CN208275382U - A kind of reaction tower with articles holding table - Google Patents

A kind of reaction tower with articles holding table Download PDF

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Publication number
CN208275382U
CN208275382U CN201820392667.4U CN201820392667U CN208275382U CN 208275382 U CN208275382 U CN 208275382U CN 201820392667 U CN201820392667 U CN 201820392667U CN 208275382 U CN208275382 U CN 208275382U
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CN
China
Prior art keywords
reaction tower
holding table
articles holding
sampling
pedestal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201820392667.4U
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Chinese (zh)
Inventor
孙火青
孙涛涛
韦玉川
孙俊华
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HAISHUN CHEMICAL CO Ltd
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HAISHUN CHEMICAL CO Ltd
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Priority to CN201820392667.4U priority Critical patent/CN208275382U/en
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Publication of CN208275382U publication Critical patent/CN208275382U/en
Expired - Fee Related legal-status Critical Current
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Abstract

The utility model discloses a kind of reaction towers with articles holding table, belong to field of chemical equipment.A kind of reaction tower with articles holding table of the utility model, including reaction tower ontology, sampler and articles holding table, sampler are arranged in reaction tower bodies top;The articles holding table includes pedestal and glove pipe, and at least two glove pipe is fixed on the pedestal;Pedestal is removably mounted at reaction tower bodies top.High settings such as the glove pipe or there are differences in height.The pedestal bottom is concave arc, or is embedded with balance weight in pedestal bottom.This programme by the improvement to sampling apparatus structure, can on-line period, while not will cause material waste.Articles holding table is arranged in this programme at the top of reaction tower, can be used for placing some detection meters, takes conveniently, be convenient for sample detection.

Description

A kind of reaction tower with articles holding table
Technical field
The utility model relates to chemical equipment technical fields, more specifically to a kind of reaction tower with articles holding table.
Background technique
Sodium alkyl sulfonate is a kind of important surfactant, it is widely used in the industry such as washing, tanning, simultaneously It is a kind of important chemical intermediate again, such as is reacted by sodium alkyl sulfonate with phosphorus pentachloride and produce alkyl sulfonyl chloride, into Enter available a variety of surfactants with special construction.
When carrying out chemical industry synthesis sodium sulfonate using reaction kettle, in order to adjust the parameter of control material in reactor in time, It needs to carry out real-time tracking to the response situation in reaction kettle, so that the sampling out of reaction kettle be needed to carry out analysis test.Such as Detect temperature, the specific gravity etc. of charging.Currently used sampling method is to utilize manual sampling, by opening reaction kettle kettle cover, or Person is to be sampled using sampling apparatus from reaction tower.After sampling, detected using detection meter.
It is well known that the general height of reaction tower is higher, in order to easy to operate, can generally be placed beside reaction tower ladder or Person is to build platform, and operator increases oneself height by ladder or platform, to meet the various operational requirements to reaction tower.
But when detecting, need to carry various detection meters, such as thermometer, densimeter, this frangible detection meter is uncomfortable Conjunction is carried, and will individually be taken when but if detecting every time and comparatively laborious.If detection meter is directly placed on reaction Top of tower, and be easy to fall to cause to detect and count damage.
By retrieval, reaction tower has sampler mostly at present, but does not provide Chinese patent and disclose one kind (application number: 201110246064.6), external circulating system being connect reactor on-line period method with reactor, sampler and outer Pipeloop connection, when need to sample, first turns on external circulating system, the material in reactor enters the special-purpose taking of reactor outer circulation pipeline In sample device, it is then shut off the valve suitable for reading of reactor, to Special sample taker plus nitrogen, pushes back external circulation line from base opening by material It is back to reactor again, is repeated several times to clean displacement, finally material is extruded from sampler outlet nitrogen and is sampled, when sampling is special It is closed with the valve that sampler is connect with external circulation line, reactor content is unaffected.
A kind of reaction kettle on-line period device (application number: 201220070920.7), including reacts as has been publicly again Kettle, the side wall of the reaction kettle are connected with probe tube, and the sample tap of the probe tube is located above the feed inlet of reaction kettle to incite somebody to action For back flow of sample into reaction kettle, the probe tube is connected with the driving mechanism that driving sample flows out sample tap from reaction kettle.Institute Stating driving mechanism is air compressor, and the compressed air that the air compressor generates blows out sample out of probe tube.
Above-mentioned two pieces patent formula is provided with sampler, but according to plan content it is found that do not provide how It is required further improvement for this problem convenient for placing the related content of detection instrument meter.
Utility model content
1. utility model technical problems to be solved
The purpose of the utility model is to overcome the deficiencies that easy-offtaking detection is not counted when sample detection in the prior art, provide Articles holding table is arranged in a kind of reaction tower with articles holding table, this programme at the top of reaction tower, can be used for placing some detections meters, takes With conveniently, it is convenient for sample detection.
2. technical solution
In order to achieve the above objectives, technical solution provided by the utility model are as follows:
A kind of reaction tower with articles holding table of the utility model, including reaction tower ontology, sampler and articles holding table, take Sampling device is arranged in reaction tower bodies top;The articles holding table includes pedestal and glove pipe, is fixed at least two on the pedestal Glove pipe;Pedestal is removably mounted at reaction tower bodies top.
Further, the glove pipe has 3.High settings such as the glove pipe or there are differences in height.
Further, the pedestal bottom is concave arc, or is embedded with balance weight in pedestal bottom.
Further, the reaction tower ontology is fed by main feed pipe, the sampling ware bottom bucket bottom of the sampler Coaxial inner sleeve is installed, the shunting sampling pipe drawn on main feed pipe is connected to inner sleeve lower end, ware bottom bucket side wall of sampling Bottom end is connected with sampling drainage conduit, for material to be discharged into reaction tower ontology;The shunting sampling pipe and sampling drainage conduit are all provided with It is equipped with control valve.
Further, it is provided with top cover in the sampling ware bottom bucket, the top cover and sampling ware bottom bucket cooperation.
Further, the inner sleeve upper end protrudes from sampling ware bottom bucket upper surface, and sampling ware bottom bucket upper end is connected with The length of bright sleeve, the transparent sleeve is greater than inner sleeve protrusion length.
Further, top cover is combined on the transparent sleeve.
Further, it is provided on the upside of the top cover and mentions handle, it is plate or annular that this, which mentions handle,.
Further, sampling ware bottom bucket bottom is provided with bracket, and ware bottom bucket of sampling is fixed on reaction by the bracket On tower ontology.
3. beneficial effect
Using technical solution provided by the utility model, compared with prior art, have the following beneficial effects:
(1) a kind of reaction tower with articles holding table of the utility model, articles holding table include pedestal and glove pipe, the pedestal On be fixed at least two glove pipe;Pedestal is removably mounted at reaction tower bodies top, and reaction is placed or be mounted on to articles holding table Tower bodies top, when detection, can directly take, easy to use, avoid the need for carrying at any time, fall the problems such as damage.
(2) a kind of reaction tower with articles holding table of the utility model, the end of main feed pipe is connected to reaction tower ontology Feed inlet, be connected sampling pipe is shunted with main feed pipe, shunt the sampling pipe other end and be connected to inner sleeve bottom end, sampling ware bottom Bucket is connected to by sampling drainage conduit with reaction tower ontology with the annular chamber between inner sleeve, and when sampling Detection, opening first is controlled Then valve can use thermometer, densimeter etc. and detect to material in annular chamber;After detection, the second control is opened Valve, sample ware bottom bucket in material be flowed into reaction tower again, on-line checking can be realized, and be avoided that material waste.
(3) a kind of reaction tower with articles holding table of the utility model is connected with transparent sleeve in sampling ware bottom bucket upper end, The length of the transparent sleeve is greater than inner sleeve protrusion length.Transparent sleeve can regard the extended segment of sampling ware bottom bucket as, Prevent material from splashing outward.Top cover can be cooperated on transparent sleeve, under the structure, even if not removing top cover, can also be observed Charging situation in ware bottom bucket of sampling.
(4) a kind of reaction tower with articles holding table of the utility model, sample ware bottom bucket on be provided with top cover, the top cover with Ware bottom bucket of sampling cooperation;If external dust can drop into sampling ware bottom bucket without top cover, then after next time detects use, It has some of the contaminants to enter in material, influences product quality.
Detailed description of the invention
Fig. 1 is the Structural assignments schematic diagram of sampler on reaction tower;
Structural schematic diagram when Fig. 2 is the high settings such as glove pipe;
Fig. 3 is the glove pipe structural schematic diagram with difference in height;
Fig. 4 is the structural schematic diagram of sampler;
Fig. 5 is the structural schematic diagram of nut cap.
Label declaration in schematic diagram: 111, ware bottom bucket of sampling;112, transparent sleeve;113, top cover;121, sampling is shunted Pipe;122, the first control valve;123, inner sleeve;131, sampling drainage conduit;132, the second control valve;201, reaction tower ontology; 202, feed inlet;203, main feed pipe;204, nut cap;301, pedestal;302, glove pipe.
Specific embodiment
For the content for further appreciating that the utility model, the utility model is described in detail in conjunction with the accompanying drawings and embodiments.
Embodiment 1
In conjunction with Fig. 1, a kind of reaction tower with articles holding table of the present embodiment, including reaction tower ontology 201, sampler and Articles holding table, sampler setting is at 201 top of reaction tower ontology.Sampler is mainly used for charging either reaction tower ontology Material in 201 is detected, and after sampler takes out material, be can use thermometer detection temperature, be can use densimeter Specific gravity is detected, can use densitometer detection material density.
Since reaction tower generally has certain altitude, need to borrow ladder either travelling platform to facilitate operator to stand It is vertical to execute various operations.If operator carries detection every time, meter is detected, and is not easy to real-time detection needs;If will inspection It surveys meter to be placed on reaction tower ontology, is easy to fall damage.
For this problem, articles holding table set by the present embodiment includes pedestal 301 and glove pipe 302, is fixed on pedestal 301 There are 2 glove pipes 302;Pedestal 301 plays firm effect, and pedestal 301 is removably mounted at 201 top of reaction tower ontology.
Pedestal 301 primarily serves firm effect, can be rectangular or round.This implementation according to the needs of use, using circle Structure.In order to more firm, 301 bottom of pedestal is concave arc structure, i.e. the bottom of pedestal 301 is recessed inwardly, its surrounding when placement With reaction tower body contacts, center of gravity concentrates on middle part, more firm.
Glove pipe 302 is tubular structure, and middle part is cavity, can be used for placing various detection meters.Used 2 glove pipes The high settings such as 302, as shown in Figure 2.The top of reaction tower ontology 201 is placed or be mounted on to articles holding table, when detection can directly take With, it is easy to use, it avoids the need for carrying at any time, fall the problems such as damage.
Embodiment 2
A kind of reaction tower with articles holding table of the present embodiment, basic system is same as Example 1, and difference exists In: in conjunction with Fig. 3, there are 3 glove pipes 302 in the present embodiment, and have certain difference in height between glove pipe 302, according to different inspections The length of meter is surveyed, the property of can choose is placed, within easy reach.
It is possible to further which in 301 bottom mosaic equilibrium block of pedestal, balance weight density is greater than the density of material of pedestal 301, Balance weight can play stabilization.Further, it is also possible to consolidate pedestal 301 in the way of clamping, grafting etc..
Embodiment 3
A kind of reaction tower with articles holding table of the present embodiment, basic system is same as Example 2, and difference exists In: the feed inlet of reaction tower ontology 201 is connect with main feed pipe 203, defeated into reaction tower ontology 201 by main feed pipe 203 Send material.Sampling ware bottom bucket 111 in sampler can be cylinder-like structure, and sampling 111 bottom of ware bottom bucket is vertically installed with Inner sleeve 123, inner sleeve 123 can be set in the center of sampling ware bottom bucket 111.In the mounting direction, due to inner sleeve 123 perpendicular to sampling 111 bottom of ware bottom bucket, could be aware that inner sleeve 123 and sampling ware bottom bucket 111 are installed in the same direction, main feed pipe The 203 shunting sampling pipes 121 drawn are connected to 123 bottom of inner sleeve.The vertical of meaning is more hanging down on pointing the direction Directly, 111 bottom of representative sample ware bottom bucket is not necessary for planar structure.
It can be understood as inner sleeve 123 in above structure and shunt sampling pipe 121 to be two-part structure, be connected by auxiliary Or the modes such as welding link together.The structure, which can also be, is inserted into sampling ware bottom bucket 111 for a shunting sampling pipe 121 In, Seal treatment then is carried out to sampling 111 bottom of ware bottom bucket and is obtained, there is no limit for specific type of attachment.
Sampling 111 bottom end side wall of ware bottom bucket is connected with sampling drainage conduit 131, sample 131 other end of drainage conduit and reaction tower Ontology 201 is connected to, and the material overflowed from inner sleeve 123 enters in sampling ware bottom bucket 111, and can be from sampling discharge It is discharged in pipe 131.Control valve, material in convenience sampling detection are provided with shunting sampling pipe 121 and sampling drainage conduit 131 Control.
Specifically, in conjunction with Fig. 4, such as the charging of reaction tower ontology 201 is detected, reaction tower ontology 201 passes through master Feed pipe 203 is fed.In use, the device is in parallel with feed pipe, i.e., shunting sampling pipe 121 is in parallel with main feed pipe 203, main The end of feed pipe 203 is connected to the feed inlet 202 on 201 cover board of reaction tower ontology.Sampling drainage conduit in sampler 131 discharge gate is similarly connected to feed inlet 202.
When starting sampling, the first control valve 122 shunted on sampling pipe 121 is opened, material is flowed into pumping from inner sleeve 123 In sample ware bottom bucket 111, the first control valve 122 is closed, the progress such as thermometer, densimeter then can be taken from glove pipe 302 Detection meter after detection, is put into glove pipe 302, opens the second control valve 132, the material in ware bottom bucket 111 of sampling by detection It is flowed into reaction tower ontology 201 again, detection meter need not be carried, while avoid the problem of falling.
Embodiment 4
A kind of reaction tower with articles holding table of the present embodiment, basic system is same as Example 3, and difference exists In: it is provided with top cover 113 in sampling ware bottom bucket 111, the top cover 113 and sampling ware bottom bucket 111 cooperate.
If external dust can drop into sampling ware bottom bucket 111 without top cover 113, then after next time detects use, meeting There are some of the contaminants to enter in material, influences product quality.
It can be arranged on the upside of top cover 113 and mention handle, it is plate or annular that this, which mentions handle, convenient for the pick-and-place of top cover 113.Due to interior Casing 123 protrudes from sampling 111 upper surface of ware bottom bucket, therefore top cover 113 has side wall, side wall and sampling ware in the present embodiment Bottom bucket 111 cooperates, and top cover 113 can cover inner sleeve 123.
Embodiment 5
A kind of reaction tower with articles holding table of the present embodiment, basic system is same as Example 4, and difference exists In: the upper end of the present embodiment inner sleeve 123 protrudes from sampling 111 upper surface of ware bottom bucket, is connected in sampling 111 upper end of ware bottom bucket The length of transparent sleeve 112, the transparent sleeve 112 is greater than 123 protrusion length of inner sleeve.
Transparent sleeve 112 can regard the extended segment of sampling ware bottom bucket 111 as, prevent material from splashing outward.Further, It can cooperate top cover 113 on transparent sleeve 112, under the structure, even if not removing top cover 113, can also observe sampling ware bottom Charging situation in bucket 111.
Further, the side wall of 112 upper end of transparent sleeve tilts outward, convenient for placing detection meter, while facilitating top cover 113 lids are closed onto transparent sleeve 112.
Embodiment 6
A kind of reaction tower with articles holding table of the present embodiment, basic system is same as Example 5, and difference exists In: 111 bottom of sampling ware bottom bucket is provided with bracket, is fixed on reaction tower by the bracket.Bracket can be cylinder knot Structure is also possible to be made of multiple stabilizer blades.Shunting sampling pipe 121 and sampling drainage conduit 131 is four fluorine tube, can be corrosion-resistant.
Embodiment 7
A kind of reaction tower with articles holding table of the present embodiment, basic system is same as Example 6, and difference exists In: in conjunction with Fig. 5, nut cap 204 is stamped in the opening on 201 top of reaction tower ontology, nut cap 204 is cylindrical structure open at one end, Notch is provided in the cylinder side wall.
It, will also be using detector to inside other than the inspections such as feeding temperature and specific gravity when carrying out sodium sulfonate production Material is detected, and then needs circuit of arranging on reaction tower ontology, is that reaction tower ontology is put into from top mostly together, such as Fruit be using locking device, when detection practical inconvenience, if external contaminants is easily accessible shadow in tower body without blocking Ring product quality.And set nut cap 204 can cover wiring mouth just, the notch of nut cap can not influence route of arranging, real It is preferable with effect.
Schematically the utility model and embodiments thereof are described above, description is not limiting, attached drawing Shown in be also one of the embodiments of the present invention, actual structure is not limited to this.So if this field Those of ordinary skill enlightened by it, without deviating from the purpose of the present invention, not inventively design Frame mode similar with the technical solution and embodiment, all should belong to the protection range of the utility model.

Claims (10)

1. a kind of reaction tower with articles holding table, it is characterised in that: including reaction tower ontology (201), sampler and articles holding table, Sampler setting is at the top of reaction tower ontology (201);The articles holding table includes pedestal (301) and glove pipe (302), and described At least two glove pipe (302) is fixed on seat (301);Pedestal (301) is removably mounted at the top of reaction tower ontology (201).
2. a kind of reaction tower with articles holding table according to claim 1, it is characterised in that: the glove pipe (302) has 3 It is a.
3. a kind of reaction tower with articles holding table according to claim 1, it is characterised in that: described glove pipe (302) etc. High setting or there are differences in height.
4. a kind of reaction tower with articles holding table according to claim 1, it is characterised in that: pedestal (301) bottom For concave arc, or in pedestal (301) bottom it is embedded with balance weight.
5. a kind of reaction tower with articles holding table according to claim 1, it is characterised in that: the reaction tower ontology (201) it is fed by main feed pipe (203), sampling ware bottom bucket (111) bottom of the sampler is equipped with coaxial inner sleeve It manages (123), the shunting sampling pipe (121) drawn on main feed pipe (203) is connected to inner sleeve (123) lower end, ware bottom bucket of sampling (111) side wall bottom end is connected with sampling drainage conduit (131), for material to be discharged into reaction tower ontology (201);The shunting sampling Pipe (121) and sampling drainage conduit (131) are provided with control valve.
6. a kind of reaction tower with articles holding table according to claim 5, it is characterised in that: the sampling ware bottom bucket (111) top cover (113) are provided on, the top cover (113) and sampling ware bottom bucket (111) cooperation.
7. a kind of reaction tower with articles holding table according to claim 5, it is characterised in that: on the inner sleeve (123) Distal process is connected with transparent sleeve (112), the transparent sheath for sampling ware bottom bucket (111) upper surface, sampling ware bottom bucket (111) upper end The length of cylinder (112) is greater than inner sleeve (123) protrusion length.
8. a kind of reaction tower with articles holding table according to claim 7, it is characterised in that: the transparent sleeve (112) On be combined with top cover (113).
9. a kind of reaction tower with articles holding table according to claim 6 or 8, it is characterised in that: on the top cover (113) Side, which is provided with, mentions handle, and it is plate or annular that this, which mentions handle,.
10. a kind of reaction tower with articles holding table according to claim 5, it is characterised in that: the sampling ware bottom bucket (111) bottom is provided with bracket, and sampling ware bottom bucket (111) is fixed on reaction tower ontology (201) by the bracket.
CN201820392667.4U 2018-03-22 2018-03-22 A kind of reaction tower with articles holding table Expired - Fee Related CN208275382U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820392667.4U CN208275382U (en) 2018-03-22 2018-03-22 A kind of reaction tower with articles holding table

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820392667.4U CN208275382U (en) 2018-03-22 2018-03-22 A kind of reaction tower with articles holding table

Publications (1)

Publication Number Publication Date
CN208275382U true CN208275382U (en) 2018-12-25

Family

ID=64749846

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820392667.4U Expired - Fee Related CN208275382U (en) 2018-03-22 2018-03-22 A kind of reaction tower with articles holding table

Country Status (1)

Country Link
CN (1) CN208275382U (en)

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20181225

Termination date: 20210322

CF01 Termination of patent right due to non-payment of annual fee