CN208430120U - A kind of device using poultry and aquatic products waste grease preparation biodiesel - Google Patents
A kind of device using poultry and aquatic products waste grease preparation biodiesel Download PDFInfo
- Publication number
- CN208430120U CN208430120U CN201821015119.6U CN201821015119U CN208430120U CN 208430120 U CN208430120 U CN 208430120U CN 201821015119 U CN201821015119 U CN 201821015119U CN 208430120 U CN208430120 U CN 208430120U
- Authority
- CN
- China
- Prior art keywords
- poultry
- reaction kettle
- valve
- bottle
- aquatic products
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P30/00—Technologies relating to oil refining and petrochemical industry
- Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
Landscapes
- Fats And Perfumes (AREA)
Abstract
The utility model relates to bioenergies to utilize technical field, more particularly to a kind of device using poultry and aquatic products waste grease preparation biodiesel, including ester exchange reaction device, magnetic recovery device and high temperature evaporation device, the ester exchange reaction device is connected to magnetic recovery device, and the magnetic recovery device is connected to high temperature evaporation device；It is provided with methanol, magnetic solid catalyst and waste oil in the ester exchange reaction device, further includes rotating separation device, glycerol recyclable device and diesel oil collection device.The recycling of magnetic catalyst may be implemented in the utility model, and can efficiently separate the methanol and glycerol after reaction.
Description
Technical field
The utility model relates to bioenergies to utilize technical field, utilize poultry and aquatic products abandoned oil more particularly to a kind of
The device of rouge preparation biodiesel.
Background technique
With the high speed development of today's society, just growing day by day, we are being enjoyed for demand of the people to the energy and consumption
While the various energy offer convenience for us, the energy is still suffered from using bring environmental problem, in particular, fossil fuel makes
With being the main reason for leading to greenhouse effects.Therefore, it develops a kind of clean reproducible energy and replaces existing fossil energy, have
Highly important meaning.Biodiesel belongs to biomass energy, is the energy using biomass as carrier, it derives from solar energy, with
The characteristics of chemical energy form is stored in biomass, meets renewable energy.
In the technique of preparing biodiesel by ester interchange, the selection of raw material and catalyst and the place of by-product glycerin
Reason becomes key.Raw material mainly include edible fats and unedible oil rouge, derived from discarded poultry and seafood oils (such as from
The liquid fat being extract in slaughter animals leftover bits and pieces and chicken and duck and the greasyfoot of fish) or kitchen waste oil as non-
Edible oil and fat raw material also gradually obtain the attention of people.Common catalyst is mainly homogenous acid or base catalysts and heterogeneous acid
Base catalyst.By-product glycerin needs are able to separate simultaneously and use is in other field.
Main problems faced is that prices of raw materials valuableness is difficult to obtain and catalyst efficiency uses low, recycling at present
Difficulty and by-product glycerin are difficult to the problem of handling.
Utility model content
In order to overcome the deficiencies of the prior art, the utility model provides prepares biology using poultry and aquatic products waste grease
The service efficiency of catalyst can be improved in the device of diesel oil, facilitates the recycling of catalyst and can be effectively treated what reaction generated
Glycerol.
The utility model adopts the following technical solutions: a kind of dress using poultry and aquatic products waste grease preparation biodiesel
It sets, including ester exchange reaction device, magnetic recovery device and high temperature evaporation device, the ester exchange reaction device and magnetic recovery
Device connection, the magnetic recovery device are connected to high temperature evaporation device；Methanol, magnetic are provided in the ester exchange reaction device
Property solid catalyst and waste oil.The ester exchange reaction device includes reaction kettle, and the upper end of the reaction kettle is equipped with first entrance
And second entrance, the lower end of the reaction kettle are equipped with outlet, the outer surface ring set of the reaction kettle has the first heating mantle, described anti-
The outlet of kettle is answered to be connected to by drain pipe with magnetic recovery device, the second entrance is connected by exhaust pipe and high temperature evaporation device
It is logical.
Further, further include rotating separation device, glycerol recyclable device and diesel oil collection device, arranged from high temperature evaporation device
Solution out enters rotating separation device and is separated, and solution obtained after separation separately flows into glycerol recyclable device and magnetic time
In receiving apparatus.
Further, the upper surface of the reaction kettle is equipped with motor, and the motor shaft vertical of the motor extends downwardly into reaction kettle
Inner cavity after be fixedly connected with shaft, Teflon stir bar is laid in shaft.
Further, the exit is equipped with the first valve, and first valve is connected to drain pipe, and drain pipe is close to magnetic
One end of recyclable device is equipped with the second valve, and the magnetic recovery device includes removal of impurities bottle, and the outer wall of the removal of impurities bottle is equipped with magnetic
The exit of iron, the removal of impurities bottle is equipped with third valve, and third valve be connected to by hose with the pump housing, the pump housing pass through liquid supply pipe and
The connection of high temperature recyclable device, liquid supply pipe are equipped with the 4th valve close to one end of the pump housing.
Further, the high temperature recyclable device includes heating bottle, and the outer wall ring set of the heating bottle has the second heating mantle, institute
The top for stating heating bottle is equipped with gas outlet, and gas outlet is connected to exhaust pipe, and the lower section of the heating bottle is equipped with tap hole.
Further, the rotating separation device includes centrifuge, and centrifuge tube is equipped in the centrifuge, tap hole discharge
Liquid flows into centrifuge tube, and the liquid in centrifuge tube is respectively implanted glycerol recyclable device or diesel oil collection device after centrifugation
In.
Further, the exhaust pipe is equipped with the 5th valve close to one end of reaction kettle.
Compared with prior art, the utility model has the beneficial effects that
1) the utility model uses poultry and aquatic products waste grease or discarded kitchen oil as raw material, cheap easy
It can also accomplish waste utilization while obtaining.While catalyst recycles, it can be used for the production of next stage, accomplish biodiesel
Ensured sustained development production, substantially increases production efficiency.
2) extra methanol is recycled, and for the production of next stage, saves raw material, save the cost；Collecting product bavin
While oily, by-product glycerin can also be collected and for other aspects.
3) preparation process is simple, is not necessarily to high temperature, high-tension apparatus.And used equipment has versatility, can reduce
Cost of investment.
Detailed description of the invention
The accompanying drawings constituting a part of this application is used to provide further understanding of the present application, and the application's shows
Meaning property embodiment and its explanation are not constituted an undue limitation on the present application for explaining the application.
Fig. 1 is the overall structure diagram of the utility model embodiment 1；
Fig. 2 is the overall structure diagram of the utility model embodiment 2.
In figure, the 1, first heating mantle；2, reaction kettle；3, first entrance；4, motor；5, shaft；6, Teflon stir
Stick；7, exhaust pipe；7A, the 5th valve；8, second entrance；9, gas outlet；10, heating bottle；11, the second heating mantle；12, tapping
Mouthful；13, liquid supply pipe；14, the 4th valve；15, bottom plate；16, the pump housing；17, third valve；18, clean bottle；19, magnet；20,
Two valves；21, drain pipe；22, the first valve；23, centrifuge；24, centrifuge tube.
Specific embodiment
It is noted that following detailed description is all illustrative, it is intended to provide further instruction to the application.Unless another
It indicates, all technical and scientific terms used herein has usual with the application person of an ordinary skill in the technical field
The identical meanings of understanding.
It should be noted that term used herein above is merely to describe specific embodiment, and be not intended to restricted root
According to the illustrative embodiments of the application.
As used herein, unless the context clearly indicates otherwise, otherwise singular is also intended to include plural shape
Formula, additionally, it should be understood that, when the term " comprising " and/or " including " is used in this specification, indicate in the presence of special
Sign, step, operation, device, component and/or their combination.
Embodiment 1, as shown in Figure 1, a kind of device using poultry and aquatic products waste grease preparation biodiesel, including ester
Exchange reaction device, magnetic recovery device and high temperature evaporation device, the ester exchange reaction device are connected to magnetic recovery device,
The magnetic recovery device is connected to high temperature evaporation device；Methanol is provided in the ester exchange reaction device, magnetic retention is urged
Agent and waste oil.
The ester exchange reaction device includes reaction kettle 2, and the upper end of the reaction kettle 2 is equipped with first entrance 3 and second and enters
The lower end of mouth 8, the reaction kettle 2 is equipped with outlet, and the outer surface ring set of the reaction kettle 2 has the first heating mantle 1, the reaction kettle
2 outlet is connected to by drain pipe 21 with magnetic recovery device, and the second entrance 8 passes through exhaust pipe 7 and high temperature evaporation device
Connection.
The upper surface of the reaction kettle 2 is equipped with motor 4, and 4 axis of motor of the motor 4 protrudes into reaction kettle 2 straight down
It is fixedly connected behind inner cavity with shaft 5, Teflon stir bar 6 is laid in shaft 5.
The exit is equipped with the first valve 22, and first valve 22 is connected to drain pipe 21, and drain pipe 21 is close to magnetic
Property recyclable device one end be equipped with the second valve 20, the magnetic recovery device includes removal of impurities bottle 18, the removal of impurities bottle 18 it is outer
Wall is equipped with magnet 19, and the exit of the removal of impurities bottle 18 is equipped with third valve 17, and third valve 17 is connected by hose and the pump housing 16
Logical, the pump housing 16 is connected to by liquid supply pipe 13 with high temperature recyclable device, and liquid supply pipe 13 is equipped with the 4th valve close to one end of the pump housing 16
14。
The high temperature recyclable device includes heating bottle 10, and the outer wall ring set of the heating bottle 10 has the second heating mantle 11, institute
The top for stating heating bottle 10 is equipped with gas outlet 9, and gas outlet 9 is connected to exhaust pipe 7, and the outer wall of exhaust pipe 7 is coated with condensing unit
(how using condensing unit the methanol gas in exhaust pipe 7 to be liquefied and belong to the prior art, details are not described herein again).It is described to add
The lower section of hot bottle 10 is equipped with tap hole 12.
The exhaust pipe 7 is equipped with the 5th valve 7A close to one end of reaction kettle 2.
Removal of impurities bottle 18 is detachable structure, removal of impurities bottle 18 can be dismantled and clean its inner wall, not show to remove in attached drawing
How miscellaneous bottle 18 is dismantled, and those skilled in the art can be with self-setting.In order to avoid the magnetic catalyst of omission flows into the pump housing,
One layer of strainer can be set in the exit of removal of impurities bottle, solution successively flows into the pump housing through filter screen and hose.
In addition reaction kettle 2, removal of impurities bottle 18, the pump housing 16 and heating bottle 10 are all mounted on bottom plate 15 by bracket.
Glycerol recyclable device and diesel oil collection device can be easy to collect the storage device of liquid using bottle body, bucket etc.,
The application is without limitation, while the application does not provide the attached drawing of glycerol recyclable device and diesel oil collection device yet, herein not
It is considered to be unclear.
Working principle: when using the present apparatus, kitchen waste oil, methanol and magnetic catalyst are sent into from first entrance 3
Reaction kettle 2 carries out esterification, heats entire reaction kettle 2 using the first heating mantle 1 while esterification carries out；Work as esterification
After completion of the reaction, open the first valve 22, the second valve 20, third valve 17 and 14 solution of the 4th valve and magnetic catalyst from
Drain pipe 21 flows into the removal of impurities bottle 18 of magnetic recovery device, because of the presence of magnet 19, magnetic catalyst is attracted to removal of impurities
On 18 inner walls of bottle, then mixed solution is pumped into heating bottle 10 from the pump housing 16, and the second heating mantle 11 of starting reaches methanol
Enter exhaust pipe 7 from gas outlet 9 after boiling point, can become liquid again by the condensing unit on exhaust pipe 7, liquid methanol from
Second entrance 8 reenters in reaction kettle 2.
After reaction carries out primary, the first valve 22, the second valve 20 are closed.With the 4th valve 14, will removal of impurities bottle 18 with
Drain pipe 21 and hose disconnect, and the inner surface of miscellaneous bottle 18 is brushed using polytetrafluoroethylene (PTFE) brush, is brushing miscellaneous 18 inner surface of bottle
While rinse and recycle using n-hexane, magnetic catalyst after the recovery is placed in reaction kettle 2 again in next secondary response.
Teflon stir bar is driven to rotate using motor in esterification reaction process, so that reaction speed is faster.
In esterification reaction process, closes the first valve, the 5th valve and first entrance and reaction kettle is made to keep sealed shape
State.
Embodiment 2, as shown in Fig. 2, the other structures of the present embodiment are same as Example 1, difference place is, further includes
Rotating separation device, glycerol recyclable device and diesel oil collection device.The rotating separation device includes centrifuge 23, the centrifugation
Centrifuge tube 24 is equipped in machine 23, the liquid that tap hole 12 is discharged flows into centrifuge tube 24, and the liquid in centrifuge tube 24 is by centrifugation
After be respectively implanted in glycerol recyclable device or diesel oil collection device.
Working principle: successively accepting the solution that tap hole 12 leaves using centrifuge tube 24, then by centrifuge tube 24 be put into from
It being centrifuged in scheming 23, the revolving speed of centrifuge 23 is maintained at 8000 and turns left the right side, after the glycerol and diesel oil layering in centrifuge tube 24,
Glycerol and diesel oil are poured into respectively in glycerol recyclable device and diesel oil acquisition device.
The foregoing is merely preferred embodiment of the present application, are not intended to limit this application, for the skill of this field
For art personnel, various changes and changes are possible in this application.Within the spirit and principles of this application, made any to repair
Change, equivalent replacement, improvement etc., should be included within the scope of protection of this application.
Claims (7)
1. a kind of device using poultry and aquatic products waste grease preparation biodiesel, characterized in that filled including ester exchange reaction
It sets, magnetic recovery device and high temperature evaporation device, the ester exchange reaction device are connected to magnetic recovery device, the magnetism time
Receiving apparatus is connected to high temperature evaporation device；Methanol, magnetic solid catalyst and waste oil are provided in the ester exchange reaction device；
The ester exchange reaction device includes reaction kettle, and the upper end of the reaction kettle is equipped with first entrance and second entrance, described
The lower end of reaction kettle is equipped with outlet, and the outer surface ring set of the reaction kettle has the first heating mantle, and the outlet of the reaction kettle passes through
Drain pipe is connected to magnetic recovery device, and the second entrance is connected to by exhaust pipe with high temperature evaporation device.
2. utilizing the device of poultry and aquatic products waste grease preparation biodiesel as described in claim 1, characterized in that also wrap
Rotating separation device, glycerol recyclable device and diesel oil collection device are included, the solution being discharged from high temperature evaporation device enters rotation point
It is separated from device, solution obtained after separation separately flows into glycerol recyclable device and magnetic recovery device.
3. utilizing the device of poultry and aquatic products waste grease preparation biodiesel as described in claim 1, characterized in that described
The upper surface of reaction kettle is equipped with motor, the motor shaft vertical of the motor extend downwardly into behind the inner cavity of reaction kettle with shaft is fixed connects
It connects, Teflon stir bar is laid in shaft.
4. utilizing the device of poultry and aquatic products waste grease preparation biodiesel as claimed in claim 3, characterized in that described
Exit is equipped with the first valve, and first valve is connected to drain pipe, and drain pipe is equipped with close to one end of magnetic recovery device
Second valve, the magnetic recovery device include removal of impurities bottle, and the outer wall of the removal of impurities bottle is equipped with magnet, the outlet of the removal of impurities bottle
Place is equipped with third valve, and third valve is connected to by hose with the pump housing, and the pump housing is connected to by liquid supply pipe with high temperature recyclable device, supplies
Liquid pipe is equipped with the 4th valve close to one end of the pump housing.
5. utilizing the device of poultry and aquatic products waste grease preparation biodiesel as claimed in claim 4, characterized in that described
High temperature recyclable device includes heating bottle, and the outer wall ring set of the heating bottle has the second heating mantle, and the top of the heating bottle is equipped with
Gas outlet, gas outlet are connected to exhaust pipe, and the lower section of the heating bottle is equipped with tap hole.
6. utilizing the device of poultry and aquatic products waste grease preparation biodiesel as claimed in claim 2, characterized in that described
Rotating separation device includes centrifuge, and centrifuge tube is equipped in the centrifuge, and the liquid of tap hole discharge flows into centrifuge tube, from
Liquid in heart pipe is respectively implanted in glycerol recyclable device or diesel oil collection device after centrifugation.
7. utilizing the device of poultry and aquatic products waste grease preparation biodiesel as described in claim 1, characterized in that described
Exhaust pipe is equipped with the 5th valve close to one end of reaction kettle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821015119.6U CN208430120U (en) | 2018-06-28 | 2018-06-28 | A kind of device using poultry and aquatic products waste grease preparation biodiesel |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821015119.6U CN208430120U (en) | 2018-06-28 | 2018-06-28 | A kind of device using poultry and aquatic products waste grease preparation biodiesel |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208430120U true CN208430120U (en) | 2019-01-25 |
Family
ID=65099272
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821015119.6U Expired - Fee Related CN208430120U (en) | 2018-06-28 | 2018-06-28 | A kind of device using poultry and aquatic products waste grease preparation biodiesel |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208430120U (en) |
-
2018
- 2018-06-28 CN CN201821015119.6U patent/CN208430120U/en not_active Expired - Fee Related
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104893961B (en) | The kitchen castoff energy and fertilizer integrated treatment unit and method | |
| US20110245523A1 (en) | Single step transesterification of biodiesel feedstock using a gaseous catalyst | |
| CN102021082A (en) | Method for preparing fatty acid methyl ester and glycerol from kitchen waste oil by utilizing acid-base two-step method | |
| CN210215295U (en) | Eucalyptol rectifying device | |
| CN208430120U (en) | A kind of device using poultry and aquatic products waste grease preparation biodiesel | |
| CN103194314B (en) | Method for treating waste oil | |
| CN102816636A (en) | Extraction method for microalgae grease | |
| CN202430144U (en) | D-bomeol extraction equipment suitable for field sites | |
| CN105779105A (en) | Method for extracting biodiesel based on waste coffee grounds | |
| CN105647652A (en) | Microalgae biodiesel production device | |
| CN102344886A (en) | Methane generating pit with methane generation rate increased by complementary solar photothermal power generation and wind power generation | |
| CN209602489U (en) | A kind of Rosa Damascana extraction element | |
| CN201144245Y (en) | Novel automatic feed and discharge large rotary cracking mixing methane tank | |
| US20150267145A1 (en) | Single step transesterification of biodiesel feedstock using a gaseous catalyst | |
| CN207136752U (en) | A kind of coffee machine | |
| CN104998887B (en) | The damp and hot pretreatment unit of homogeneous de-oiling integration steam spin and preprocess method | |
| CN102676311A (en) | Reaction device for manufacturing biodiesel | |
| CN204281719U (en) | A kind of mobile biodiesel preparation facilities | |
| CN209576479U (en) | A kind of biodiesel raw material mixing apparatus | |
| CN208115287U (en) | A kind of environment-friendly type biodiesel filter | |
| CN106902546B (en) | One kind extracting nickel sulfate hydraulic mixing energy conservation extraction equipment from old and useless battery | |
| CN206204186U (en) | A kind of continuous esterification separation equipment of pure fatty acid high | |
| CN208627290U (en) | A kind of reaction kettle with circulating cooling function | |
| CN201258326Y (en) | Pneumatic biogas residue remover | |
| CN114431042B (en) | Micro-grid agricultural planting greenhouse integrating wind energy, light energy and biomass energy |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190125 Termination date: 20210628 |