing.
Embodiment two
As shown in Fig. 2, fixed frame is rectangular configuration in the present embodiment, in fixed frame heating sheet along fixed frame length
Direction is connected in parallel, and the two sides of fixed frame are respectively as the threading frame of threading, and heating sheet is fixed on two sides up and down, between heating sheet
It is equipped with interval.When shaft drives fixed frame rotation, heating sheet follows rotation, since there are gap, solution between heating sheet
Gap can be passed through when being stirred and forms turbulent flow, further enhance the effect of heated contact surface and stirring.
Embodiment three
In the present embodiment, fixed frame is fixedly connected with axes of rotation skew, and the fixed frame being obliquely installed can play and propeller
Similar effect carries out internal solution more uniformly in reaction.
Claims (5)
1. a kind of amion acetic acid production ammonification synthesis reactor, the inside of autoclave body and kettle cover including reaction kettle, autoclave body are equipped with shaft,
The top of kettle cover is equipped with the driving device of drive shaft rotation, which is characterized in that the shaft circumference direction is equipped with several connections
Arm is fixedly connected with fixed frame, the fixed several groups heating sheet in the inside of the fixed frame on the outside of linking arm；The top of the shaft
Outside spacers are equipped with annular electro pole piece, and electrode slice is separately connected the positive and negative anodes of heating sheet, and the outside of the electrode slice is equipped with and electricity
The fixed brush of pole piece electrical connection, the fixed brush are fixedly connected with fixing seat and are electrically connected with extraneous power supply unit.
2. amion acetic acid production ammonification synthesis reactor according to claim 1, which is characterized in that the electrode slice is located at kettle
The side of covering, the brush are mounted on the inside of the brush carrier block of annular.
3. amion acetic acid according to claim 1 or 2 production ammonification synthesis reactor, which is characterized in that the fixed frame is
Rectangular configuration, heating sheet is connected in parallel along the length direction of fixed frame in fixed frame.
4. amion acetic acid production ammonification synthesis reactor according to claim 3, which is characterized in that the fixed frame and shaft
Inclination is fixedly connected.
5. amion acetic acid production ammonification synthesis reactor according to claim 4, which is characterized in that be all provided between institute's heating sheet
There is interval.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821064136.9U CN208449314U (en) | 2018-07-06 | 2018-07-06 | A kind of amion acetic acid production ammonification synthesis reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821064136.9U CN208449314U (en) | 2018-07-06 | 2018-07-06 | A kind of amion acetic acid production ammonification synthesis reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208449314U true CN208449314U (en) | 2019-02-01 |
Family
ID=65170724
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821064136.9U Active CN208449314U (en) | 2018-07-06 | 2018-07-06 | A kind of amion acetic acid production ammonification synthesis reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208449314U (en) |
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2018
- 2018-07-06 CN CN201821064136.9U patent/CN208449314U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: An ammoniation reactor for aminoacetic acid production Effective date of registration: 20201102 Granted publication date: 20190201 Pledgee: Qingzhou Shandong rural commercial bank Limited by Share Ltd. Pledgor: SHANDONG ZHENXING CHEMICAL Co.,Ltd. Registration number: Y2020980007443 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right |