CN208171630U - A kind of vacuum sampling device - Google Patents
A kind of vacuum sampling device Download PDFInfo
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- CN208171630U CN208171630U CN201820917844.6U CN201820917844U CN208171630U CN 208171630 U CN208171630 U CN 208171630U CN 201820917844 U CN201820917844 U CN 201820917844U CN 208171630 U CN208171630 U CN 208171630U
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Abstract
The utility model discloses a kind of vacuum sampling devices, it is characterized in that, it includes the vacuum lead, sampling container, vacuum generator connecting with reaction kettle, sampling pipe is connected between sampling container and vacuum lead, sampling pipe is provided at least two-stage ball valve, to increase sample rate.The utility model structure is simple, and use is easy to control.
Description
Technical field
The utility model relates to material production technical fields, more particularly to a kind of vacuum in plastics-production
Sampler.
Background technique
Reaction kettle is comprehensive reaction vessel, the design according to reaction condition to reaction kettle structure function and configuration attachment.Extensively
It is general be applied to petroleum, chemical industry, rubber, pesticide, dyestuff, medicine, food, for complete vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization,
Pressure vessel of the technical process such as condensation, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.；Material generally have carbon manganese steel,
Stainless steel, zirconium, Ni-based (Kazakhstan, Monel, inconel) alloy and other composite materials.It is equal from charging-reaction-discharging of beginning
Pre-set reaction step can be completed with higher the degree of automation, to the temperature in reaction process, pressure, mechanics control
The important parameters such as system (stirring, air blast etc.), reactant/product concentration carry out stringent regulation, and structure is generally by autoclave body, transmission
Device, agitating device, heating device, cooling device, sealing device composition.The response situation of material is to need to pass through vacuum sample
Device sampling monitoring, but currently, the device has that sampling efficiency is not high, need to be further increased.
Summary of the invention
The purpose of this utility model be exactly in order to solve the deficiency of the prior art and a kind of structure for providing is simple, manipulation side
Just vacuum sampling device.
The utility model is to realize above-mentioned purpose using following technical solution：A kind of vacuum sampling device, it is special
Sign is that it includes the vacuum lead, sampling container, vacuum generator connecting with reaction kettle, sampling container and vacuum-pumping tube
Sampling pipe is connected between road, sampling pipe is provided at least two-stage ball valve, to increase sample rate.
As a further illustration of the above scheme, the vacuum lead is provided with nitrogen inlet, on nitrogen inlet
It is provided with valve.
Further, reaction kettle includes autoclave body and the rabbling mechanism being arranged inside, and the side of autoclave body is provided at least two groups
Hollow clamping sleeve is filled with conduction oil, the hollow folder of at least one group at least two groups hollow clamping sleeve at least one group hollow clamping sleeve
Coolant liquid is filled in set, the upper and lower side for filling the hollow clamping sleeve of conduction oil is respectively arranged with conduction oil import and export, filling cooling
The upper and lower side of the hollow clamping sleeve of liquid is respectively arranged with coolant liquid import and export；At least two groups liquid coil pipe is provided in the middle part of autoclave body,
Conduction oil is filled at least two groups liquid coil pipe at least one group liquid coil pipe, is filled at least one group liquid coil pipe
Coolant liquid, the upper and lower side of autoclave body is respectively arranged with entery and delivery port corresponding with liquid coil pipe, so that the inside and outside of autoclave body can be simultaneously
Heating cools down simultaneously.
Further, rabbling mechanism includes electric machine, stands to being arranged in the intracorporal stirring rod of kettle, and stirring rod is located at liquid
The top of autoclave body, connection driving stirring rod is arranged in the middle part of coil pipe, electric machine.
Preferably, two groups of hollow clamping sleeves are arranged in the side of the autoclave body, wherein conduction oil is filled in one group of hollow clamping sleeve,
Coolant liquid is filled in another group of hollow clamping sleeve.
Preferably, two groups of liquid coil pipes are arranged in the middle part of the autoclave body, wherein conduction oil is filled in one group of liquid coil pipe,
Coolant liquid is filled in another group of liquid coil pipe.
The utility model is using the attainable beneficial effect of above-mentioned technical solution institute：
The utility model is used and is mainly made of the vacuum lead, sampling container, vacuum generator connecting with reaction kettle
Vacuum sampling device, vacuum lead is provided at least two-stage ball valve, and to increase sample rate, structure is simple and effective.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model.
Description of symbols：1, vacuum lead 2, sampling container 3, vacuum generator 4, sampling pipe 5, ball valve
6, rabbling mechanism 7, hollow clamping sleeve.
Specific embodiment
The technical program is explained in detail below in conjunction with specific embodiment.
As shown in Figure 1, the utility model is a kind of vacuum sampling device, it includes the vacuum lead connecting with reaction kettle
1, sampling container 2, vacuum generator 3, it includes the vacuum lead 1 connecting with reaction kettle, sampling container 2, vacuum generator
3, sampling pipe 4 is connected between sampling container and vacuum lead, sampling pipe is provided at least two-stage ball valve 5, to increase
Sample rate.Vacuum lead is provided with nitrogen inlet, is provided with valve on nitrogen inlet.Reaction kettle include autoclave body and its
The rabbling mechanism 6 of interior setting, the side of autoclave body are provided at least two groups hollow clamping sleeve 7, at least two groups hollow clamping sleeve at least
It is filled with conduction oil in one group of hollow clamping sleeve, is filled with coolant liquid at least one group hollow clamping sleeve, fills the hollow of conduction oil
The upper and lower side of collet is respectively arranged with conduction oil import and export, fill the hollow clamping sleeve of coolant liquid upper and lower side be respectively arranged with it is cold
But liquid import and export；At least two groups liquid coil pipe, at least one group liquid at least two groups liquid coil pipe are provided in the middle part of autoclave body
Be filled with conduction oil in coil pipe, be filled with coolant liquid at least one group liquid coil pipe, the upper and lower side of autoclave body be respectively arranged with
The corresponding entery and delivery port of liquid coil pipe, so that the inside and outside of autoclave body can heat up while cool down simultaneously.In the present embodiment, the kettle
Two groups of hollow clamping sleeves are arranged in the side of body, wherein conduction oil is filled in one group of hollow clamping sleeve, filling in another group of hollow clamping sleeve
There is coolant liquid.Two groups of liquid coil pipes are arranged in the middle part of autoclave body, wherein being filled with conduction oil, another group of liquid in one group of liquid coil pipe
Coolant liquid is filled in coil pipe.
Further, rabbling mechanism 6 includes electric machine, stands to being arranged in the intracorporal stirring rod of kettle, and stirring rod is located at liquid
The top of autoclave body, connection driving stirring rod is arranged in the middle part of body disc pipe, electric machine.
The utility model compared with prior art, using mainly by connect with reaction kettle vacuum lead, sampling container,
The vacuum sampling device that vacuum generator is constituted, vacuum lead is provided at least two-stage ball valve, to increase sample rate, structure
It is simple and effective.
Above-described is only preferred embodiments of the present invention, it is noted that for the ordinary skill of this field
For personnel, without departing from the concept of the present invention, various modifications and improvements can be made, these all belong to
In the protection scope of the utility model.
Claims (6)
1. a kind of vacuum sampling device, which is characterized in that it includes the vacuum lead connecting with reaction kettle, sampling container, true
Empty generator, is connected with sampling pipe between sampling container and vacuum lead, sampling pipe is provided at least two-stage ball valve.
2. a kind of vacuum sampling device according to claim 1, which is characterized in that the vacuum lead is provided with nitrogen
Input port is provided with valve on nitrogen inlet.
3. a kind of vacuum sampling device according to claim 1, which is characterized in that reaction kettle includes autoclave body and is arranged inside
Rabbling mechanism, the side of autoclave body is provided at least two groups hollow clamping sleeve, and at least one group is hollow at least two groups hollow clamping sleeve
It is filled with conduction oil in collet, is filled with coolant liquid at least one group hollow clamping sleeve, fills the upper of the hollow clamping sleeve of conduction oil
Lower end is respectively arranged with conduction oil import and export, fill the hollow clamping sleeve of coolant liquid upper and lower side be respectively arranged with coolant liquid into and out of
Mouthful；It is provided at least two groups liquid coil pipe in the middle part of autoclave body, is filled out at least one group liquid coil pipe at least two groups liquid coil pipe
Filled with conduction oil, it is filled with coolant liquid at least one group liquid coil pipe, the upper and lower side of autoclave body is respectively arranged with and liquid coil pipe
Corresponding entery and delivery port.
4. a kind of vacuum sampling device according to claim 3, which is characterized in that rabbling mechanism includes electric machine, stands
To being arranged in the intracorporal stirring rod of kettle, stirring rod is located at the middle part of liquid coil pipe, and the top of autoclave body is arranged in electric machine, connection
Drive stirring rod.
5. a kind of vacuum sampling device according to claim 3, which is characterized in that two groups of skies are arranged in the side of the autoclave body
Heart collet is filled with coolant liquid wherein being filled with conduction oil in one group of hollow clamping sleeve in another group of hollow clamping sleeve.
6. a kind of vacuum sampling device according to claim 3, which is characterized in that two groups of liquid are arranged in the middle part of the autoclave body
Body disc pipe is filled with coolant liquid wherein being filled with conduction oil in one group of liquid coil pipe in another group of liquid coil pipe.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820917844.6U CN208171630U (en) | 2018-06-13 | 2018-06-13 | A kind of vacuum sampling device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820917844.6U CN208171630U (en) | 2018-06-13 | 2018-06-13 | A kind of vacuum sampling device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208171630U true CN208171630U (en) | 2018-11-30 |
Family
ID=64363663
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820917844.6U Active CN208171630U (en) | 2018-06-13 | 2018-06-13 | A kind of vacuum sampling device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208171630U (en) |
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2018
- 2018-06-13 CN CN201820917844.6U patent/CN208171630U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A vacuum sampling device Effective date of registration: 20210312 Granted publication date: 20181130 Pledgee: Guangdong Nanhai rural commercial bank Limited by Share Ltd. Li Shui branch Pledgor: FOSHAN HUABORUN MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2021980001605 |
|
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: 528000 No.29, area a, datangyuan, central science and Technology Industrial Zone, Sanshui District, Foshan City, Guangdong Province (self number: F4, F5) Patentee after: Guangdong Huaborun Material Technology Co.,Ltd. Address before: 528143 No. 29, Zone A, Datangyuan, Central Science and Technology Industrial Zone, Sanshui District, Foshan City, Guangdong Province (self numbers: F4, F5) Patentee before: FOSHAN HUABORUN MATERIAL TECHNOLOGY Co.,Ltd. |