CN208300878U - A kind of system that can improve protein extracting effect - Google Patents
A kind of system that can improve protein extracting effect Download PDFInfo
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- CN208300878U CN208300878U CN201721430353.0U CN201721430353U CN208300878U CN 208300878 U CN208300878 U CN 208300878U CN 201721430353 U CN201721430353 U CN 201721430353U CN 208300878 U CN208300878 U CN 208300878U
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- disintegrating apparatus
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Abstract
The utility model provides a kind of system that can improve protein extracting effect, which includes agitator tank and disintegrating apparatus a;Agitator tank lower end is connected by pipeline with the feed inlet of the upper end disintegrating apparatus a;Valve is provided on the pipeline;Agitating device is provided in the agitator tank, agitator tank top is provided with feed inlet;The disintegrating apparatus a is provided with discharge port.Water consumption when can effectively reduce the grain diameter of albumen using the system of the utility model, improve protein dissolution, extraction efficiency, shorten the protein extracting time, reduce the residual volume of albumen in bean dregs, improve the stability of protein body, while reduce extracting protein.
Description
Technical field
The utility model relates to a kind of systems that can improve protein extracting effect, belong to Protein processing technical field.
Background technique
Soybean protein is a kind of vegetable protein, rich in a variety of aminoacid ingredients needed by human, there is unique battalion
Support value.Soybean protein isolate is a kind of full-price protein food additive produced using low temperature desolventizing Soybean Meal as raw material.Greatly
The heavy technique of alkali soluble acid is generally adopted by beans protein isolate process, protein extracting process is mainly alkali soluble principle, is passed through
It controls the conditions such as certain pH value, temperature and carrys out extracting protein.
The processing of soybean protein isolate extraction process generallys use conventional device, the method extracted with the device
Are as follows: dregs of beans raw material is mixed with water with 45 degree or so of the extraction after vapour heating and is extracted, and is passed through after extracting certain time
Centrifugal pump is transported to seperator and carries out separating to obtain soya-bean milk and solid phase bean dregs, and the soya-bean milk by one or two extractions enters mixing soya-bean milk tank and enters
The heavy process of acid, the output of solid phase bean dregs carry out the processing such as taking out;Progress precipitating separates to obtain curdled milk after hydrochloric acid is added into mixing soya-bean milk,
Gained curdled milk enters neutralization step after machine for decomposing and smashing reamer solution is broken.Using above-mentioned conventional equipment, effect of extracting is by extraction time
It influences, extraction time is longer, and generally at 30 minutes or so, and effect of extracting is not good enough, and protein dissolution efficiency is lower, protein body
Stability is poor, and more to the consumption dosage of water in extraction process.
Chinese patent literature CN106720920A discloses a kind of soybean protein isolate for improving dissolubility, eliminating beany flavor
Preparation method, this method mix dregs of beans with water, and antioxidant sodium iso-vc then is added or L-cysteine is extracted, through dividing
From acid is heavy, and curdled milk separation neutralizes, enzymatic hydrolysis, and primary sterilization flash distillation, re-pasteurization flash distillation, secondary flash liquid is through high-pressure homogeneous, so
After be spray-dried, obtain soybean protein isolate product;But this method equally uses traditional alkali soluble acid sink device, equally
Have the shortcomings that present in conventional apparatus.
Therefore, to solve the above problems, proposing the utility model.
Summary of the invention
In view of the deficienciess of the prior art, the utility model provides a kind of system that can improve protein extracting effect.It adopts
It can be improved protein dissolution, extraction efficiency with the system of the utility model, shorten the protein extracting time, reduce albumen in bean dregs
Residual volume, improves the stability of protein body, while water consumption when reducing extracting protein.
The technical solution of the utility model is as follows:
A kind of system that can improve protein extracting effect, including agitator tank and disintegrating apparatus a;Agitator tank lower end passes through pipeline
It is connected with the feed inlet of the upper end disintegrating apparatus a;Valve is provided on the pipeline;
Agitating device is provided in the agitator tank, agitator tank top is provided with feed inlet;
The disintegrating apparatus a is provided with discharge port.
Preferred according to the utility model, the agitator tank is two, and disintegrating apparatus a is two;Every disintegrating apparatus a's
The feed inlet of upper end is connected with pipeline respectively and converges the lower end for being connected to two agitator tanks.
Preferably, valve is respectively arranged on the pipeline for being separately connected two disintegrating apparatus a.Pass through control valve reality
Existing material switches to the flow direction of different disintegrating apparatus.
Preferred according to the utility model, the valve is ball valve, and is connected with control room.To realize remote control.
Preferably, the ball valve is pneumatic ball valve or manual ball valve.
Preferred according to the utility model, the agitating device is quick agitator, stirring rate 0-5000r/
min.The agitating device is the prior art, commercially available acquisition, and being installed in agitator tank by the prior art.
Preferred according to the utility model, the disintegrating apparatus a is research of super-pine crush equipment.The research of super-pine crush equipment is existing
There are technology, commercially available acquisition.
Preferably, it is provided with sawtooth on the blade in the research of super-pine crush equipment, is the ultra-fine grinding of 80-200 mesh backlash
Equipment.
Preferably, the research of super-pine crush equipment is HOP-L55 type cutting-type wet process disintegrator.Above-mentioned pulverizer is existing skill
Art, commercially available acquisition.
Preferred according to the utility model, the system that can improve protein extracting effect further includes seperator a, seperator
B, disintegrating apparatus b and the heavy tank of acid, the discharge port of disintegrating apparatus a are connected with the feed inlet of seperator a, the discharge port of seperator a and
The feed inlet of the heavy tank of acid is connected, and the discharge port of the heavy tank of acid is connected with the feed inlet of disintegrating apparatus b, the discharge port of disintegrating apparatus b and
The feed inlet of seperator b is connected.
According to the utility model, the method for carrying out extracting protein using the above-mentioned system that can improve protein extracting effect, packet
Include step:
Protein-contg raw material, water and defoaming agent are added in agitator tank by the feed inlet of agitator tank, filled in stirring
Set under stirring, 28-35 DEG C immersion 5-30 minutes, obtain mixed liquor;Then control valve makes mixed liquor enter crushing by pipeline and sets
Shearing crushing is carried out in standby a;Then extract liquor is flowed out to obtain by the discharge port of disintegrating apparatus a, through seperator a separate albumin milk and
Filter residue.
Preferred according to the utility model, the protein-contg raw material are can be by the heavy method extraction of traditional alkali soluble acid
The raw material of albumen in material.
Preferably, the protein-contg raw material are dregs of beans.
Preferred according to the utility model, the mass ratio of the protein-contg raw material and water is 1:4-10.
Preferably, the mass ratio of the protein-contg raw material and water is 1:8.
Preferred according to the utility model, the defoaming agent is food-grade defoaming agent, and the defoaming agent is protein-contg original
The 1-2 ‰ of the quality of material.
Preferred according to the utility model, the stirring rate is 4000-5000r/min;Preferably 4500r/min.
Preferred according to the utility model, it is 2000-4000r/min that the shearing, which crushes revolving speed, and shearing crush efficiency is
0.2-0.4m3/ min, shearing grinding time are 2-10min.
It is preferred according to the utility model, the method for the extracting protein further include: obtained albumin milk enters the heavy tank of acid
Middle progress acid is heavy, obtains the heavy liquid of acid;The heavy liquid of acid enters through the heavy tank discharge port of acid carries out shearing crushing in disintegrating apparatus b, most pass through afterwards
The isolated albumen curd of seperator b.
Preferably, the heavy acid used of acid is food grade hydrochloric acid, and dosage is that albumin milk per ton corresponds to 120-150kg food grade salt
Acid makes the pH of the heavy liquid of acid in 4.4-4.6.
Preferably, it is 2000-4000r/min that the shearing, which crushes revolving speed, and shearing crush efficiency is 0.2-0.4m3/ min,
Shearing grinding time is 2-10min.
According to the utility model, the heavy technique of acid is the prior art, common process.
It the technical characterstic of the utility model and has the beneficial effect that:
1, it is provided with quick agitator in the utility model agitator tank, can guarantee the materials such as protein-contg raw material and water
Be sufficiently mixed in short time, fast reaction while, protein-contg raw material can be allowed uniformly to be suspended in tank body, will not be produced
On unboiled water and protein-contg raw material the phenomenon that lower leaf, and can effectively ensure that discharging homogeneity and stable solid-liquid
Than.
2, protein-contg raw material enter in disintegrating apparatus after extracting in agitator tank, are formed at high speed high-intensitive
Shearing force, clipped smashed extract liquor sieve with 100 mesh sieve it is achievable 100% sieving.At pulverizer through the utility model
Reason, the partial size of albumen obviously become smaller, and improve the dissolution of albumen, Protein Separation effect has clear improvement, while protein body is steady
Qualitative increase is conducive to the progress of the techniques such as subsequent neutralization;After the sieving of gained extract liquor, residue is compared and does not apply this reality on sieve
About 32wt% is reduced with Novel mill, isolated albumin milk CP (protein content) improves about 5.3%, Protein Separation effect
Improved.
3, when water and protein-contg raw material quality ratio are 8:1, by the obtained extraction of the system of the utility model
Liquid pol can reach 11.2, isolate filter residue, and the CP for then manually squeezing isolated albumin milk is reduced than common process
4.5 percentage point;It can be seen that high-speed stirred extraction and the raising of shearing crushing effect are conducive to the dissolution and acceleration of albumen
The swelling of fiber, and extraction time can be shortened;
When water and protein-contg raw material quality ratio are 5:1, are crushed, still be able to after impregnating 5min under stiring
Effect promotes protein dissolution and fiber swelling;It follows that even if the system of the utility model is in lesser ratio of water to material, short period
Stirring soaking conditions under, remain to effectively facilitate protein dissolution and fiber swelling, and lead to albuminous degeneration without liquid heating
The case where.
4, simultaneously, there is lesser grain fineness using the albumen curd that the system of the utility model is prepared, it is right
The water suction aging of albumen has facilitation after subsequent neutralization, can shorten ageing time.
Detailed description of the invention
Fig. 1 is the system diagram that the utility model can improve protein dissolution effect;
Wherein, 1, agitator tank, 2, pipeline, 3, pneumatic ball valve, 4, research of super-pine crush equipment a, 5, discharge port, 6, control room, 7,
Quick agitator.
Fig. 2 is the system diagram that protein dissolution effect can be improved in the utility model embodiment 2;
Wherein, 8, seperator a, 9, the heavy tank of acid, 10, research of super-pine crush equipment b, 11, seperator b.
Specific embodiment
The utility model is described further in the following with reference to the drawings and specific embodiments, but the protection model of the utility model
It encloses without being limited thereto.
Experimental method, equipment described in following embodiments are unless otherwise specified conventional method, equipment simultaneously;It is described
Reagent and material commercially obtain unless otherwise specified.
Embodiment 1
A kind of system that can improve protein extracting effect, including two agitator tanks 1 and two research of super-pine crush equipment a4;Every
The feed inlet of the upper end research of super-pine crush equipment a4 is connected with pipeline 2 respectively and converges the lower end for being connected to two agitator tanks 1.Described point
Pneumatic ball valve 3 Lian Jie not be respectively arranged on the pipeline 2 of two research of super-pine crush equipment a4.Object is realized by control pneumatic ball valve 3
Expect to switch to the flow direction of different research of super-pine crush equipment a4;
Quick agitator 7, stirring rate 0-5000r/min are provided in the agitator tank 1;The agitator tank 1
Top is provided with feed inlet.The quick agitator 7 is the prior art, commercially available acquisition;And it is installed on and stirs by the prior art
It mixes in tank 1.
The research of super-pine crush equipment a4 is provided with discharge port 5, and research of super-pine crush equipment a4 is HOP-L55 type cutting-type wet process powder
Broken machine, commercially available acquisition, Wuxi He Pu light equipment Technology Co., Ltd. are on sale.
The pneumatic ball valve 3 is connected with control room 6.To realize remote control.
Embodiment 2
A kind of system that can improve protein extracting effect, including two agitator tanks 1 and two research of super-pine crush equipment a4;Every
The feed inlet of the upper end research of super-pine crush equipment a4 is connected with pipeline 2 respectively and converges the lower end for being connected to two agitator tanks 1.Described point
Pneumatic ball valve 3 Lian Jie not be respectively arranged on the pipeline 2 of two research of super-pine crush equipment a4.Object is realized by control pneumatic ball valve 3
Expect to switch to the flow direction of different research of super-pine crush equipment a4;
Quick agitator 7, stirring rate 0-5000r/min are provided in the agitator tank 1;The agitator tank 1
Top is provided with feed inlet.The quick agitator 7 is the prior art, commercially available acquisition;And it is installed on and stirs by the prior art
It mixes in tank 1.
The research of super-pine crush equipment a4 is provided with discharge port 5, and research of super-pine crush equipment a4 is HOP-L55 type cutting-type wet process powder
Broken machine, commercially available acquisition.
The pneumatic ball valve 3 is connected with control room 6.To realize remote control.
The system also includes seperator a8, seperator b11, research of super-pine crush equipment b10 and the heavy tank 9 of acid, two superfine powders
The discharge port of broken equipment a4 is converged by pipeline is connected to seperator a8, and seperator a8 is connected with the feed inlet of the heavy tank 9 of acid, and acid is heavy
The discharge port of tank 9 is connected with the feed inlet of the upper end research of super-pine crush equipment b10, the discharge port and seperator of research of super-pine crush equipment b10
B11 is connected;The heavy tank 9 of the seperator a8, seperator b11, research of super-pine crush equipment b10, acid is the prior art, commercially available to obtain
?;Wherein, research of super-pine crush equipment b10 is HOP-L55 type cutting-type wet process disintegrator, and commercially available acquisition, Wuxi He Pu light industry sets
Standby Technology Co., Ltd. is on sale.
Application examples 1
The method for carrying out extracting protein using system described in embodiment 1, comprising steps of
1000g dregs of beans, 8L water and 2g food-grade defoaming agent are added in agitator tank 1, in the stirring of quick agitator 7
Under (stirring rate 4500r/min), 30 DEG C impregnate 25 minutes;Then remote control pneumatic ball valve 3, makes mixed liquor pass through pipeline
2 enter in research of super-pine crush equipment a4, and in the research of super-pine crush equipment of 80 mesh backlash, shearing is crushed 3 minutes under 3000 revolving speeds, cut
Cutting crush efficiency is 0.3m3/ min obtains extract liquor 1;Then in the research of super-pine crush equipment of 200 mesh backlash, under 3000 revolving speeds
Shearing crushes 3 minutes, and shearing crush efficiency is 0.3m3/ min obtains extract liquor 2, and surveying its pol is 11.2BX.Extract liquor 2 is through dividing
The a that disembarks separates to obtain soya-bean milk and bean dregs.
It takes extract liquor 1,2 sample of extract liquor to sieve with 100 mesh sieve respectively, has a small amount of fiber remnants, extract liquor on the sieve of extract liquor 1
Without fiber remnants on 2 sieves.
Application examples 2
The method for carrying out extracting protein using system described in embodiment 1, comprising steps of
1000g dregs of beans, 5L water and 2g food-grade defoaming agent are added in agitator tank 1, in the stirring of quick agitator 7
Under (stirring rate 4500r/min), 30 DEG C impregnate 5 minutes;Then remote control pneumatic ball valve 3 makes mixed liquor pass through pipeline 2
Into in research of super-pine crush equipment a4, in the research of super-pine crush equipment of 80 mesh backlash, shearing is crushed 3 minutes under 3000 revolving speeds, is cut
Cutting crush efficiency is 0.3m3/ min obtains extract liquor 1;Then in the research of super-pine crush equipment of 200 mesh backlash, under 3000 revolving speeds
Shearing crushes 3 minutes, and shearing crush efficiency is 0.3m3/ min obtains extract liquor 2, and surveying its pol is 16.5BX.Extract liquor 2 is through dividing
The a that disembarks separates to obtain soya-bean milk and bean dregs.
Application examples 3
The method for carrying out extracting protein using system described in embodiment 2, comprising steps of
Acid is carried out in the heavy tank of soya-bean milk and food grade hydrochloric acid addition acid that application examples 1 is obtained to sink, and obtains sour heavy liquid;The acid is heavy
Technique is the prior art, and common process, the heavy temperature of acid is room temperature, and the dosage of food grade hydrochloric acid is the pH 4.5 for making the heavy liquid of acid;Institute
The heavy liquid of obtained acid enters in the research of super-pine crush equipment b of 80 mesh backlash through the heavy tank discharge port of acid, is 3000r/min in revolving speed, cuts
Crushing 3 minutes is cut, shearing crush efficiency is 0.3m3/ min, obtains mixed liquor;Gained mixed liquor is isolated solidifying through seperator b
Cream.
Application examples 4
The method of extracting protein is as described in application examples 3, the difference is that research of super-pine crush equipment b is 200 mesh backlash, it is other
Condition step and application examples 3 are consistent.
Comparative example 1
1000g dregs of beans is mixed with 45 degree of the 8L water after vapour heating and is extracted, must be extracted after extracting 25min
Liquid;Extract liquor is transported to seperator through centrifugal pump and carries out separating to obtain soya-bean milk and bean dregs.
Comparative example 2
1000g dregs of beans is mixed with 45 degree of the 5L water after vapour heating and is extracted, must be extracted after extracting 25min
Liquid;Extract liquor is transported to seperator through centrifugal pump and carries out separating to obtain soya-bean milk and bean dregs.
Test example 1
Extract liquor 1,2 sample of extract liquor in application examples 1 are taken, respectively with bean dregs and soya-bean milk are taken after 200 mesh filtered through gauze, is surveyed
(Nitrogen Solubility Index is commonly used to indicate big by moisture, CP (crude protein mass content) and NSI in examination bean dregs, soya-bean milk and extract liquor 2
The mass content of beans protein isolate solubility and its contained functional soy albumen);And the bean dregs that test comparison example 1 obtains simultaneously
With the content of moisture, CP and NSI in soya-bean milk, result data is as shown in table 1:
The index test of 1 soya-bean milk of table
Sample | Moisture | CP | NSI |
The soya-bean milk that extract liquor 1 obtains | 91.2 | 65.6 | 17.3 |
The soya-bean milk that extract liquor 2 obtains | 91.5 | 69.3 | 47.3 |
Extract liquor 2 | 89.9 | 59.7 | 16 |
The soya-bean milk that comparative example 1 obtains | 91.1 | 64 | / |
The index test of 2 bean dregs of table
Sample | Moisture | CP |
The bean dregs that extract liquor 1 obtains | 80.6 | 27.2 |
The bean dregs that extract liquor 2 obtains | 81 | 25.9 |
The bean dregs that comparative example 1 obtains | 85.2 | 30.4 |
By this test example it is found that after ultra-fine pulverizer disintegrating, the CP of isolated soya-bean milk is improved compared to comparative example 1
5.3%, Protein Separation effect is improved;The obtained CP in bean dregs reduces by 4.5 percentages than common process (comparative example 1)
Point;It can be seen that quick agitator 7 and research of super-pine crush equipment a4 are conducive to the dissolution of albumen and the swelling of accelerating fibers.
Test example 2
To in 2 step of application examples extract liquor 1 and extract liquor 2 carry out index of correlation test, test method is as follows:
It takes the extract liquor 1 in application examples 2,2 sample of extract liquor to sieve with 100 mesh sieve respectively, tests the upper fibre of the sieve of extract liquor 1,2 respectively
Dimension residual quantity accounts for the ratio of extract liquor 1 or 2 mass, abbreviation oversize mass ratio.
The extract liquor sample for taking extract liquor 1, extract liquor 2 and comparative example 2 to obtain tests wherein moisture, CP, NSI and pol,
As a result as shown in the table:
The index test of 3 extract liquor of table
By this test example it is found that even if under the stirring soaking conditions of short period, of the invention is in lesser ratio of water to material
System remains to effectively facilitate protein dissolution and fiber swelling, and shears that degree of grinding is bigger, and soybean protein isolate contains in extract liquor
It measures higher.
Test example 3
To the mixed liquor sampling in application examples 3,4, respectively through 100 mesh screens, the quality that upper residue is sieved in test accounts for mixed
Close the ratio of liquid quality, abbreviation oversize mass ratio;The oversize mass ratio for the mixed liquor that application examples 3 obtains is 10%,
The mixed liquor that application examples 4 obtains is after 100 mesh screens, noresidue on sieve.
It is as shown in table 4 that moisture, CP and NSI test, test result are carried out to the curdled milk that application examples 3,4 obtains;
The index test of 4 curdled milk of table
Sample | Moisture | CP | NSI |
The curdled milk that application examples 3 obtains | 78.9 | 87.4 | 5.9 |
The curdled milk that application examples 4 obtains | 86.8 | 84.9 | 8 |
By this test example it is found that protein content is higher in the curdled milk being prepared using system of the invention, by 200 mesh
The ultra-fine pulverizer disintegrating of backlash makes albumen have smaller grain diameter, the more conducively separation of soybean protein isolate, albumen point
It is preferable from effect.
Claims (10)
1. a kind of system that can improve protein extracting effect, which is characterized in that including agitator tank and disintegrating apparatus a;Under agitator tank
End is connected by pipeline with the feed inlet of the upper end disintegrating apparatus a;Valve is provided on the pipeline;
Agitating device is provided in the agitator tank, agitator tank top is provided with feed inlet;
The disintegrating apparatus a is provided with discharge port.
2. the system according to claim 1 that protein extracting effect can be improved, which is characterized in that the agitator tank is two
Platform, disintegrating apparatus a are two;The feed inlet of the upper end of every disintegrating apparatus a, which is connected respectively and is converged with pipeline, is connected to two
The lower end of agitator tank.
3. the system according to claim 2 that protein extracting effect can be improved, which is characterized in that described to be separately connected two
Valve is respectively arranged on the pipeline of disintegrating apparatus a.
4. the system according to claim 1 that protein extracting effect can be improved, which is characterized in that the valve is ball valve,
And it is connected with control room.
5. the system according to claim 4 that protein extracting effect can be improved, which is characterized in that the ball valve is Pneumatic ball
Valve or manual ball valve.
6. the system according to claim 1 that protein extracting effect can be improved, which is characterized in that the agitating device is fast
Fast agitating device, stirring rate 0-5000r/min.
7. the system according to claim 1 that protein extracting effect can be improved, which is characterized in that the disintegrating apparatus a is
Research of super-pine crush equipment.
8. the system according to claim 7 that protein extracting effect can be improved, which is characterized in that the research of super-pine crush equipment
Blade on be provided with sawtooth, be 80-200 mesh backlash research of super-pine crush equipment.
9. the system according to claim 7 that protein extracting effect can be improved, which is characterized in that the research of super-pine crush equipment
For HOP-L55 type cutting-type wet process disintegrator.
10. the system according to claim 1 that protein extracting effect can be improved, which is characterized in that described to improve albumen
The system of effect of extracting further includes seperator a, seperator b, disintegrating apparatus b and the heavy tank of acid, the discharge port of disintegrating apparatus a and separation
The feed inlet of machine a is connected, and the discharge port of seperator a is connected with the feed inlet of the heavy tank of acid, the discharge port and disintegrating apparatus b of the heavy tank of acid
Feed inlet be connected, the discharge port of disintegrating apparatus b is connected with the feed inlet of seperator b.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107744048A (en) * | 2017-10-30 | 2018-03-02 | 山东禹王生态食业有限公司 | A kind of system and method that can improve protein extracting effect |
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CN107744048A (en) * | 2017-10-30 | 2018-03-02 | 山东禹王生态食业有限公司 | A kind of system and method that can improve protein extracting effect |
CN107744048B (en) * | 2017-10-30 | 2023-11-28 | 山东禹王生态食业有限公司 | System and method capable of improving protein extraction effect |
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TR01 | Transfer of patent right |
Effective date of registration: 20191206 Address after: 164800 Yuan Yi grain depot yard, Chunhe street, Kedong Town, Kedong County, Qiqihar City, Heilongjiang Province Patentee after: Soybean protein food Co. Ltd. Yuwang Kedong Address before: 251200 Fuhua street, hi tech Development Zone, Shandong, Dezhou Patentee before: Shandong Yuwang Ecological Food Industry Co., Ltd. |
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TR01 | Transfer of patent right |