CN208288016U - A kind of reaction kettle that can quickly remove water - Google Patents
A kind of reaction kettle that can quickly remove water Download PDFInfo
- Publication number
- CN208288016U CN208288016U CN201820618994.7U CN201820618994U CN208288016U CN 208288016 U CN208288016 U CN 208288016U CN 201820618994 U CN201820618994 U CN 201820618994U CN 208288016 U CN208288016 U CN 208288016U
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- main tank
- tank body
- reaction kettle
- reaction
- condenser
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 53
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 47
- 238000010438 heat treatment Methods 0.000 claims abstract description 12
- 238000005086 pumping Methods 0.000 claims abstract description 11
- 230000005540 biological transmission Effects 0.000 claims abstract description 7
- 230000008878 coupling Effects 0.000 claims abstract description 7
- 238000010168 coupling process Methods 0.000 claims abstract description 7
- 238000005859 coupling reaction Methods 0.000 claims abstract description 7
- 238000010079 rubber tapping Methods 0.000 claims abstract description 5
- 238000000338 in vitro Methods 0.000 claims abstract description 3
- 229920000742 Cotton Polymers 0.000 claims description 8
- 238000007789 sealing Methods 0.000 claims description 4
- 239000002994 raw material Substances 0.000 abstract description 14
- 230000032050 esterification Effects 0.000 abstract description 5
- 238000005886 esterification reaction Methods 0.000 abstract description 5
- 239000007795 chemical reaction product Substances 0.000 abstract description 4
- 238000004064 recycling Methods 0.000 abstract description 2
- 239000004615 ingredient Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000006227 byproduct Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000001914 filtration Methods 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000012808 vapor phase Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
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- Fats And Perfumes (AREA)
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Abstract
The utility model discloses the reaction kettles that one kind can be removed water quickly, including main tank body, the upper end of main tank body is equipped with decelerating motor, the lower end of decelerating motor is successively arranged transmission shaft, shaft coupling, blender, main tank is arranged with hot steam heating layer in vitro, the side outer wall of hot steam heating layer is equipped with air inlet, and other side outer wall is equipped with gas outlet, and the outside of gas outlet is equipped with drain valve；The side wall of main tank body is equipped with vacuum port, vacuum port is externally provided with Temperature control valve, Temperature control valve is connected with the constant warm tube for tilting upward setting, constant warm tube is connected with condenser, the lower end of condenser is equipped with tapping sample tap, condenser is connect by conveyance conduit, check valve, the first booster pump with oil water separator, and oil water separator is connected with the second-pumping pipeline for protruding into main tank interior.The reaction kettle of the utility model can rapidly remove moisture content, and the reaction raw materials and reaction product that are mingled in recycling moisture content continue to participate in reaction, improve the yield of esterification or aldolisation.
Description
Technical field
The utility model relates to reaction kettle fields, and in particular to the reaction kettle that one kind can be removed water quickly.
Background technique
In esterification or aldolisation, usually reaction kettle will be put into together with the materials such as raw material and acid base catalysator
In, with continuous heating, reaction carries out towards the positive direction, can generate a large amount of by-product water, and water can diluting reaction product and not instead
Complete raw material is answered, hinders reaction forward to carry out, slows down reaction rate.Existing reaction kettle is concentrated using vacuum pump pressure mostly
Remove moisture content.But the vacuum port aperture of vacuum pump connection is smaller, water removal slowly, can also carry a large amount of reaction raw materials and anti-
Product is answered, reaction yield is reduced.Therefore, it is necessary to the reaction kettle water removing structures under a kind of normal pressure, and can recycle lacking for moisture content carrying
Quantitative response raw material and reaction product improve reaction yield to promote reaction forward to carry out.
Utility model content
In order to solve the above technical problems, the purpose of this utility model is to provide the reactions that one kind can be removed water quickly
Kettle can rapidly remove the moisture content in reaction kettle, and the reaction raw materials and reaction product that are mingled in recycling moisture content continue to participate in
Reaction, improves the yield of esterification or aldolisation.
The purpose of this utility model can be achieved through the following technical solutions:
A kind of reaction kettle that can quickly remove water, including main tank body, the upper end of main tank body are equipped with decelerating motor, the deceleration electricity
The lower end of machine is successively arranged coaxially connected transmission shaft, shaft coupling, blender, and main tank is arranged with hot steam heating layer, institute in vitro
The side outer wall for stating hot steam heating layer is equipped with air inlet, and other side outer wall is equipped with gas outlet, and the outside of gas outlet is equipped with hydrophobic
Valve；The side wall of the main tank body is equipped with vacuum port, and vacuum port is externally provided with Temperature control valve, and Temperature control valve, which is connected with, tilts upward setting
Constant warm tube, constant warm tube is connected with condenser by condensing water conduit, and the lower end of condenser is equipped with tapping sample tap, and condenser is logical
It crosses conveyance conduit, check valve, the first booster pump to connect with oil water separator, oil water separator, which is connected with, protrudes into main tank interior
Second-pumping pipeline.
Further, the junction of the decelerating motor and main tank body is equipped with sealing bearing, and the shape of the blender is
Anchor formula or flat frame.
Further, the vacuum port includes the bolt of ring flange and clamp flange disk, and the internal orifice dimension of ring flange is 10-
15cm。
Further, it is 105-110 DEG C that the temperature of the constant warm tube is constant, is equipped with several layers in constant warm tube and filters cotton paper.
Further, the second-pumping pipeline is equipped with one-way throttle valve and the second booster pump.
The reaction kettle that can quickly remove water of the utility model when in use, reaction raw materials is put into main tank body, and opening subtracts
Speed motor, decelerating motor drive transmission shaft, shaft coupling, blender to rotate and stir material, hot steaming are constantly passed through into air inlet
Vapour, hot steam are discharged from gas outlet, and hot steam heating layer heats main tank body, stablize when being heated to reaction system to 100
DEG C or more when, the by-product water of generation can evaporate, and Temperature control valve is opened, and constant warm tube can make water remain vapor phase and wear
Through filter pulp paper, oily ingredient will be filtered cotton paper absorption, and vapor is condensed into liquid by condensing water conduit, condenser, beats
Opening one-way valve, the first booster pump, liquid can be along conveyance conduits and under the pressurization of the first booster pump, into water-oil separating
It is layered in device；When the oily component density for being mingled with reaction raw materials, product is smaller, layering is on upper layer, and the bigger meeting of water density divides
Layer is in lower layer；After layering is stablized, the second booster pump can be opened, and adjust one-way throttle valve, reaction raw materials, product will be mingled with
Oily ingredient continues to participate in reaction along second-pumping pipeline to main tank body.
The utility model has the beneficial effects that
(1) reaction kettle that can quickly remove water of the utility model incudes the temperature of steam by Temperature control valve, so that being mingled with
The vapor of reaction raw materials and product is being condensed by condenser, after oil water separator layering, can will be mingled with reaction raw materials, be produced
The oily ingredient of object, which is delivered in main tank body, to be continued to participate in reaction, which can rapidly remove the moisture content in reaction kettle, mention
High esterification or aldolisation etc. generate the yield of the high-temperature pressures such as by-product water reaction.
(2) vacuum port fastens ring flange using bolt, while the internal orifice dimension of ring flange is larger, it is ensured that big stream
The steam of amount passes through, and improves water rem oval.
(3) contact area of the blender and material of anchor formula or flat frame is big, and stability of rotation, accelerates esterification or contracting
The rate of aldehyde reaction.
(4) there are filtering cotton paper good Adsorption Filtration Properties can obstruct absorption vapor when steam passes through constant warm tube
In oily drop ingredient alleviate subsequent oil water separator, second-pumping pipeline so that the vapor of higher degree passes through
Workload.
Detailed description of the invention
The utility model will be further described below with reference to the accompanying drawings.
Fig. 1 is the structural schematic diagram of the reaction kettle that can quickly remove water of embodiment 1；
Fig. 2 is the structural schematic diagram of the reaction kettle that can quickly remove water of embodiment 2.
In figure: 1, main tank body, 2, hot steam heating layer, 3, decelerating motor, 4, transmission shaft, 5, shaft coupling, 6, blender, 7,
Temperature control valve, 8, constant warm tube, 9, condensing water conduit, 10, condenser, 11, vacuum port, 12, conveyance conduit, 13, check valve, 14,
First booster pump, 15, oil water separator, 16, second-pumping pipeline, 17, sealing bearing, 18, one-way throttle valve, 19, second increases
Press pump, 21, air inlet, 22, gas outlet, 23, drain valve, 81, filtering cotton paper, 101, tapping sample tap, 111, ring flange, 112,
Bolt.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without creative efforts
All other embodiment obtained, fall within the protection scope of the utility model.
Embodiment 1
As shown in Figure 1, a kind of reaction kettle that can quickly remove water, including main tank body 1 are present embodiments provided, main tank body 1
Upper end is equipped with decelerating motor 3, and the lower end of decelerating motor 3 is successively arranged coaxially connected transmission shaft 4, shaft coupling 5, blender 6, main
Hot steam heating layer 2 is arranged with outside tank body 1.The side outer wall of hot steam heating layer 2 is equipped with air inlet 21, and other side outer wall is equipped with
The outside of gas outlet 22, gas outlet is equipped with drain valve 23.The side wall of main tank body 1 is equipped with vacuum port 11, and vacuum port 11 is externally provided with control
Warm valve 7, Temperature control valve 7 are connected with the constant warm tube 8 for tilting upward setting, and constant warm tube 8 is connected with condensation by condensing water conduit 9
Device 10, the lower end of condenser 10 are equipped with tapping sample tap 101, and condenser 10 is pressurized by conveyance conduit 12, check valve 13, first
Pump 14 is connect with oil water separator 15, and oil water separator 15 is connected with the second-pumping pipeline 16 protruded into inside main tank body 1.Slow down
The junction of motor 3 and main tank body 1 is equipped with sealing bearing 17, and the shape of blender 6 is anchor formula.Vacuum port 11 includes ring flange
111 and clamp flange disk 111 bolt 112, the internal orifice dimension of ring flange 111 is 10-15cm.The temperature of constant warm tube 8 is constant to be
105-110 DEG C, the interior several layers that are equipped with of constant warm tube 8 filter cotton paper 81.Second-pumping pipeline 16 is equipped with one-way throttle valve 18 and the
Two booster pumps 19.
The reaction kettle of the present embodiment, specific work process the following steps are included:
(1) reaction raw materials are put into main tank body 1, open decelerating motor 3, and decelerating motor 3 drives transmission shaft 4, shaft coupling
5, blender 6 rotates and stirs material, and hot steam is constantly passed through into air inlet 21, and hot steam is discharged from gas outlet 22, is passed through
There is the hot steam heating layer 2 of hot steam to heat main tank body 1；
(2) when stable to 100 DEG C or more of temperature of reaction system in main tank body 1, the by-product water of generation can evaporate, control
Warm valve 7 is opened, so that water remains vapor phase and penetrates filter cotton paper 81, oily ingredient will be filtered 8 meeting of constant warm tube
Cotton paper 81 adsorbs, and vapor is condensed into liquid by condensing water conduit 9, condenser 10；
(3) check valve 13, the first booster pump 14 are opened, liquid can be along conveyance conduit 12 and in the increasing of the first booster pump 14
Under pressure effect, into being layered in oil water separator 15；When the oily component density for being mingled with reaction raw materials, product is smaller, layering
On upper layer, and water density is bigger can be layered in lower layer；
(4) after layering is stablized, the second booster pump 19 is opened, and adjust one-way throttle valve 18, reaction raw materials, product will be mingled with
Oily ingredient be delivered in main tank body 1 along second-pumping pipeline 16, continue to participate in reaction.
Embodiment 2
As shown in Fig. 2, the reaction kettle that can quickly remove water of the present embodiment, the difference from embodiment 1 is that, blender 6 is
Plate and frame, it is big with the contact area of reaction mass, increase reaction rate.
Above content is only to the utility model structure example and explanation, the technology people of affiliated the art
Member makes various modifications or additions to the described embodiments or is substituted in a similar manner, without departing from reality
With novel structure or beyond the scope defined by this claim, all should belong to the protection range of the utility model.
Claims (5)
1. the upper end of the reaction kettle that one kind can be removed water quickly, including main tank body, main tank body is equipped with decelerating motor, the decelerating motor
Lower end be successively arranged coaxially connected transmission shaft, shaft coupling, blender, main tank is arranged with hot steam heating layer in vitro, special
Sign is that the side outer wall of the hot steam heating layer is equipped with air inlet, and other side outer wall is equipped with gas outlet, the outside of gas outlet
Equipped with drain valve；The side wall of the main tank body is equipped with vacuum port, and vacuum port is externally provided with Temperature control valve, and Temperature control valve is connected with inclination
The constant warm tube set up, constant warm tube are connected with condenser by condensing water conduit, and the lower end of condenser is equipped with tapping sample tap,
Condenser is connect by conveyance conduit, check valve, the first booster pump with oil water separator, and oil water separator, which is connected with, protrudes into main tank
The second-pumping pipeline in internal portion.
2. the reaction kettle according to claim 1 that can quickly remove water, which is characterized in that the decelerating motor and main tank body
Junction is equipped with sealing bearing, and the shape of the blender is anchor formula or flat frame.
3. the reaction kettle according to claim 1 that can quickly remove water, which is characterized in that the vacuum port include ring flange and
The bolt of clamp flange disk, the internal orifice dimension of ring flange are 10-15cm.
4. the reaction kettle according to claim 1 that can quickly remove water, which is characterized in that the temperature of the constant warm tube is constant to be
105-110 DEG C, the interior several layers that are equipped with of constant warm tube filter cotton paper.
5. the reaction kettle according to claim 1 that can quickly remove water, which is characterized in that the second-pumping pipeline is equipped with
One-way throttle valve and the second booster pump.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820618994.7U CN208288016U (en) | 2018-04-27 | 2018-04-27 | A kind of reaction kettle that can quickly remove water |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820618994.7U CN208288016U (en) | 2018-04-27 | 2018-04-27 | A kind of reaction kettle that can quickly remove water |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208288016U true CN208288016U (en) | 2018-12-28 |
Family
ID=64703770
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820618994.7U Expired - Fee Related CN208288016U (en) | 2018-04-27 | 2018-04-27 | A kind of reaction kettle that can quickly remove water |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208288016U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113967449A (en) * | 2021-10-16 | 2022-01-25 | 江苏优普生物化学科技股份有限公司 | Chemical colloid production is with catalytic reaction equipment that has quantitative material loading structure |
-
2018
- 2018-04-27 CN CN201820618994.7U patent/CN208288016U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113967449A (en) * | 2021-10-16 | 2022-01-25 | 江苏优普生物化学科技股份有限公司 | Chemical colloid production is with catalytic reaction equipment that has quantitative material loading structure |
| CN113967449B (en) * | 2021-10-16 | 2022-08-12 | 江苏优普生物化学科技股份有限公司 | Chemical colloid production is with catalytic reaction equipment that has quantitative material loading structure |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20191213 Address after: Donggang Zhen Dong Qinggil Cun Tin District of Xishan city of Wuxi province Jiangsu 214000 North Canal Bridge Bridge Patentee after: HUGO NEW MATERIALS (WUXI) CO.,LTD. Address before: Longpan road Xuanwu District of Nanjing city of Jiangsu Province, No. 159 210037 Patentee before: Nanjing Forestry University |
|
| TR01 | Transfer of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20181228 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |