CN208449264U - Boosting type pyrophillite for synthesis assembles block - Google Patents

Boosting type pyrophillite for synthesis assembles block Download PDF

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Publication number
CN208449264U
CN208449264U CN201820377284.XU CN201820377284U CN208449264U CN 208449264 U CN208449264 U CN 208449264U CN 201820377284 U CN201820377284 U CN 201820377284U CN 208449264 U CN208449264 U CN 208449264U
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pyrophillite
boosting type
synthesis
pressure inlet
column
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CN201820377284.XU
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衡军
史春燕
骈小璇
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ZHENGZHOU NEW ASIA SUPERHARD MATERIAL COMPOSITE CO Ltd
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ZHENGZHOU NEW ASIA SUPERHARD MATERIAL COMPOSITE CO Ltd
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Abstract

The utility model discloses a kind of boosting type pyrophillites for synthesis to assemble block, including in polyhedral pyrophillite ontology, the high compression mold cavities for penetrating pyrophillite ontology are provided on pyrophillite ontology, the both ends of the high compression mold cavities are disposed with steel pad, conducting steel ring, pressurization column, pressure inlet from the outside to the core, and the pressure inlet is internally provided with the heating component for synthetic sample.The utility model is easy to operate, pressure transmission is high-efficient, can be improved the inside effective pressure of pyrophyllite block package assembly.

Description

Boosting type pyrophillite for synthesis assembles block
Technical field
Block is assembled the utility model relates to a kind of synthesis pyrophillite more particularly to a kind of boosting type leaf for synthesis is cured Stone assembles block.
Background technique
In superhard material synthesis technology, mainly using the Static Catalyst of cubic hinge press cooperation pyrophillite synthesis mould Method, the main function of pyrophyllite material are pressure transmission, sealing and heat preservation.When being pressurized using which, pyrophillite synthetic cavity Maximum pressure could not break through 6GPa always, and currently used assembling block, which synthesizes intracavitary portion, can produce 5.0-5.5GPa high pressure, continue The service life that synthesis pressure influences whether cubic hinge press synthesis device and its auxiliary accessories is improved, top hammer consumption can be especially made It increases, not only increases production cost, there is also some potential safety problemss.Therefore, it is necessary to improve the prior art to solve Above-mentioned technical problem.
Utility model content
In view of this, the present invention provides a kind of boosting type pyrophillites for synthesis to assemble block, easy to operate, biography Inside effective pressure that is high-efficient, can be improved pyrophyllite block package assembly is pressed, is realized in particular by following technical scheme:
A kind of boosting type pyrophillite for synthesis described in the utility model assembles block, including at cured in polyhedral leaf Stone ontology is provided with the high compression mold cavities for penetrating pyrophillite ontology on pyrophillite ontology, and the both ends of the high compression mold cavities are from the outside to the core It is disposed with steel pad, conducting steel ring, pressurization column, pressure inlet, the pressure inlet is internally provided with adding for synthetic sample Hot component.
Further, the pressurization column is stepped;Pressurization column one end is bonded with conducting steel ring, is pressurized the other end insertion of column It is bonded inside pressure inlet with heating component;Pyrophillite ring I is provided at ladder on the pressurization column, pyrophillite ring I, which is located at, to be increased Between compression leg, pressure inlet.
Further, the pressure inlet includes tungsten carbide pipe and magnesia tube, and the magnesia tube is located inside tungsten carbide pipe; The pyrophillite ontology, tungsten carbide pipe and heating component are successively bonded.
Further, the heating component includes the heating tube being set in magnesia tube, the heating tube and pressurization column it Between be provided with heating sheet;The heating tube and heating sheet are closed for containing the cavity of sample at one after being installed.
Further, salt pipe is provided between the sample and heating tube, between the sample and heating sheet outside to inside successively It is provided with salt piece and mica.
Further, the tungsten carbide thickness of pipe wall is greater than 5mm, and the magnesia tube wall thickness is less than 3mm.
Further, be provided with pyrophillite ring II outside the conducting steel ring, the pressurization outer surface of column and conducting steel ring and Face after pyrophillite ring II is installed is overlapped.
Further, the high compression mold cavities are cylindrical or rib tubular, pressure inlet are cylinder barrel shaped or rib tubular.
The utility model has the beneficial effects that pressurization column described in the utility model and pressure inlet are all set in pyrophillite ontology In high compression mold cavities and in the same high compression mold cavities of closer at a distance from sample and sample, the effect for increasing pressure is good;The pressure inlet For cylinder barrel shaped or rib tubular, the effect for increasing sample synthesis pressure sample " full package " is more preferable;The pressurization column and Pressure inlet can reuse, good economy performance.Other beneficial effects of the utility model will in conjunction in embodiment in detail below into Row further instruction.
Detailed description of the invention
The utility model is further described with reference to the accompanying drawings and examples:
FIG. 1 is a schematic structural view of the utility model;
In figure: 1, pyrophillite ontology;2, steel pad;3, conducting steel ring;4, pyrophillite ring II;5, it is pressurized column;6, pyrophillite ring Ⅰ;7, tungsten carbide pipe;8, magnesia tube;9, heating sheet;10, heating tube;11, salt pipe;12, salt piece;13, mica;14, sample.
Specific embodiment
The boosting type pyrophillite described in the present embodiment for synthesis assembles block as shown in Figure 1:, including in polyhedron Pyrophillite ontology 1, be provided with the high compression mold cavities for penetrating pyrophillite ontology, the both ends of the high compression mold cavities on pyrophillite ontology 1 It is disposed with steel pad 2, conducting steel ring 3, pressurization column 5, pressure inlet from the outside to the core, the pressure inlet is internally provided with for closing At the heating component of sample.The preferred tungsten carbide of material of the pressurization column 5, can also be certainly is tungsten, molybdenum, titanium or iron and its conjunction Gold.
In the present embodiment, the pressurization column 5 is stepped;Pressurization 5 one end of column is bonded with conducting steel ring 3, pressurization column 5 It is bonded inside other end insertion pressure inlet with heating component;It is provided with pyrophillite ring I 6 at ladder on the pressurization column 5, leaf is cured Stone ring I 6 is located between pressurization column 5, pressure inlet.Preferential, the pressurization column 5 is at " T " font.Pyrophillite ring I 6 has when being pressurized Flowability, compressibility, preferable pressure transmission and leakproofness.Two pressurization columns 5 form similar two sides top pressure transmission structure pressure transmission effect Rate is high;High pressure mold cavity effective pressure can be made to further increase using its mobility and leakproofness provided with pyrophillite ring I 6, Significantly improve diamond or cubic boron nitride sintered body performance.
In the present embodiment, the pressure inlet includes tungsten carbide pipe 7 and magnesia tube 8, and the magnesia tube 7 is located at carbon Change inside tungsten pipe 8;The pyrophillite ontology 1, tungsten carbide pipe 7 and heating component are successively bonded.The tungsten carbide pipe 7 and magnesia Pressurization column 5 and pyrophillite ring I 6 of its tubular design of pipe 8 with synthesis T-shape form the closing of a sealing for sample Room, the sealing performance for having this excellent in sample 14 while efficient pressure transmission are conducive to the stable target material of synthesis performance.
In the present embodiment, the heating component includes the heating tube 10 being set in magnesia tube, the heating tube 10 Heating sheet 9 is provided between pressurization column 5;The heating tube 10 and heating sheet 9 are closed for containing at one after being installed The cavity of sample 14.Further, the heating tube and heating sheet preferentially select carbon pipe or carbon plate, the heating tube 10 and heating Piece 9 again can be sealed sample 14 while heating to sample 14 and further increase leakproofness.
In the present embodiment, salt pipe 11, the sample 14 and heating sheet are provided between the sample 14 and heating tube 10 Salt piece 12 and mica 13 are disposed between 9 outside to inside.Setting mica 13 act on be prevent between sample 14 and sample, sample It is mutually viscous between 14 and salt to be melted together, under salt pipe 11,9 high temperature and pressure of salt piece, it can be achieved that pressure transmission is uniform, while completely cut off sample With external contact, contaminated samples are prevented.
In the present embodiment, 7 wall thickness of tungsten carbide pipe is greater than 5mm, and 8 wall thickness of magnesia tube is less than 3mm.Carbon is set Change tungsten tube thickness and be greater than 5mm, ensure that tungsten carbide pipe 7 is not squeezed and broken and deforms under high pressure, setting 8 thickness of magnesia tube is little The insulation effect in 3mm is, and space appropriate is provided for sample 14.
In the present embodiment, be provided with pyrophillite ring II 4 outside the conducting steel ring 3, the pressurization outer surface of column with lead Face after electric steel ring 3 and pyrophillite ring II 4 are installed is overlapped.The pyrophillite ring II 4 is set to the outer end of high compression mold cavities and is located at The technical issues of 2 inside of steel pad, the setting of such level solves pressure transmission, heat preservation, poor sealing performance in high compression mold cavities, performance is excellent It is good first more preferable than traditional pyrophillite assembling block pressure transmission, heat preservation, sealing performance.
In the present embodiment, the high compression mold cavities are cylindrical or rib tubular, pressure inlet are cylinder barrel shaped or rib tubular.
Finally, it is stated that above embodiments are merely intended for describing the technical solutions of the present application, but not for limiting the present application, although ginseng The utility model is described in detail according to preferred embodiment, those skilled in the art should understand that, it can be to this The technical solution of utility model is modified or replaced equivalently, without departing from the objective and model of technical solutions of the utility model It encloses, should all cover in the scope of the claims of the utility model.

Claims (8)

1. a kind of boosting type pyrophillite for synthesis assembles block, including in polyhedral pyrophillite ontology, pyrophillite ontology On be provided with the high compression mold cavities for penetrating pyrophillite ontology, it is characterised in that: the both ends of the high compression mold cavities are successively set from the outside to the core It is equipped with steel pad, conducting steel ring, pressurization column, pressure inlet, the pressure inlet is internally provided with the heating component for synthetic sample.
2. the boosting type pyrophillite according to claim 1 for synthesis assembles block, it is characterised in that: the pressurization column is in It is ladder-like;Pressurization column one end is bonded with conducting steel ring, is pressurized inside the other end insertion pressure inlet of column and is bonded with heating component;? Pyrophillite ring I is provided on the pressurization column at ladder, pyrophillite ring I is located between pressurization column, pressure inlet.
3. the boosting type pyrophillite according to claim 2 for synthesis assembles block, it is characterised in that: the pressure inlet packet Tungsten carbide pipe and magnesia tube are included, the magnesia tube is located inside tungsten carbide pipe;The pyrophillite ontology, tungsten carbide pipe and add Hot component is successively bonded.
4. the boosting type pyrophillite according to claim 3 for synthesis assembles block, it is characterised in that: the heating component Including the heating tube being set in magnesia tube, heating sheet is provided between the heating tube and pressurization column;The heating tube and Heating sheet is closed for containing the cavity of sample at one after being installed.
5. it is according to claim 4 for synthesis boosting type pyrophillite assemble block, it is characterised in that: the sample with plus It is provided with salt pipe between heat pipe, is disposed with salt piece and mica between the sample and heating sheet outside to inside.
6. the boosting type pyrophillite according to claim 3-5 any claim for synthesis assembles block, feature exists In: the tungsten carbide thickness of pipe wall is greater than 5mm, and the magnesia tube wall thickness is less than 3mm.
7. the boosting type pyrophillite described in -5 any claims for synthesis assembles block according to claim 1, feature exists In: it is provided with pyrophillite ring II, the pressurization outer surface of column and conducting steel ring outside the conducting steel ring and pyrophillite ring II is pacified Face after dress is overlapped.
8. the boosting type pyrophillite according to claim 7 for synthesis assembles block, it is characterised in that: the high compression mold cavities Cylindrical or rib tubular, pressure inlet are cylinder barrel shaped or rib tubular.
CN201820377284.XU 2018-03-20 2018-03-20 Boosting type pyrophillite for synthesis assembles block Active CN208449264U (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108211995A (en) * 2018-03-20 2018-06-29 郑州新亚复合超硬材料有限公司 Super-pressure pyrophillite assembles block
CN113084172A (en) * 2020-06-30 2021-07-09 郑州新亚复合超硬材料有限公司 Method for preparing impregnated teeth by using ultrahigh temperature and high pressure and impregnated teeth thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108211995A (en) * 2018-03-20 2018-06-29 郑州新亚复合超硬材料有限公司 Super-pressure pyrophillite assembles block
CN113084172A (en) * 2020-06-30 2021-07-09 郑州新亚复合超硬材料有限公司 Method for preparing impregnated teeth by using ultrahigh temperature and high pressure and impregnated teeth thereof

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