CN208373091U - A kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device - Google Patents
A kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device Download PDFInfo
- Publication number
- CN208373091U CN208373091U CN201820785130.4U CN201820785130U CN208373091U CN 208373091 U CN208373091 U CN 208373091U CN 201820785130 U CN201820785130 U CN 201820785130U CN 208373091 U CN208373091 U CN 208373091U
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- CN
- China
- Prior art keywords
- decarboxylation
- carboxylic acid
- tank body
- controller
- preparation process
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
The utility model discloses a kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation devices, including decarboxylation tank body, flow control pipe, motor, controller and PH detection meter, the decarboxylation can outer surface adheres to matcoveredn, the decarboxylation tank interior is provided with shaft, the shaft is connected to the retarder above the decarboxylation tank body, the motor for driving the shaft rotation is provided with above the retarder, the decarboxylation tank interior is additionally provided with the flow control pipe, the flow control pipe links together with the flow container above the decarboxylation tank body, flow valve is provided on the flow control pipe, steam spray line is provided on the outside of the shaft, the steam spray line is connected to steam pipeline.Beneficial effect is: the reacting dose of two sides solvent can be accurately controlled the control for the flow valve that the feedback and controller of pH value are controlled by PH detection meter, not will cause waste, and surplus solution does not have excessive residual volume, it is more intelligent.
Description
Technical field
The utility model relates to field of chemical equipment, and it is de- to be specifically related to a kind of 1-aminocyclobutane carboxylic acid preparation process use
Carboxylic device.
Background technique
Disease incidence of the prostate cancer in China male is lower, and stepping in America and Europe is one of most common cancer, Bu Guosui
Environmental pollution eating habit change, job and life stress, which increases, etc. influences, China's prostate-cancer incidence also constantly soaring,
There are many treatment means of prostate cancer, including operation, hormone, chemotherapy, radiotherapy and Chinese medicine treatment etc., and RAN-509 is a kind of new
Type drugs for prostate cancer is increasingly favored by many patients, and therapeutic effect is significant, 1-aminocyclobutane carboxylic acid conduct
Its key intermediates has very big economic value, and traditional 1-aminocyclobutane carboxylic acid synthesis production needs manpower constantly
Detection solution and manually addition control are removed, it is not only time-consuming and laborious, and error is relatively large, measures each link data and needs constantly
Statistics calculates the solution liquid measure for needing to be added, not smart enoughization.
Utility model content
The purpose of this utility model is that solve the above-mentioned problems and provides a kind of 1-aminocyclobutane carboxylic acid preparation
Process decarboxylation device.
The utility model achieves the above object through the following technical schemes:
A kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device, including decarboxylation tank body, flow control pipe, motor, control
Device and PH detection meter, the decarboxylation can outer surface adhere to matcoveredn, and the decarboxylation tank interior is provided with shaft, and described turn
Retarder above axis connection to the decarboxylation tank body, the retarder top are provided with the electricity for driving the shaft rotation
Machine, the decarboxylation tank interior are additionally provided with the flow control pipe, and the flow control pipe is connect with the flow container above the decarboxylation tank body
Together, it is provided with flow valve on the flow control pipe, steam spray line is provided on the outside of the shaft, the steam spray line connects
It is connected to steam pipeline, the protective layer outer surface is additionally provided with the controller.
In above structure, when the sodium salt solution and sodium hydroxide solution for being contained with carboxylic acid in two flow containers respectively, two
Person is trickled down under the control of the flow valve, and the solution ph after reflection completely is fixed in proportion, the PH detection
The real-time pH value of solution is passed to the controller by meter, and numerical value is bigger than normal or less than normal pass through the controller and controls self-action stream
The control valve is measured to adjust the rate of outflow of liquid pot liquid described in two sides, so that the solution of the decarboxylation tank interior
Reaction completely, the solution after reaction does not have the sodium salt solution and sodium hydroxide solution of excessive carboxylic acid, in order to avoid cause to waste.
In order to further increase the use function of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device, the steam is defeated
Pipe is sent to connect with the steam generator being arranged on the outside of the decarboxylation tank body.
In order to further increase the use function of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device, the flow valve
Using DKTS model flux-adjustable solenoid valve and it is wired on the controller.
In order to further increase the use function of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device, the controller
Using HAD-SC200SC200 model and pass through motor described in polygon control survey.
In order to further increase the use function of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device, the PH detection
Meter is wired to the input terminal of the controller, and heat-insulated cavernous body is provided in the protective layer, and the flow container is logical
Bolt is crossed to be fixed on the decarboxylation tank body.
Beneficial effect is: the control of the flow valve controlled to the feedback and controller of pH value by PH detection meter can be with
The reacting dose for accurately controlling two sides solvent, not will cause waste, and surplus solution does not have excessive residual volume, more intelligently
Change.
Detailed description of the invention
Fig. 1 is a kind of main view of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device of the utility model.
The reference numerals are as follows:
1, decarboxylation tank body；2, protective layer；3, flow control pipe；4, air pressure valve；5, flow valve；6, flow container；7, retarder；8, electric
Machine；9, steam pipeline；10, steam spray line；11, shaft；12, controller；13, stirring body；14, PH detection meter.
Specific embodiment
The utility model is described in further detail with reference to the accompanying drawing:
As shown in Figure 1, a kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device, including decarboxylation tank body 1, flow control pipe
3, motor, controller 12 and PH detection meter 14, matcoveredn 2 is adhered in 1 outer surface of decarboxylation tank body, and decarboxylation tank body 1 is internally provided with
Shaft 11, shaft 11 are connected to the retarder 7 of 1 top of decarboxylation tank body, are provided with above retarder 7 and rotate for drive shaft 11
Motor 8, flow control pipe 3 is additionally provided with inside decarboxylation tank body 1, the flow container 6 of 1 top of flow control pipe 3 and decarboxylation tank body links together,
It is provided with flow valve 5 on flow control pipe 3, steam spray line 10 is provided on the outside of shaft 11, it is defeated that steam spray line 10 is connected to steam
Pipe 9 is sent, 2 outer surface of protective layer is additionally provided with controller 12.
In above structure, when the sodium salt solution and sodium hydroxide solution for being contained with carboxylic acid in two flow containers 6 respectively, the two exists
It trickles down under the control of flow valve 5, the solution ph after reflection completely is fixed in proportion, and PH detection counts 14 for solution
Real-time pH value passes to controller 12, and numerical value is bigger than normal or less than normal controls self-action flow control valve 5 by controller 12 to adjust
The rate of outflow of liquid in two sides flow container 6 is saved, so that the solution inside decarboxylation tank body 1 reacts completely, the solution after reaction
The sodium salt solution and sodium hydroxide solution of excessive carboxylic acid are not had, in order to avoid cause to waste.
In order to further increase the use function of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device, steam pipeline
9 connect with the steam generator that 1 outside of decarboxylation tank body is arranged in, and flow valve 5 is using DKTS model flux-adjustable solenoid valve and leads to
It crosses conducting wire to be connected on controller 12, controller 12 is using HAD-SC200SC200 model and passes through polygon control survey motor 8, PH inspection
The input terminal that meter 14 is wired to controller 12 is surveyed, is provided with heat-insulated cavernous body in protective layer 2, flow container 6 passes through spiral shell
Bolt is fixed on decarboxylation tank body 1.
The basic principles and main features and advantage of the utility model have been shown and described above.The technical staff of the industry
It should be appreciated that the present utility model is not limited to the above embodiments, the above embodiments and description only describe this
The principle of utility model, on the premise of not departing from the spirit and scope of the utility model, the utility model also has various change
And improvement, these various changes and improvements fall within the scope of the claimed invention.The utility model requires protection scope
It is defined by appending claims and equivalents.
Claims (5)
1. a kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device, including decarboxylation tank body, flow control pipe, motor, controller
It detects and counts with PH, it is characterised in that: the decarboxylation can outer surface adheres to matcoveredn, and the decarboxylation tank interior, which is provided with, to be turned
Axis, the shaft are connected to the retarder above the decarboxylation tank body, are provided with above the retarder for driving described turn
The motor of axis rotation, the decarboxylation tank interior are additionally provided with the flow control pipe, the flow control pipe and decarboxylation tank body top
Flow container link together, be provided with flow valve on the flow control pipe, be provided with steam spray line, the steaming on the outside of the shaft
Vapour spray line is connected to steam pipeline, and the protective layer outer surface is additionally provided with the controller.
2. a kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device according to claim 1, it is characterised in that: institute
It states steam pipeline and is connect with the steam generator being arranged on the outside of the decarboxylation tank body.
3. a kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device according to claim 1, it is characterised in that: institute
Flow valve is stated using DKTS model flux-adjustable solenoid valve and is wired on the controller.
4. a kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device according to claim 1, it is characterised in that: institute
Controller is stated using HAD-SC200SC200 model and by motor described in polygon control survey.
5. a kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device according to claim 1, it is characterised in that: institute
The input terminal that PH detection meter is wired to the controller is stated, is provided with heat-insulated cavernous body, institute in the protective layer
Flow container is stated to be bolted on the decarboxylation tank body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820785130.4U CN208373091U (en) | 2018-05-25 | 2018-05-25 | A kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820785130.4U CN208373091U (en) | 2018-05-25 | 2018-05-25 | A kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208373091U true CN208373091U (en) | 2019-01-15 |
Family
ID=64972146
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820785130.4U Expired - Fee Related CN208373091U (en) | 2018-05-25 | 2018-05-25 | A kind of 1-aminocyclobutane carboxylic acid preparation process decarboxylation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208373091U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111001357A (en) * | 2019-11-29 | 2020-04-14 | 浙江荣凯科技发展有限公司 | Catalyst dripping system for alkaline phenolic resin synthesis |
-
2018
- 2018-05-25 CN CN201820785130.4U patent/CN208373091U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111001357A (en) * | 2019-11-29 | 2020-04-14 | 浙江荣凯科技发展有限公司 | Catalyst dripping system for alkaline phenolic resin synthesis |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190115 Termination date: 20200525 |