CN208340706U - A kind of ternary coprecipitation reaction kettle - Google Patents
A kind of ternary coprecipitation reaction kettle Download PDFInfo
- Publication number
- CN208340706U CN208340706U CN201820343816.8U CN201820343816U CN208340706U CN 208340706 U CN208340706 U CN 208340706U CN 201820343816 U CN201820343816 U CN 201820343816U CN 208340706 U CN208340706 U CN 208340706U
- Authority
- CN
- China
- Prior art keywords
- cutting ferrule
- autoclave body
- ball valve
- air inlet
- inlet pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 26
- 238000000975 co-precipitation Methods 0.000 title claims abstract description 18
- 238000005520 cutting process Methods 0.000 claims abstract description 73
- 238000007789 sealing Methods 0.000 claims abstract description 10
- 239000000463 material Substances 0.000 claims description 12
- 229910001220 stainless steel Inorganic materials 0.000 claims description 4
- 239000010935 stainless steel Substances 0.000 claims description 4
- 230000000694 effects Effects 0.000 abstract description 5
- 239000007788 liquid Substances 0.000 abstract description 5
- 238000004891 communication Methods 0.000 abstract description 2
- 238000010586 diagram Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 239000000908 ammonium hydroxide Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a kind of ternary coprecipitation reaction kettles, including autoclave body, the top of autoclave body is fixed with kettle cover, the middle part on autoclave body top is equipped with feed inlet, and the middle part of autoclave body bottom end is equipped with discharge port, and one end at the top of autoclave body is fixedly installed with the first cutting ferrule, the interspersed connection air inlet pipe in the inside of first cutting ferrule, one end of air inlet pipe passes through the bottom that autoclave body is placed in autoclave body, and the top that the first cutting ferrule is placed at the top of air inlet pipe is fixedly installed with the first ball valve, and the top of the first ball valve is equipped with air inlet.The utility model passes through the first cutting ferrule being equipped with and the second cutting ferrule each serves as connection and fixes the effect of air inlet pipe and overflow discharge nozzle, play the role of sealing the junction of fixed air inlet pipe and kettle cover by the sealing ring being equipped with, prevent gas and liquid from overflowing, gas and liquid communication are controlled convenient for staff by the first ball valve being equipped with and the second ball valve, fixed air inlet pipe and overflow discharge nozzle are played the role of by the locking nut being equipped with.
Description
Technical field
The utility model relates to a kind of reaction kettle, specially a kind of ternary coprecipitation reaction kettle.
Background technique
At present known to us, the broad understanding of reaction kettle has the container physically or chemically reacted, passes through the knot to container
Structure design and parameter configuration, realize the mixed function for heating, evaporation, cooling and the low high speed that technique requires, and reaction kettle is continuously given birth to
It produces and overflow port progress nature overflow is opened using side, protection gas enters from bottom, and then the overflow of kettle cover top-side is gone out.
However existing reaction kettle reaction kettle continuous production uses side to have overflow port progress nature overflow, in this way a meeting at present
Appearance material is unmixed to go out with regard to overflow completely, and has ammonium hydroxide in material, volatile, so protection air-flow can take away one when going out
Partial material forms waste, while the material at top can only be discharged from side for existing reaction kettle, so that low efficiency
Under, so being unsatisfactory for the demand of reaction kettle instantly, therefore we make improvement to this, propose a kind of ternary coprecipitation reaction kettle.
Utility model content
To solve of the existing technology serious to material loss and overflow port, small in size cause can only be the material at top
The defect of discharge, the utility model provide a kind of ternary coprecipitation reaction kettle.
In order to solve the above-mentioned technical problem, the utility model provides the following technical solution:
A kind of ternary coprecipitation reaction kettle of the utility model, including autoclave body, the top of the autoclave body are fixed with kettle cover, institute
The middle part for stating autoclave body top is equipped with feed inlet, and the middle part of the autoclave body bottom end is equipped with discharge port, and one end at the top of the autoclave body is solid
Dingan County is equipped with the first cutting ferrule, and the interspersed connection air inlet pipe in the inside of first cutting ferrule, one end of the air inlet pipe is set across autoclave body
In the bottom of autoclave body, the other end that the air inlet pipe passes through the first cutting ferrule is fixedly installed with the first ball valve, first ball valve
Top is equipped with air inlet, and the other end at the top of the kettle cover is fixedly installed with the second cutting ferrule, and the top of second cutting ferrule is fixed
Right angle cutting ferrule is installed, the inside of the right angle cutting ferrule is interspersed to be connected with overflow discharge nozzle, and one end of the overflow discharge nozzle is worn
The bottom that autoclave body is placed in autoclave body is crossed, the other end that the overflow discharge nozzle passes through right angle cutting ferrule is fixedly installed with the second ball valve, institute
The one end for stating the second ball valve is equipped with overflow port.
Further, the junction and the second cutting ferrule of first cutting ferrule and kettle cover and the junction of kettle cover are arranged with close
Seal, the first cutting ferrule, the second cutting ferrule and right angle cutting ferrule are made of stainless steel material.
Further, the middle part of first card outer wall and the middle part of the second card outer wall are threaded with locking screw
The screw top of mother, the right angle cutting ferrule are connected with cutting ferrule nut.
Further, the side of first ball valve and the side of the second ball valve are fixed with valve rod, the valve rod point
Not Chuan Guo the first ball valve and the second ball valve connect with the sphere in portion disposed within.
Compared with prior art, the utility model has the following beneficial effects: this kind of ternary coprecipitation reaction kettle, by setting
The first cutting ferrule and the second cutting ferrule played the role of each serves as connection and fixed air inlet pipe and overflow discharge nozzle, close by what is be equipped with
Seal plays the role of sealing the junction of fixed air inlet pipe and kettle cover, prevents gas and liquid from overflowing, by be equipped with first
Ball valve and the second ball valve control gas and liquid communication convenient for staff, play fixation by the locking nut being equipped with
The effect of air inlet pipe and overflow discharge nozzle, while after unscrewing locking nut, it is adjusted convenient for the height to overflow discharge nozzle, from
And staff is facilitated to carry out overflow to different height and positions, by being passed through protective gas into air inlet pipe, so that in autoclave body
Portion generates air pressure and so that material is pressed into autoclave body bottom material is overflowed from bottom, while air pressure overflow can be with
Preferably realize control discharging flow.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of ternary coprecipitation reaction kettle of the utility model；
Fig. 2 is a kind of structural schematic diagram of ternary coprecipitation reaction kettle cutting ferrule of the utility model；
Fig. 3 is a kind of structural schematic diagram of ternary coprecipitation reaction kettle right angle cutting ferrule of the utility model；
Fig. 4 is a kind of structural schematic diagram of ternary coprecipitation reaction kettle ball valve of the utility model.
In figure: 1, autoclave body；2, kettle cover；3, air inlet；4, overflow port；5, the first ball valve；6, the first cutting ferrule；7, sealing ring；
8, air inlet pipe；9, overflow discharge nozzle；10, the second cutting ferrule；11, right angle cutting ferrule；12, the second ball valve；13, locking nut；14, cutting ferrule
Nut.
Specific embodiment
To be easy to understand the technical means, creative features, achievement of purpose, and effectiveness of the utility model, below
In conjunction with specific embodiment, the utility model is further described.
As shown in Figs 1-4, a kind of ternary coprecipitation reaction kettle, including autoclave body 1, the top of autoclave body 1 are fixed with kettle cover 2,
The middle part on 1 top of autoclave body is equipped with feed inlet, and the middle part of 1 bottom end of autoclave body is equipped with discharge port, and the one end at 1 top of autoclave body is fixedly installed with
First cutting ferrule 6, the interspersed connection air inlet pipe 8 in the inside of the first cutting ferrule 6, one end of air inlet pipe 8 passes through the bottom that autoclave body 1 is placed in autoclave body 1
Portion, the other end that air inlet pipe 8 passes through the first cutting ferrule 6 are fixedly installed with the first ball valve 5, and the top of the first ball valve 5 is equipped with air inlet
3, the other end at 2 top of kettle cover is fixedly installed with the second cutting ferrule 10, and the top of the second cutting ferrule 10 is fixedly installed with right angle cutting ferrule 11,
The inside of right angle cutting ferrule 11 is interspersed to be connected with overflow discharge nozzle 9, and one end of overflow discharge nozzle 9 passes through the bottom that autoclave body 1 is placed in autoclave body 1
Portion, the other end that overflow discharge nozzle 9 passes through right angle cutting ferrule 11 are fixedly installed with the second ball valve 12, and one end of the second ball valve 12 is equipped with
Overflow port 4.
Wherein, the first cutting ferrule 6 is arranged with sealing with the junction of kettle cover 2 and the junction of the second cutting ferrule 10 and kettle cover 2
Circle 7, the first cutting ferrule 6, the second cutting ferrule 10 and right angle cutting ferrule 11 are made of stainless steel material, and sealing ring 7 plays sealing fixation
Effect prevents gas and liquid from overflowing, and stainless steel material has good corrosion resistance.
Wherein, the middle part of 10 outer wall of the middle part of 6 outer wall of the first cutting ferrule and the second cutting ferrule is threaded with locking nut 13,
The screw top of right angle cutting ferrule 11 is connected with cutting ferrule nut 14, and locking nut 13, which plays, fixes the first cutting ferrule 6 and the second cutting ferrule 10
The effect of internal pipeline, while convenient for staff to being highly adjusted, cutting ferrule nut 14 plays in fixed right angle cutting ferrule 11
The effect of portion's pipeline.
Wherein, the side of the first ball valve 5 and the side of the second ball valve 12 are fixed with valve rod, and valve rod is each passed through first
Ball valve 5 and the second ball valve 12 are connect with the sphere in portion disposed within, and valve rod controls the first ball valve 5 by sphere convenient for staff
With the opening and closing of the second ball valve 12.
It should be noted that the utility model is a kind of ternary coprecipitation reaction kettle, when specific works, staff first
First cutting ferrule 6 is fixedly mounted on to the one end at 2 top of kettle cover, while using sealing ring 7 junction is sealed, then by air inlet
Pipe 8 passes through the first cutting ferrule 6, then passes through in autoclave body 1, is placed in its bottom, is then consolidated by locking nut 13 to air inlet pipe 8
Fixed, the top of air inlet pipe 8 is fixedly mounted by the first cutting ferrule 6 and the first ball valve 5, so that air inlet pipeline is formed, then by second
Cutting ferrule 10 is fixedly mounted on the other end at 2 top of kettle cover, then with sealing ring 7 junction is sealed, then overflow discharges
Pipe 9 is socketed in the second cutting ferrule 10, is placed in its bottom across autoclave body 1, then makes overflow discharge nozzle 9 solid by locking nut 13
It is fixed, finally the top of overflow discharge nozzle 9 is fixedly mounted by right angle cutting ferrule 11 with the second ball valve 12, forms overflow passage, this
When complete the assembling of reaction kettle, then open the second ball valve 12 to protection gas is passed through inside autoclave body 1 by air inlet 3, work as autoclave body
After air pressure inside 1 reaches a certain level, overflow can be carried out by pressure difference, while by the locking nut 13 on the second cutting ferrule 10
Unscrew, adjust the height of overflow discharge nozzle 9, convenient for carrying out overflow to different height position, finally again locks locking nut 13.
The basic principles and main features of the present invention and the advantages of the present invention have been shown and described above.Current row
The technical staff of industry is described in above embodiments and description it should be appreciated that the present utility model is not limited to the above embodiments
Only illustrate the principles of the present invention, on the premise of not departing from the spirit and scope of the utility model, the utility model is also
It will have various changes and improvements, these various changes and improvements fall within the scope of the claimed invention.The utility model
Claimed range is defined by the appending claims and its equivalent thereof.
Claims (4)
1. a kind of ternary coprecipitation reaction kettle, including autoclave body (1), which is characterized in that the top of the autoclave body (1) is fixed with kettle
It covers (2), the middle part on autoclave body (1) top is equipped with feed inlet, and the middle part of autoclave body (1) bottom end is equipped with discharge port, the kettle
One end at the top of body (1) is fixedly installed with the first cutting ferrule (6), interspersed connection air inlet pipe (8) in the inside of first cutting ferrule (6),
One end of the air inlet pipe (8) passes through the bottom that autoclave body (1) is placed in autoclave body (1), and the air inlet pipe (8) passes through the first cutting ferrule (6)
The other end be fixedly installed with the first ball valve (5), the top of first ball valve (5) is equipped with air inlet (3), the kettle cover (2)
The other end at top is fixedly installed with the second cutting ferrule (10), and the top of second cutting ferrule (10) is fixedly installed with right angle cutting ferrule
(11), the inside of the right angle cutting ferrule (11) is interspersed is connected with overflow discharge nozzle (9), and one end of the overflow discharge nozzle (9) is worn
The bottom that autoclave body (1) is placed in autoclave body (1) is crossed, the other end that the overflow discharge nozzle (9) passes through right angle cutting ferrule (11) is fixedly mounted
Have the second ball valve (12), one end of second ball valve (12) is equipped with overflow port (4).
2. a kind of ternary coprecipitation reaction kettle according to claim 1, which is characterized in that first cutting ferrule (6) and kettle
The junction of the junction and the second cutting ferrule (10) and kettle cover (2) of covering (2) is arranged with sealing ring (7), the first cutting ferrule (6), the
Two cutting ferrules (10) and right angle cutting ferrule (11) are made of stainless steel material.
3. a kind of ternary coprecipitation reaction kettle according to claim 1, which is characterized in that the first cutting ferrule (6) outer wall
Middle part and the middle part of the second cutting ferrule (10) outer wall be threaded with locking nut (13), the top of the right angle cutting ferrule (11)
It is threaded with cutting ferrule nut (14).
4. a kind of ternary coprecipitation reaction kettle according to claim 1, which is characterized in that the one of first ball valve (5)
Side and the side of the second ball valve (12) are fixed with valve rod, and the valve rod is each passed through the first ball valve (5) and the second ball valve
(12) it is connect with the sphere in portion disposed within.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820343816.8U CN208340706U (en) | 2018-03-14 | 2018-03-14 | A kind of ternary coprecipitation reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820343816.8U CN208340706U (en) | 2018-03-14 | 2018-03-14 | A kind of ternary coprecipitation reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208340706U true CN208340706U (en) | 2019-01-08 |
Family
ID=64885076
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820343816.8U Expired - Fee Related CN208340706U (en) | 2018-03-14 | 2018-03-14 | A kind of ternary coprecipitation reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208340706U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111151213A (en) * | 2020-03-12 | 2020-05-15 | 沧州磐希化工有限公司 | N-N-diethyl m-methylbenzamide reactor |
-
2018
- 2018-03-14 CN CN201820343816.8U patent/CN208340706U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111151213A (en) * | 2020-03-12 | 2020-05-15 | 沧州磐希化工有限公司 | N-N-diethyl m-methylbenzamide reactor |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190108 |