CN208350627U - A kind of pumping equipment for atomic absorption spectrophotometer - Google Patents

A kind of pumping equipment for atomic absorption spectrophotometer Download PDF

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Publication number
CN208350627U
CN208350627U CN201820932159.0U CN201820932159U CN208350627U CN 208350627 U CN208350627 U CN 208350627U CN 201820932159 U CN201820932159 U CN 201820932159U CN 208350627 U CN208350627 U CN 208350627U
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CN
China
Prior art keywords
pipe
bend pipe
waste
outlet
spray chamber
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Expired - Fee Related
Application number
CN201820932159.0U
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Chinese (zh)
Inventor
林永强
杜桂銮
林启武
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Xiamen Weizheng Testing Technology Co Ltd
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Xiamen Weizheng Testing Technology Co Ltd
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Priority to CN201820932159.0U priority Critical patent/CN208350627U/en
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Abstract

The utility model discloses a kind of pumping equipments for atomic absorption spectrophotometer, to solution must not timely and effective discharge waste liquid the problems such as, it includes spray chamber, the burner on spray chamber and the acetylene sample feeding pipe and air intlet pipe connecting with spray chamber, spray chamber left end is equipped with atomizer, and spray chamber has waste liquid outlet pipe;The bottom of waste liquid outlet pipe is integrally in " W word " type, is equipped with first level pipe in the junction of first bend pipe and tail bend pipe, the height of horizontal tube is less than the height of first bend pipe liquid inlet and tail bend pipe outlet end;The outlet end of tail bend pipe is connected with the second horizontal tube, and the second horizontal tube is connected with container;The bottom of first bend pipe and tail bend pipe is respectively connected with waste pipe, and waste pipe is equipped with valve, and looped pipeline is equipped on first bend pipe, and looped pipeline rear end connects syringe by the sub-joint stretched out, and front end of the syringe needle is equipped with unidirectional liquid feed valve;The upper end of first level pipe is equipped with outlet tube, and outlet tube is equipped with check valve, and outlet tube is connected to aspirator.

Description

A kind of pumping equipment for atomic absorption spectrophotometer
Technical field
The utility model belongs to detection device technical field, specially a kind of drain for atomic absorption spectrophotometer Device.
Background technique
Atomic Absorption Spectrometer is also known as atomic absorption spectrophotometer, is inhaled according to substance ground state atom steam to characteristic radiation The effect of receipts carries out metallic element analysis, it sensitive can reliably measure micro or trace element.Carrying out sample analysis When, it is commonly present ponding blockage problem, influences whether flame instability, absorbance non-return-to-zero, and in such a way that water has been put, but Palliative, survey several samples has ponding again, and tracing it to its cause, some are stifled for predominantly sewer pipe;And making organic solvent sample When analysis, the organic solvent of discharge will swim in the upper surface of water in water seal since specific gravity is less than water, be not easy discharge and long-time Easily corrode pipe.
A kind of waste liquid discharge device of atomic absorption spectrophotometer is disclosed in notification number CN206311506U, is set A U-shaped water seal is set, the left end of U-shaped water seal is connected to waste liquid outlet pipe by sealing-liquid duct pipe, and the right end of U-shaped water seal passes through water Envelope outlet is connected to waste liquid outlet hose, and the inclination of waste liquid outlet hose is connected to container, when with atomic absorption spectrophotometer In the analytic process for making organic solvent sample, the organic solvent being discharged will swim in water in water seal since specific gravity is less than water The upper surface of, when waste liquid is more than water seal height, the organic liquid waste above water seal will flow to waste liquid outlet by water seal outlet Hose, and then flow into container, after analysis detection is finished, the service valve of water seal lower end is opened, can will be given up by overhauling pipe Liquid complete liquidation is clean.
However its discharge organic solvent be the left end fallen in U-shaped water seal, be swim in U-shaped water seal left end water it is upper Face, and water seal outlet is the right end for being connected to U-shaped water seal;Certainly, a small amount of organic solvent is had in the effect of drippage gravity Lower transfer swims in the waterborne of U-shaped water seal right end, and when waste liquid is more than water seal height, the organic liquid waste of U-shaped water seal right end can lead to Cross water seal outlet and flow to waste liquid outlet hose, but the organic liquid waste of the U-shaped water seal left end of volume still remains in pipe, can not and When be discharged, can not completely effectively solve the problems, such as.
Meanwhile when doing other materials analysis using the device, when the waste liquid specific gravity of discharge is greater than water, waste liquid can be accumulated In the bottom of U-shaped water seal, extra water can flow to waste liquid outlet hose from water seal outlet;At this point, if being discharged when thinking of useless Liquid then needs to open service valve, and after opening the outflow of service valve solution, the water in U-shaped water seal can be reduced, it will affect water seal effect, There are security risks;If being discharged not in time, and can there are the problems such as blocking, a kind of original disclosed in notification number CN206311506U The waste liquid discharge device applicability and practicability of sub- absorption spectrophotometer be not strong.
Utility model content
The purpose of this utility model is to provide a kind of pumping equipments for atomic absorption spectrophotometer, on solving State the problem of proposing in background technique.
To achieve the above object, the utility model provides the following technical solutions: one kind being used for atomic absorption spectrophotometer Pumping equipment comprising spray chamber, the burner on spray chamber and the acetylene sample feeding pipe and sky being connect with spray chamber Gas inlet pipe, spray chamber left end are equipped with atomizer, and atomizer lower left side is equipped with air intake duct, and atomizer one end is put into spray chamber Interior, the other end is connected with sample introduction capillary, and sample introduction capillary is inserted in sample container, and spray chamber has waste liquid outlet pipe;It is useless The bottom of liquid outlet is integrally in " W word " type, is equipped with first level pipe, the height of horizontal tube in the junction of first bend pipe and tail bend pipe Degree is less than the height of first bend pipe liquid inlet and tail bend pipe outlet end;The outlet end of tail bend pipe is connected with the second horizontal tube, the second water Flat pipe is connected with a container;The bottom of first bend pipe and tail bend pipe is respectively connected with a waste pipe, and waste pipe is equipped with a valve, first A looped pipeline is equipped on bend pipe, looped pipeline rear end connects syringe by the sub-joint stretched out, and front end of the syringe needle is equipped with unidirectional feed liquor Valve;The upper end of first level pipe is equipped with outlet tube, and outlet tube is equipped with a check valve, and outlet tube is connected to an aspirator.
Further, filter,primary and the second filter disc are equipped with positioned at the top of valve in waste pipe;Waste pipe medial end In shape of threads, an annular groove is arranged in lateral edge inner wall in shape of threads;Filter,primary and waste pipe end thread cooperate, end face annular It is uniformly arranged several first through hole;Second filter disc and annular groove nested type cooperate, and are bonded with filter,primary, if end face is arranged Several second through-holes corresponding with first through hole position are done, are arranged in the annular region where several second through-holes several recessed The top pillar that slot one compressed spring of interior setting at groove and is connected with the compression spring;Compressed spring one end is fixedly connected on the bottom of groove End, one end are connected in the middle part of top pillar end face.
Further, the minimum value of top pillar and compressed spring length is equal to the depth of groove.
Further, the inlet tube of first bend pipe is inclined, and well azimuth be towards first level pipe it is opposite one Side.
Further, the inlet tube of first bend pipe is inclined, and well azimuth be towards first level pipe it is opposite one Side.
Further, in rotational direction side is wedge shape to top pillar.
Compared with prior art, the utility model has the beneficial effects that this is used for the drain of atomic absorption spectrophotometer When device does the analysis of solvent sample, organic liquid waste is dropped in first bend pipe, and part organic liquid waste turns under gravity Shifting is swum in first level pipe, then is had only small amounts of organic liquid waste to continue transfer and be floated to the outlet end of tail bend pipe and along the Two horizontal tubes enter in container;At this point, being filled the water by syringe into first bend pipe, the liquid in first bend pipe is disturbed, makes to be located at Organic liquid waste in first bend pipe drives the outlet end for effectively further entering to first level pipe or tail bend pipe, and bottom through water flow Portion is integrally in the design of " W word " type, forms double sealing structure for water, water filling is avoided to influence water seal effect when disturbing;Positioned at first level pipe Interior organic liquid waste pumps out under the mating reaction of aspirator and check valve;The design of double sealing structure for water and the water filling of syringe Design is also avoided when aspirating and flowing out extra water, is managed interior water and is reduced, influences water seal effect, whole design ensures The timely and effective exclusion of organic liquid waste.
When making the analysis of inorganic samples of the atomic absorption spectrophotometer, waste liquid is dropped in first bend pipe and is deposited in The bottom end of first bend pipe drives the waste liquid entered in tail bend pipe to be deposited in the bottom end of tail bend pipe, manages interior isometric through water flow on a small quantity Water then entered in container from the outlet end of tail bend pipe along the second horizontal tube;It is located at first bend pipe and tail bend pipe at this point, opening Valve on the waste pipe of bottom flows out waste liquid from waste pipe, can be by syringe to first bend pipe during waste liquid discharge Interior water filling avoids water in waste liquid outlet bottom of the tube from reducing, influences water seal effect, there are problems that security risk.
Detailed description of the invention
Fig. 1 is the utility model overall structure diagram;
Fig. 2 is the structural schematic diagram of Anti-blocking structure in the utility model waste pipe;
Fig. 3 is the structural schematic diagram of the second filter disc of the utility model;
In figure: 1, spray chamber;2, burner;3, acetylene sample feeding pipe;4, air intlet pipe;5, atomizer;6, air inlet Pipe;7, sample introduction capillary;8, sample container;9, waste liquid outlet pipe;10, first bend pipe;11, tail bend pipe;12, first level pipe;13, Liquid inlet;14, outlet end;15, the second horizontal tube;16, container;17, waste pipe;18, valve;19, looped pipeline;20, sub-joint; 21, syringe;22, inlet tube;23, unidirectional liquid feed valve;24, outlet tube;25, check valve;26, aspirator;27, filter,primary; 28, the second filter disc;29, annular groove;30, first through hole;31, the second through-hole;32, groove;33, compressed spring;34, top pillar.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
As shown in Fig. 1 ~ Fig. 3, which includes spray chamber 1, is located at atomization Burner 2 on room 1 and the acetylene sample feeding pipe 3 and air intlet pipe 4 connecting with spray chamber 1,1 left end of spray chamber are equipped with atomization Device 5,5 lower left side of atomizer are equipped with air intake duct 6, and 5 one end of atomizer is put into spray chamber 1, and the other end is connected with sample introduction hair Tubule 7, sample introduction capillary 7 are inserted in sample container 8, and spray chamber 1 has waste liquid outlet pipe 9;Through sample introduction hair in sample container 8 Tubule 7 is brought into spray chamber 1, so that the analysis to sample is carried out, the conventional equipment and tool of atomic absorption spectrophotometer Body running principle has been conventional prior, is disclosed in lot of documents, be for technology known to technical field technical staff, Therefore to save space, don't explain too much here.
The bottom for being used for the waste liquid outlet pipe 9 of atomic absorption spectrophotometer is integrally in " W word " type, in first 10 He of bend pipe The junction of tail bend pipe 11 is equipped with first level pipe 12, and the height of horizontal tube is less than first 10 liquid inlet 13 of bend pipe and goes out with tail bend pipe 11 The height at liquid end 14;The outlet end 14 of tail bend pipe 11 is connected with the second horizontal tube 15, and the second horizontal tube 15 is connected with a container 16; The bottom of first bend pipe 10 and tail bend pipe 11 is respectively connected with a waste pipe 17, and waste pipe 17 is equipped with a valve 18, on first bend pipe 10 It is equipped with a looped pipeline 19,19 rear end of looped pipeline connects syringe 21 by the sub-joint 20 stretched out, and connection can refer to injector for medical purpose 21 connection type;21 front end of syringe is equipped with unidirectional liquid feed valve 23, and unidirectional liquid feed valve 23 limits gas-liquid can only be from syringe 21 End enters in looped pipeline 19;The upper end of first level pipe 12 is equipped with outlet tube 24, and outlet tube 24 is equipped with a check valve 25, check valve 25 limitation gas-liquids can only enter in outlet tube 24 from 12 end of first level pipe, and outlet tube 24 is connected to an aspirator 26, for aspirating Liquid in outlet tube 24.
The bottom of waste liquid outlet pipe 9 is integrally in " W word " type, and two sealing structure for water are integrally formed, and makes water seal effect more preferably more Safety;When making the analysis of solvent sample of the atomic absorption spectrophotometer, organic liquid waste is dropped in first bend pipe 10, portion Divide organic liquid waste to shift under gravity to swim in first level pipe 12, then there is only small amounts of organic liquid waste to continue to shift It is floated to the outlet end 14 of tail bend pipe 11 and is entered in container 16 along the second horizontal tube 15;At this point, by syringe 21 to Water filling in first bend pipe 10 disturbs the liquid in first bend pipe 10, drives the organic liquid waste being located in first bend pipe 10 into one through water flow Step effectively enters the outlet end 14 to first level pipe 12 or tail bend pipe 11, and bottom is integrally in the design of " W word " type, is formed double Sealing structure for water avoids water filling from influencing water seal effect when disturbing;Organic liquid waste in first level pipe 12 is in 26 He of aspirator It is pumped out under the mating reaction of check valve 25;The design of double sealing structure for water and the water filling design of syringe 21 also avoid aspirating And when flowing out extra water, manages interior water and reduce, influence water seal effect, whole design ensures the timely and effective of organic liquid waste It excludes.
When making the analysis of inorganic samples of the atomic absorption spectrophotometer, waste liquid is dropped in first bend pipe 10 and is accumulated In the bottom end of first bend pipe 10, drives the waste liquid entered in tail bend pipe 11 to be deposited in the bottom end of tail bend pipe 11 through water flow on a small quantity, manage Interior isometric water then enters in container 16 from the outlet end 14 of tail bend pipe 11 along the second horizontal tube 15;At this point, open position Valve 18 on 11 bottom waste pipe 17 of first bend pipe 10 and tail bend pipe flows out waste liquid from waste pipe 17, in waste liquid discharge In the process, it can be filled the water by syringe 21 into first bend pipe 10, water in 9 bottom of waste liquid outlet pipe is avoided to reduce, influence water seal effect There is security risk in fruit.
This is for being equipped with 27 He of filter,primary positioned at the top of valve 18 in the waste pipe 17 of atomic absorption spectrophotometer Second filter disc 28;17 medial end of waste pipe is in shape of threads, and an annular groove 29 is arranged in lateral edge inner wall in shape of threads;Filter,primary 27 cooperate with 17 end thread of waste pipe, and end face annular is uniformly arranged several first through hole 30;Second filter disc 28 and annular groove The cooperation of 29 nested types, and be bonded with filter,primary 27, end face setting several corresponding with 30 position of first through hole several second Through-hole 31 is arranged several grooves 32 in the annular region where several second through-holes 31, a compressed spring 33 is arranged in groove 32 And the top pillar 34 being connect with compressed spring 33;33 one end of compressed spring is fixedly connected on the bottom end of groove 32, and one end is connected to top In the middle part of 34 end face of column, the minimum value of top pillar 34 and 33 length of compressed spring is equal to the depth of groove 32.In drain, filter,primary 27 and second the first through hole 30 on filter disc 28 and the alignment of the second through-hole 31 second is filtered when first through hole 30 blocks Piece 28 is rotated along annular groove 29, and the second filter disc 28 can be connect with micro-driving motor, driving the second filter disc 28 rotation;When When groove 32 is aligned with first through hole 30, compressed spring 33 can make top pillar 34 pop up and enter in first through hole 30, and first is led to Tamper ejection in hole 30 is non-stop run when due to the rotation of the second filter disc 28, so can insert in same first through hole 30 Enter multiple top pillar 34, make tamper discharge thoroughly, in rotational direction side is wedge shape to top pillar 34, facilitates the second filter disc 28 Rotation;The setting of its overall structure rationally, avoids the phenomenon that blocking in waste pipe 17 when drain.
The preferred embodiment of the utility model are as follows: the inlet tube 22 of first bend pipe 10 is inclined, and well azimuth is court The side opposite to first level pipe 12, convenient for when carrying out the analysis of solvent sample, organic liquid waste can more enter To first level pipe 12.
The preferred embodiment of the utility model are as follows: the inlet tube 22 of first bend pipe 10 is inclined, and well azimuth is court The side opposite to first level pipe 12, convenient for when carrying out the analysis of solvent sample, staying in the organic of first 10 left side of bend pipe Waste liquid can adequately enter in first level pipe 12 under the drive of water filling water flow.
When in specific implementation, at work, as the analysis of solvent sample, organic liquid waste drops to first bend pipe 10 Interior, part organic liquid waste shifts swim in first level pipe 12 under gravity, then have only small amounts of organic liquid waste after It is continuous to shift the outlet end 14 for being floated to tail bend pipe 11 and entered in container 16 along the second horizontal tube 15;At this point, passing through injection Device 21 is filled the water into first bend pipe 10, disturbs the liquid in first bend pipe 10, makes the organic liquid waste being located in first bend pipe 10 through water flow band The dynamic outlet end 14 for effectively further entering to first level pipe 12 or tail bend pipe 11, and bottom is integrally in the design of " W word " type, Double sealing structure for water are formed, water filling is avoided to influence water seal effect when disturbing;Organic liquid waste in first level pipe 12 is aspirating It is pumped out under the mating reaction of device 26 and check valve 25;The design of double sealing structure for water and the water filling design of syringe 21 also avoid When aspirating and flowing out extra water, manage in water reduce, influence water seal effect, whole design ensure organic liquid waste and Shi Youxiao is excluded.
As inorganic samples analysis when, waste liquid drops in first bend pipe 10 and is deposited in the bottom end of first bend pipe 10, on a small quantity The waste liquid entered in tail bend pipe 11 is driven to be deposited in the bottom end of tail bend pipe 11 through water flow, the interior isometric water of pipe is then from tail bend pipe 11 outlet end 14 enters in container 16 along the second horizontal tube 15;It is located at first bend pipe 10 and 11 bottom of tail bend pipe at this point, opening Valve 18 on portion's waste pipe 17, make waste liquid from waste pipe 17 flow out, waste liquid discharge during, can by syringe 21 to Water filling in first bend pipe 10 avoids water in 9 bottom of waste liquid outlet pipe from reducing, influences water seal effect, there are problems that security risk.
Although the utility model is described in detail with reference to the foregoing embodiments, come for those skilled in the art Say, it is still possible to modify the technical solutions described in the foregoing embodiments, or to part of technical characteristic into Row equivalent replacement, within the spirit and principle of the utility model, any modification, equivalent replacement, improvement and so on should all It is included within the scope of protection of this utility model.

Claims (6)

1. a kind of pumping equipment for atomic absorption spectrophotometer, including spray chamber (1), the combustion being located on spray chamber (1) Burner (2) and the acetylene sample feeding pipe (3) and air intlet pipe (4) connecting with spray chamber (1), spray chamber (1) left end are set Have atomizer (5), atomizer (5) lower left side is equipped with air intake duct (6), and described atomizer (5) one end is put into spray chamber (1) in, the other end is connected with sample introduction capillary (7), and the sample introduction capillary (7) is inserted in sample container (8), the spray chamber (1) waste liquid outlet pipe (9) are had;It is characterized by: the bottom of the waste liquid outlet pipe (9) is integrally in " W word " type, first curved The junction for managing (10) and tail bend pipe (11) is equipped with first level pipe (12), and the height of the horizontal tube (12) is less than first bend pipe (10) height of liquid inlet (13) and tail bend pipe (11) outlet end (14);The outlet end (14) of the tail bend pipe (11) is connected with Two horizontal tubes (15), second horizontal tube (15) are connected with a container (16);The head bend pipe (10) and tail bend pipe (11) Bottom is respectively connected with a waste pipe (17), and the waste pipe (17) is equipped with a valve (18), is all provided on the head bend pipe (10) Have a looped pipeline (19), looped pipeline (19) rear end connects syringe (21) by the sub-joint (20) stretched out, before syringe (21) End is equipped with unidirectional liquid feed valve (23);The upper end of the first level pipe (12) is equipped with outlet tube (24), on the outlet tube (24) Equipped with a check valve (25), the outlet tube (24) is connected to an aspirator (26).
2. a kind of pumping equipment for atomic absorption spectrophotometer according to claim 1, it is characterised in that: described Top in waste pipe (17) positioned at the valve (18) is equipped with filter,primary (27) and the second filter disc (28);The waste pipe (17) medial end is in shape of threads, lateral edge inner wall setting one annular groove (29) in shape of threads;The filter,primary (27) and row Useless pipe (17) end thread cooperation, end face annular are uniformly arranged several first through hole (30);Second filter disc (28) and annular The cooperation of sliding slot (29) nested type, and be bonded with filter,primary (27), end face setting is several corresponding with first through hole (30) position Several second through-holes (31), several grooves (32), the groove are set in the annular region where several second through-holes (31) (32) setting one compressed spring (33) and the top pillar (34) being connect with compressed spring (33) in;Described compressed spring (33) one end is solid Surely it is connected to the bottom end of groove (32), one end is connected in the middle part of top pillar (34) end face.
3. a kind of pumping equipment for atomic absorption spectrophotometer according to claim 2, it is characterised in that: described The minimum value of top pillar (34) and the compressed spring (33) length is equal to the depth of the groove (32).
4. a kind of pumping equipment for atomic absorption spectrophotometer according to claim 1, it is characterised in that: described The inlet tube (22) of first bend pipe (10) is inclined, and well azimuth is the side opposite towards first level pipe (12).
5. a kind of pumping equipment for atomic absorption spectrophotometer according to claim 1, it is characterised in that: described Looped pipeline (19) is connected to inlet tube (22) inclination of first bend pipe (10), and inclined direction is upward, the looped pipeline (19) and inlet tube (22) angle between is 5 ~ 15 degree.
6. a kind of pumping equipment for atomic absorption spectrophotometer according to claim 3, it is characterised in that: described In rotational direction side is wedge shape to top pillar (34).
CN201820932159.0U 2018-06-15 2018-06-15 A kind of pumping equipment for atomic absorption spectrophotometer Expired - Fee Related CN208350627U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820932159.0U CN208350627U (en) 2018-06-15 2018-06-15 A kind of pumping equipment for atomic absorption spectrophotometer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820932159.0U CN208350627U (en) 2018-06-15 2018-06-15 A kind of pumping equipment for atomic absorption spectrophotometer

Publications (1)

Publication Number Publication Date
CN208350627U true CN208350627U (en) 2019-01-08

Family

ID=64884044

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820932159.0U Expired - Fee Related CN208350627U (en) 2018-06-15 2018-06-15 A kind of pumping equipment for atomic absorption spectrophotometer

Country Status (1)

Country Link
CN (1) CN208350627U (en)

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Granted publication date: 20190108