CN208378421U - For producing the quencher of insoluble sulfur - Google Patents
For producing the quencher of insoluble sulfur Download PDFInfo
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- CN208378421U CN208378421U CN201821029565.2U CN201821029565U CN208378421U CN 208378421 U CN208378421 U CN 208378421U CN 201821029565 U CN201821029565 U CN 201821029565U CN 208378421 U CN208378421 U CN 208378421U
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- quencher
- gland
- quenching
- pedestal
- insoluble sulfur
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Abstract
The utility model provides a kind of for producing the quencher of insoluble sulfur comprising quencher pedestal, quencher gland and quencher export enlarged tube, and quencher gland is fixedly connected on quencher pedestal；It is provided with multiple cone faces on quencher gland, forms quenching liquid cavity, a quenching liquid is provided in the side wall surface of quencher gland and introduces pipe, quenching liquid introduces pipe and is connected to quenching liquid cavity, so that fluid forms high pressure ring-type cone liquid level by the gap in cone face；A quenching material feed pipe is additionally provided on quencher gland, the centre of quencher pedestal is provided with an expansion chamber, and quenching liquid cavity and quenching material feed pipe are connected to expansion chamber；Quencher outlet enlarged tube is mounted on the bottom end of quencher pedestal, is connected to expansion chamber.The quenched yield of the utility model obviously increases, and product quality has larger promotion, preferable at powder effect, reduces subsequent treatment process, reduces production cost and security risk.
Description
Technical field
It is the utility model relates to quencher field, in particular to a kind of for producing the quencher of insoluble sulfur.
Background technique
In the prior art, insoluble sulfur is that sulphur powder is heated to boiling (444.6 degrees Celsius), is inclined to anxious in cold water
The elastic sulphur of transparent obtained by cold, amorphous chain structure.Or can also dilute overheat sulphur steam with inert gas,
Be sprayed in cold mist be cooled to 90 degrees Celsius or less be made, or by sulfur in lump form be dissolved in ammonia immediately spray drying obtain.
In general, the production method of insoluble sulfur is broadly divided into vapour phase processes and liquid phase method.It is most of to use vapour phase processes technique
It is produced, the production technology that vapor phase method produces insoluble sulfur is more mature, but there are equipment throwings for vapour phase processes production technology
The defects of money is big, energy consumption is high, inflammable and explosive, also just constrains the development of insoluble sulfur production.In addition, the liquid phase method work used
Skill is substantially poured into or dropping type, and the insoluble sulfur crude product of production is in bulk, conversion insufficient due to polymerizeing and cooling down
Rate is lower.
It is used to produce the quencher of insoluble sulfur at present, quenching object injects directly into quenching liquid or other are simple
Mixing sprays into quenching apparatus at bulk, is mechanically pulverized again after filtering, drying, increases pulverizing process, improved
Cost of investment and production cost are easy to appear dust explosion simultaneously because being mechanically pulverized to powdery.
In view of this, those skilled in the art are urgently in developing a kind of novel more effective safer quencher.
Utility model content
The technical problems to be solved in the utility model be in order to overcome in the prior art quencher it is at high cost, be easy to appear powder
The defect of dust explosion provides a kind of for producing the quencher of insoluble sulfur.
The utility model is to solve above-mentioned technical problem by following technical proposals:
It is a kind of for producing the quencher of insoluble sulfur, it is characterized in that, the quencher includes quencher pedestal, quenches
Firearm gland and quencher export enlarged tube, and the quencher gland is fixedly connected on the quencher pedestal；
It is provided with multiple cone faces on the quencher gland, forms quenching liquid cavity, the side wall of the quencher gland
It is provided with a quenching liquid on face and introduces pipe, the quenching liquid introduces pipe and is connected to the quenching liquid cavity, so that fluid passes through institute
The gap for stating cone face forms high pressure ring-type cone liquid level；
A quenching material feed pipe, the centre setting of the quencher pedestal are additionally provided on the quencher gland
There is an expansion chamber, the quenching liquid cavity and the quenching material feed pipe are connected to the expansion chamber；
The quencher outlet enlarged tube is mounted on the bottom end of the quencher pedestal, is connected to the expansion chamber.
One embodiment according to the present utility model, there are two cone faces for setting on the quencher gland.
One embodiment according to the present utility model is provided with close between the quencher gland and the quencher pedestal
Cover gasket.
One embodiment according to the present utility model, between the quencher pedestal and the cone face of the quencher gland
Gap, the thickness by adjusting the sealing surface gasket is adjusted.
One embodiment according to the present utility model, the sealing surface gasket with a thickness of 0.5-5mm, in the expansion chamber
Pressure be 0.5-1.3MPa.
One embodiment according to the present utility model, the expansion chamber export enlarged tube from the quencher with an angle
It is injected in quenching apparatus, the angle ranging from 5-30 °.
One embodiment according to the present utility model passes through bolt between the quencher pedestal and the quencher gland
Nut connection.
One embodiment according to the present utility model, the expansion chamber are from top to bottom in gradual shrinkage.
One embodiment according to the present utility model is provided with equipment connecting flange at the lower end closing in of the expansion chamber,
For connecting with quenching apparatus, and the lower end of the expansion chamber is closed up and is connect with quencher outlet enlarged tube.
One embodiment according to the present utility model, the end that the quenching liquid introduces pipe are provided with charging flange.
One embodiment according to the present utility model, the angle in the cone face are 45-75 °.
The positive effect of the utility model is:
The quencher that the utility model is used to produce insoluble sulfur is quenched by gaseous phase materials and the common material spray of liquid phase material
Fire forms a kind of particle or powder material.Since two kinds of substance contact specific surface areas increase, quenched yield obviously increases
Adding, product quality has larger promotion, and it is preferable at powder effect, reduce subsequent treatment process, reduces production cost and safety
Risk.
Detailed description of the invention
The above and other feature of the utility model, property and advantage will pass through with reference to the accompanying drawings and examples
It describes and becomes apparent, identical appended drawing reference always shows identical feature in the accompanying drawings, in which:
Fig. 1 is the structural schematic diagram for the quencher that the utility model is used to produce insoluble sulfur.
Specific embodiment
It is practical to this below in conjunction with attached drawing for the above objects, features, and advantages of the utility model can be clearer and more comprehensible
Novel specific embodiment elaborates.
The embodiments of the present invention are described with detailed reference to attached drawing now.Now with detailed reference to the excellent of the utility model
Embodiment is selected, its example is shown in the drawings.In the case of any possible, will be come in all the appended drawings using identical label
Indicate the same or similar part.
In addition, although term used in the utility model is selected from public term, this reality
Some terms mentioned in novel specification may be applicant by his or her judgement come selection, and detailed meanings exist
Illustrate in the relevant portion of description herein.
Furthermore, it is desirable that not only by used actual terms, and be also to the meaning contained by each term
To understand the utility model.
Fig. 1 is the structural schematic diagram for the quencher that the utility model is used to produce insoluble sulfur.
As shown in Figure 1, the utility model discloses a kind of for producing the quencher of insoluble sulfur comprising quencher
Pedestal 10, quencher gland 20 and quencher export enlarged tube 30, and quencher gland 20 is fixedly connected on quencher pedestal 10
On.Preferably, it is connected between quencher pedestal 10 and quencher gland 20 by bolt 40 and nut 50.
It is provided with multiple cone faces 21 on quencher gland 20, forms quenching liquid cavity a, quencher of illustrating in the present embodiment
There are two cone face 21 (as shown in Figure 1) for setting on gland 20.Certainly two cone faces 21 are only for example herein, in practice cone
The quantity in face 21 is unrestricted, determines with specific reference to actual condition.In addition, the also not office of the structure on quencher gland 20 here
It is limited to that cone face 21 is arranged, is only for example herein, cone face 21 can also be substituted using the structure of other shapes, specific root
It is determined according to actual condition.It is provided with a quenching liquid in the side wall surface of quencher gland 20 and introduces pipe 22, quenching liquid is introduced into pipe 22
It is connected to quenching liquid cavity a, so that fluid forms high pressure ring-type cone liquid level by the gap in cone face 21.It is introduced in quenching liquid
The end of pipe 22 is provided with charging flange 23.The angle in cone face 21 is preferably 45-75 °, unsuitable bigger than normal and less than normal.Quenching liquid draws
The tilt angle for entering pipe 22 is identical as the quencher outlet tilt angle of enlarged tube 30.
It is additionally provided with a quenching material feed pipe 24 on quencher gland 20, is arranged in the centre of quencher pedestal 10
There is an expansion chamber 11, quenching liquid cavity a and quenching material feed pipe 24 are connected to expansion chamber 11.Quencher, which exports enlarged tube 30, pacifies
Mounted in the bottom end of quencher pedestal 10, it is connected to expansion chamber 11.
Preferably, sealing surface gasket 60 is provided between quencher gland 20 and quencher pedestal 10.The sealing surface
Gasket with a thickness of 0.5-5mm.Gap between quencher pedestal 10 and the cone face 21 of quencher gland 20, passes through adjusting
The thickness of sealing surface gasket 60 between quencher pedestal 10 and quencher gland 20 is adjusted.By adjusting gap size
Controllable quenching liquid jet velocity, thus the shearing and contact effect of two kinds of substances of control.
Meanwhile expansion chamber pressure is controlled, to influence solid material quenching effect and granular size.The bulbs of pressure are got over
The particle of small formation is bigger than normal, but has a limiting value, not only the small particle that cannot be formed to a certain extent is also easy to cause spray head stifled
Plug.Pressure limit in expansion chamber described herein is preferably 0.5-1.3MPa.Pressure is lower than 0.5MPa, and shearing force is not achieved, no
Particle can be formed, spray head is caused to block.Pressure is higher than 1.3MPa, and annular space is too small, and difficulty of processing is larger, and is easy to be blocked up by foreign matter
Plug, causes bias current.The bigger pressure in gap is smaller, and flow velocity is smaller, and shearing force is smaller.Pressure is smaller, then the particle formed is bigger than normal.
It is further preferred that expansion chamber 11 is from top to bottom in gradual shrinkage.It is provided at the lower end closing in of expansion chamber 11
Standby connecting flange 12, for connecting with quenching apparatus, and the lower end of expansion chamber 11 is closed up and is connect with quencher outlet enlarged tube 30.
It is described according to above structure, the quencher that the utility model is used to produce insoluble sulfur, which mainly relies on to come from, to be quenched
The fluid that fiery liquid introduces pipe 22 forms high pressure ring-type cone liquid level by the gap in cone face, quenches material feed pipe 24 with coming from
Gaseous fluid formation continuously contact with, form uniform solid-liquid mixture and spray into expansion chamber.The shape at the closing in of expansion chamber 11
At certain fluid-tight, and finally, by cavity pressure, from quencher outlet, enlarged tube 30 is injected in quenching apparatus at a certain angle.
The angle is preferably 5-30 °, this kind of purpose of design, which enters low-pressure area by higher-pressure region for material, the process slowly expanded, together
When guarantee jeting effect, preferably at powder, control into powder particles size.Material is set to spray into quenching apparatus at a certain angle simultaneously
It is interior, avoid materials from spattering from causing material wall sticking phenomenon to equipment inner wall.
Further specifically, quenching liquid is delivered to quencher by external conveying equipment, pipe 22 is introduced by quenching liquid
Into quencher.Cyclic annular cone liquid level is presented in gap between quencher pedestal 10 and the cone face of quencher upper press cover 20
Expansion chamber 11 is sprayed into, quenching is sufficiently mixed with the gaseous phase materials from quenching material feed pipe 24, forms solid-liquid mixture.
Then, certain fluid-tight is formed in the closing in of expansion chamber 11, is finally exported and is expanded by quencher with certain pressure
Big pipe 30 is injected into quenching apparatus, is completed entire quenching process, is ultimately formed granular material.
In addition, can be realized in the application by adjusting the gap between quencher pedestal and the cone face of quencher gland
The variation of scheme, overall construction and without big variation.Lower section horn mouth length has with tank diameter and level control height
It closes, distance at least controls 50cm or more between enlarged tube outlet and liquid level, there is a further expansion mistake after allowing material to come out
Journey.It is too low easily cause liquid level materials from spattering to enlarged tube formed up and down recoil.Liquid level is unsuitable too low simultaneously, is sprayed according to material
Expansion status is subject to and sprays material and fully enter liquid level hereinafter, being not directly contacted with equipment inner wall.Height adjustment can be by continuous
Physics cutting, which shortens, expands length of tube.
In conclusion the quencher that the utility model is used to produce insoluble sulfur is total by gaseous phase materials and liquid phase material
It is quenched with material spray, forms a kind of particle or powder material.Since two kinds of substance contact specific surface areas increase, quenched yield
It obviously increasing, product quality has larger promotion, and it is preferable at powder effect, reduce subsequent treatment process, reduces production cost
And security risk.
It is mainly used in production insoluble sulfur, it can also be used to rapid cooling Cooling Quenching powder etc. after the gasification of other products
Technique, such as some low-boiling made of metal powder etc..
Although the foregoing describe specific embodiment of the present utility model, it will be appreciated by those of skill in the art that
These are merely examples, and the protection scope of the utility model is defined by the appended claims.Those skilled in the art
Member can make numerous variations or be repaired to these embodiments under the premise of without departing substantially from the principles of the present invention and essence
Change, but these change and modification each fall within the protection scope of the utility model.
Claims (11)
1. a kind of for producing the quencher of insoluble sulfur, which is characterized in that the quencher includes quencher pedestal, quenching
Device gland and quencher export enlarged tube, and the quencher gland is fixedly connected on the quencher pedestal；
It is provided with multiple cone faces on the quencher gland, forms quenching liquid cavity, in the side wall surface of the quencher gland
It is provided with a quenching liquid and introduces pipe, the quenching liquid introduces pipe and is connected to the quenching liquid cavity, so that fluid passes through the cone
The gap of dignity forms high pressure ring-type cone liquid level；
A quenching material feed pipe is additionally provided on the quencher gland, the centre of the quencher pedestal is provided with one
Expansion chamber, the quenching liquid cavity and the quenching material feed pipe are connected to the expansion chamber；
The quencher outlet enlarged tube is mounted on the bottom end of the quencher pedestal, is connected to the expansion chamber.
2. as described in claim 1 for producing the quencher of insoluble sulfur, which is characterized in that on the quencher gland
There are two cone faces for setting.
3. as described in claim 1 for producing the quencher of insoluble sulfur, which is characterized in that the quencher gland and
Sealing surface gasket is provided between the quencher pedestal.
4. as claimed in claim 3 for producing the quencher of insoluble sulfur, which is characterized in that the quencher pedestal with
Gap between the cone face of the quencher gland, the thickness by adjusting the sealing surface gasket are adjusted.
5. as claimed in claim 4 for producing the quencher of insoluble sulfur, which is characterized in that the sealing surface gasket
With a thickness of 0.5-5mm, the pressure in the expansion chamber is 0.5-1.3MPa.
6. as described in claim 1 for producing the quencher of insoluble sulfur, which is characterized in that the expansion chamber is with one
Angle is injected in quenching apparatus from quencher outlet enlarged tube, the angle ranging from 5-30 °.
7. as described in claim 1 for producing the quencher of insoluble sulfur, which is characterized in that the quencher pedestal with
It is connected between the quencher gland by bolt and nut.
8. as described in claim 1 for producing the quencher of insoluble sulfur, which is characterized in that the expansion chamber by up to
It is down in gradual shrinkage.
9. as claimed in claim 8 for producing the quencher of insoluble sulfur, which is characterized in that the lower end of the expansion chamber
Equipment connecting flange is provided at closing in, for connecting with quenching apparatus, and the lower end of the expansion chamber is closed up and the quenching
Device exports enlarged tube connection.
10. as described in claim 1 for producing the quencher of insoluble sulfur, which is characterized in that the quenching liquid introduces
The end of pipe is provided with charging flange.
11. the quencher for being used to produce insoluble sulfur as described in claim 1-10 any one, which is characterized in that described
The angle in cone face is 45-75 °.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821029565.2U CN208378421U (en) | 2018-06-29 | 2018-06-29 | For producing the quencher of insoluble sulfur |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821029565.2U CN208378421U (en) | 2018-06-29 | 2018-06-29 | For producing the quencher of insoluble sulfur |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208378421U true CN208378421U (en) | 2019-01-15 |
Family
ID=64966082
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821029565.2U Active CN208378421U (en) | 2018-06-29 | 2018-06-29 | For producing the quencher of insoluble sulfur |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208378421U (en) |
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2018
- 2018-06-29 CN CN201821029565.2U patent/CN208378421U/en active Active
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