CN208406988U - For producing the device of acyl chlorides - Google Patents

For producing the device of acyl chlorides Download PDF

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Publication number
CN208406988U
CN208406988U CN201820922831.8U CN201820922831U CN208406988U CN 208406988 U CN208406988 U CN 208406988U CN 201820922831 U CN201820922831 U CN 201820922831U CN 208406988 U CN208406988 U CN 208406988U
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China
Prior art keywords
kettle
acyl chlorides
light
producing
pipeline
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Active
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CN201820922831.8U
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Chinese (zh)
Inventor
侯乐宝
王思言
刘丹
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Fengyi Surface Active Material (lianyungang) Co Ltd
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Fengyi Surface Active Material (lianyungang) Co Ltd
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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The utility model relates to a kind of for producing the device of acyl chlorides, wherein the device includes photochemical kettle and catches up with light kettle, the photochemical kettle and catching up with is connected between light kettle by pipeline, the pipeline, photochemical kettle and light kettle is caught up with to all have four fluorine structures of lining, four fluorine structure of lining successively includes the stainless steel wire stratum reticulare for being set to carbon steel substrates layer, the polytetrafluoroethylene ethylene layer for being set to the stainless steel wire stratum reticulare.Using the utility model for producing the device of acyl chlorides, solves the problems, such as equipment and corrosive pipeline in acyl chlorides production process, reduce leakage, eliminate safe hidden trouble, while guaranteeing product quality.

Description

For producing the device of acyl chlorides
Technical field
The utility model relates to acyl chlorides technical fields, in particular to a kind of for producing the device of acyl chlorides.
Background technique
Acyl chlorides is a kind of carboxylic acid derivates, is a kind of important organic intermediate, is widely used in producing surfactant, make The industries such as paper gluing agents, polymeric initiator.In traditional acyl chlorides production equipment, glassed steel reaction vessels, connecting tube are mostly used Road generally uses stainless steel material or glass lined pipeline.Long-time service has the following problems:
1) for stainless steel material, due to there is acidic materials in acyl chlorides production, chloride ion can destroy metal oxide film protection Layer forms spot corrosion or pitting corrosion, and perishable perforation, there are biggish security risks, need periodic inspection or replacement pipeline, increase Production cost, while also influencing execute-in-place environment.
2) for enamel material, although corrosion-resistant, enamel material is in temperature change and under having Vibration Condition, very It is easy burst porcelain, once burst porcelain, glassed steel reaction vessels and enamel pipeline can be by the acid material corrosion failures in acyl chlorides.Practice card Bright, the equipment of enamel material service life in acyl chlorides production is short, easily leaks, there are very big security risks.
Utility model content
The shortcomings that the purpose of the utility model is to overcome the above-mentioned prior arts provides one kind and is able to solve acyl chlorides production In the process equipment and the problem of corrosive pipeline, reduce and leak, eliminate safe hidden trouble while guaranteeing that product quality is used to producing acyl The device of chlorine.
To achieve the goals above, the device for producing acyl chlorides of the utility model has following constitute:
The device includes photochemical kettle and catches up with light kettle, and the photochemical kettle and catching up with is connected between light kettle by pipeline, The pipeline, photochemical kettle and light kettle is caught up with to all have four fluorine structures of lining, four fluorine structure of lining successively includes being set to carbon steel The stainless steel wire stratum reticulare of basal layer, the polytetrafluoroethylene ethylene layer for being set to the stainless steel wire stratum reticulare, in prefabricated reaction kettle First pre- plant, welding wire, steel mesh heat F4 powder and carry out roller coating, make polytetrafluoroethylene (PTFE) and steel wire as reinforcing rib on mould inner wall Net, which fuses into one, firmly to be adhered on the steel plate, then the treatment process such as heated.
The photochemical kettle and catch up with light kettle, can be used under conditions of positive/negative-pressure, high temperature, deep-etching, in 200 DEG C of temperature and 40 millipascal of vacuum does not play packet and does not inhale flat not dilatancy, reached the bodies such as steel fluorine hereinafter, shock heating quenching blocked operation." steel wire Teflon lined " efficiently solves damage of two kinds of material expansion differences to lining, ensure that steel lining tetrafluoro equipment Service life.
The photochemical kettle and light kettle is caught up with to be provided with stirring structure.
Using the utility model for producing the device of acyl chlorides, equipment and corrosive pipeline in acyl chlorides production process are solved Problem reduces leakage, eliminates safe hidden trouble, while guaranteeing product quality.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the device for producing acyl chlorides of the utility model.
Appended drawing reference
1 photochemical kettle
2 catch up with light kettle
3 lining tetrafluoro pipelines
4 stirring structures
Specific embodiment
In order to more clearly describe the technology contents of the utility model, carry out combined with specific embodiments below into one The description of step.
As shown in Figure 1, the device provided by the utility model for producing acyl chlorides includes photochemical kettle 1 and catches up with light kettle 2, it is described Photochemical kettle 1 and catching up be connected between light kettle 2 by pipeline 3, the pipeline, photochemical kettle 1 and light kettle 2 is caught up with to all have lining tetrafluoro Structure, four fluorine structure of lining successively include stainless steel wire stratum reticulare, polytetrafluoroethylene ethylene layer, wherein in four fluorine structure of lining Stainless steel wire stratum reticulare adjacent to carbon steel substrates layer inner surface be arranged.
Lining tetrafluoro (F4) main component is polytetrafluoroethylene (PTFE), has the characteristics that antiacid alkali resistant, resists various organic solvents, almost Insoluble in all solvents.Meanwhile the coefficient of friction for serving as a contrast F4 is extremely low, it can be to avoid the corrosion of equipment pipe, and can bear certain Negative pressure.Therefore, in conjunction with the case where the process characteristic and temperature, pressure of acyl chlorides production, using molding lining F4 pipeline and " steel wire is poly- Tetrafluoroethene lining " serves as a contrast tetrafluoro reactor.
In a kind of preferably embodiment, the photochemical kettle and light kettle is caught up with to be provided with stirring structure 4.
Using the utility model for producing the device of acyl chlorides, solve in acyl chlorides production process equipment and corrosive pipeline with And product color the problem of deepening, strict control metal ion enter in acyl chlorides product, improve acyl chlorides product quality, reduce Because of leakage of perforating caused by equipment corrosion, eliminate safe hidden trouble, it can economy and efficient delay apparatus service life and guarantor Demonstrate,prove the stability of product.
In this description, the utility model is described with reference to its specific embodiment.But it is clear that still may be used With the spirit and scope that various modification can be adapted and converts without departing from the utility model.Therefore, the description and the appended drawings should be considered It is illustrative and be not restrictive.

Claims (2)

1. a kind of for producing the device of acyl chlorides, which is characterized in that the device includes photochemical kettle and catches up with light kettle, the light Change kettle and catching up with to be connected between light kettle by pipeline, the pipeline, photochemical kettle and light kettle is caught up with to all have four fluorine structures of lining, it is described Four fluorine structure of lining successively include the stainless steel wire stratum reticulare for being set to carbon steel substrates layer, be set to the stainless steel wire stratum reticulare Polytetrafluoroethylene ethylene layer.
2. according to claim 1 for producing the device of acyl chlorides, which is characterized in that the photochemical kettle and catch up with light kettle equal It is provided with stirring structure.
CN201820922831.8U 2018-06-14 2018-06-14 For producing the device of acyl chlorides Active CN208406988U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820922831.8U CN208406988U (en) 2018-06-14 2018-06-14 For producing the device of acyl chlorides

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820922831.8U CN208406988U (en) 2018-06-14 2018-06-14 For producing the device of acyl chlorides

Publications (1)

Publication Number Publication Date
CN208406988U true CN208406988U (en) 2019-01-22

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820922831.8U Active CN208406988U (en) 2018-06-14 2018-06-14 For producing the device of acyl chlorides

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CN (1) CN208406988U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114797735A (en) * 2021-11-08 2022-07-29 开封华瑞化工新材料股份有限公司 Device for preparing isooctyl chloroformate from phosgene

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114797735A (en) * 2021-11-08 2022-07-29 开封华瑞化工新材料股份有限公司 Device for preparing isooctyl chloroformate from phosgene

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