CN208161578U - A kind of continous way synchronization planet mechanico-chemical reaction system - Google Patents
A kind of continous way synchronization planet mechanico-chemical reaction system Download PDFInfo
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- CN208161578U CN208161578U CN201820364263.4U CN201820364263U CN208161578U CN 208161578 U CN208161578 U CN 208161578U CN 201820364263 U CN201820364263 U CN 201820364263U CN 208161578 U CN208161578 U CN 208161578U
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Abstract
A kind of synchronous planet mechanico-chemical reaction system of continous way of the utility model includes reactor, cyclone separator, blower, condenser, dissolution kettle, solvent recovery kettle, crystallization kettle, first filter, the second filter, liquid pump, helicoidal pump, air pump.The tiny structure system that a kind of synchronous planet mechanico-chemical reaction system of continous way of the utility model is made up of blower and cyclone separator, realizes the continuous extraction of reactor discharging, while avoiding the leakage of material；The separation system being made up of dissolution kettle, solvent recovery kettle, crystallinity kettle, first filter and the second filter, realizes the separation of reactant；Temperature and pressure monitoring probe is set on the reaction sphere mill chamber of reactor, realizes the detection to reaction process temperature, pressure；Collet is set in reaction chamber, realizes and the temperature of reaction process is controlled.A kind of synchronous planet mechanico-chemical reaction system of continous way of the utility model is able to achieve the continuous production of mechanochemical process, has preferable commercial application prospect.
Description
Technical field
The invention belongs to mechanochemistry field more particularly to a kind of synchronous planet mechanico-chemical reaction systems of continous way.
Background technique
Mechanochemistry（Mechanochemical）It is the combination of machining and chemical reaction in molecular level, including machine
Tool crushing, the chemical reaction under action of mechanical pressure, friction, mechanical degradation polymer, void effect, ultrasonic wave physical chemistry and
Active force etc. during molecule.Mechanochemistry can be regarded as the cross discipline of a chemical industry and mechanical industry.In recent years,
The mechanico-chemical reaction technology green pharmaceutical technology emerging as one kind of interdisciplinary field, promptly emerges and develops, obtain
The concern of lot of domestic and foreign scholar is arrived.Mechanico-chemical reaction process has substrate contact surface big, mass-transfer efficiency height, reaction rate
Fastly, the good feature of selectivity is not only able to reduce the use of the unfriendly solvent/reagent of environment, additionally it is possible to effectively improve reaction
Energy efficiency and product yield, or even promote the reaction being difficult to happen in solution（Such as C-Cl bond activation, the covalent skeleton activation of non-carbon
Deng）Efficiently carry out, thus development prospect is wide.So far, it has successfully been realized using mechanico-chemical reaction technology a series of important
Solvent-free drug synthetic reaction, such as metal catalytic coupling, cyclization, asymmetric addition etc. and flavones, polysaccharide, triterpenic acid, biology
The degradation of the vegetable materials such as the extraction of the multiclass active ingredient of autonomic drug such as alkali and lignin, cellulose.These successful stories are equal
It is related between different material phase（Such as solid-solid, solid-liquid）Chemical reaction, and show conventional process mode can not reach it is excellent
More property.
Realize that the reaction unit of mechanochemistry is known as mechanico-chemical reaction device, the most commonly used is ball mills, including row
Celestial body grinding machine, vibration ball mill and tumbling ball mill etc..Planetary ball mill energy intensity is high, and the system object of application is more, however
Planetary ball mill is since grinding chamber is around central axis high speed rotation, and itself is also being rotated, exist how the difficulty of continuous feeding and discharging,
It is typically only capable to grasp using interval, the utilization which has limited it in large-scale production is such as able to achieve the continuous metaplasia of planetary ball mill
It produces, bottleneck of the mechanochemical reaction in scale, industrialization are used can be broken through.
Patent（201310237964.3 a kind of hypergravity microchannel reactor）Use for reference high speed adverse current chromatogram（HSCCC）'s
Special construction realizes pipeline unwinding when synchronous planetary motion, and pipeline is avoided to twist off, thus realizes material of being back to back.Patent
（201810152756.6 a kind of synchronous planet mechanico-chemical reaction device of continous way）Use for reference patent（201310237964.3 a kind of
Hypergravity microchannel reactor）Imagination realize the serialization of planetary mechanico-chemical reaction device, but do not disclose whole system.
Summary of the invention
To solve deficiency and defect existing for conventional method, the present invention is in patent（201810152756.6 a kind of continous way
Synchronous planet mechanico-chemical reaction device）On the basis of basic conception, a kind of continous way synchronization planet mechanico-chemical reaction system is invented
System.
The present invention solves technical solution used by above-mentioned technical problem, and a kind of continous way synchronization planet mechanochemistry is anti-
Answer system include reactor, cyclone separator, blower, condenser, dissolution kettle, solvent recovery kettle, crystallization kettle, first filter,
Second filter, liquid pump, helicoidal pump, air pump；The reactor is equipped with tube bank import and product exit；The cyclone separator is set
There are import, solid outlet, gas vent；The dissolution kettle is equipped with feed inlet, solvent inlet and discharge port；The first filter
Respective import, solid outlet and liquid outlet are equipped with the second filter；The solvent recovery kettle is equipped with import, gas goes out
Mouth, liquid outlet；The condenser is shell-and-tube heat exchanger, is equipped with tube side import and tube side exports；The crystallization kettle is equipped with original
Liquid inlet and outlet is applied in material import；The outlet of the liquid pump is connected to one end of liquid delivery tube, liquid delivery tube it is another
End penetrates tube bank import；The outlet of the helicoidal pump is connected to one end of powder conveying pipe, and the other end of powder conveying pipe penetrates
Restrain import；The outlet of the air pump is connected to one end of air shooter, and the other end of air shooter penetrates tube bank import；
The product exit of the reactor and the inlet communication of cyclone separator, the gas vent of the cyclone separator and blower into
Mouth connection；The solid outlet of the cyclone separator is connected to the feed inlet of the dissolution kettle, the discharge port of dissolution kettle and first
The inlet communication of filter；The liquid outlet of the first filter and the inlet communication of solvent recovery kettle；The solvent recovery
The tube side outlet of the gas vent of kettle and the tube side inlet communication of condenser, condenser is connected to the solvent inlet of dissolution kettle；Institute
The liquid outlet for stating solvent recovery kettle is connected to the material inlet of crystallization kettle；The outlet of the crystallization kettle and second filter into
Mouth connection；The liquid outlet of second filter and crystallization kettle apply liquid inlet communication；
As an improvement, the reactor is made of main body and frame；The structure of the main body is as follows：Discharge nozzle（11）It is one
Section right-angle elbow pipe, one end are vertically arranged；Central shaft tube（1）Also vertically fixed and from discharge nozzle（11）It is vertically arranged in one end
The heart passes through and runs through discharge nozzle（11）；The discharge nozzle（11）The other end be reactor product exit；Taper rotating drum
（9）Conehead position and casing（12）Connection, belt pulley（13）It is fixed on casing（12）On, taper rotating drum（9）Circular bottom surface
With rotating top plate（3）Pass through vertical columns（8）It is fixed, so that taper rotating drum（9）, casing（12）, belt pulley（13）, rotation
Turn top plate（3）And vertical columns（8）Form a rigid rotating body；During the rigid rotating body is mounted on by bearing support
Central spindle tube（1）On；Reaction sphere mill chamber（2）And counterweight（7）Pass through bearing and central shaft tube（1）Axisymmetricly it is mounted on taper rotation
Turn chamber（9）Bottom surface and rotating top plate（3）Between, counterweight（7）Play balanced action；Reaction sphere mill chamber（2）And counterweight（7）It is rotating
Top plate（3）Above section Gu Dingshezhi not a central gear（6）With a planetary gear（4）, close to taper rotating drum（9）
Bottom surface also respectively be fixedly installed a central gear（6）With a planetary gear（4）；Conveying tube bank（5）One end through anti-
Answer ball milling chamber（2）The planetary gear of upper end（4）With reaction sphere mill chamber（2）Inside connection, and and planetary gear（4）It is fixed；Conveying
Tube bank（5）The other end run through central shaft tube（1）The central gear of upper end（6）, central shaft tube is passed through afterwards（1）Inside is lower than out
Expects pipe（11）Position from central shaft tube（1）Side is pierced by, and conveys tube bank（5）With central gear（6）And central shaft tube（1）Gu
Fixed, this one end is the tube bank import of reactor；The discharge nozzle（11）Internal diameter is greater than taper rotating drum（9）Casing（12）'s
Outer diameter, thus casing（12）With stationary discharge nozzle（11）Between have certain annular space；Planetary gear（4）And central gear
（6）In the same size, variable-frequency motor is worked as in intermeshing in this way（10）Drive belt pulley（13）Make rigid rotating body around central shaft tube
（1）When rotation, reaction sphere mill chamber can be made（2）Around central shaft tube（1）Make the same direction, phase around central axis while revolution
With the rotation of angle, i.e., " synchronous planetary motion ", conveying is avoided to restrain（5）Winding fractures；The structure of the frame is as follows：Bottom plate
（14）, middle plate（15）And top plate（17）Pass through column（16）It is fixed as a frame；The central shaft tube of the main body（1）Support is simultaneously
It is fixed on bottom plate（14）On, rotating top plate（3）Pass through upper bearing (metal)（18）With top plate（17）Contact, taper rotating drum（9）Round bottom
Face passes through lower bearing（19）With middle plate（15）Contact.
It is further improved, the reaction sphere mill chamber（2）By circular cylindrical cavity（2-1）, conehead be equipped with inlet tube（2-4）It is upper
Conical head（2-2）Outlet is equipped with conehead（2-5）Inferior pyramidal end socket（2-3）It constitutes；The circular cylindrical cavity（2-1）Outside
Equipped with chuck layer（2-6）, inside it is equipped with 4 pieces of separation sieve plates（2-7）Separate the cavity into 5 Cavity units, on first chamber down
Body unit is distribution cavity（2-8）, the 2nd to 4 Cavity unit is reaction member（2-9）, the 5th Cavity unit is material collection chamber
（2-10）；Temp probe is equipped in the separation sieve plate（2-11）；Each reaction member（2-9）Side be equipped with pressure measuring chamber
（2-12）, pressure measuring chamber（2-12）Across chuck layer（2-6）Pass through 4 pores and reaction member（2-9）Inside connection, the reaction
Unit（2-9）It is provided with abrasive media ball（2-13）.
It improves again, the conveying tube bank（5）Inside be installed with liquid delivery tube, powder conveying pipe, gas conveying, chuck layer into
Pipe, chuck layer outlet pipe, temperature signal line, pressure signal line, such as same root " seven core conducting wires ".
Compared with the prior art, the advantages of the present invention are as follows：The tiny structure system being made up of blower and cyclone separator,
The continuous extraction of reactor discharging is realized, while avoiding the leakage of material；Pass through dissolution kettle, solvent recovery kettle, crystallinity
The separation system that kettle, first filter and the second filter are constituted, realizes the separation of reactant；In the reaction ball milling of reactor
Temperature and pressure monitoring probe is set on chamber, realizes the detection to reaction process temperature, pressure；In reaction chamber, collet is set,
It realizes and the temperature of reaction process is controlled.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of the synchronous planet mechanico-chemical reaction system of continous way of the invention.
Fig. 2 is the schematic perspective view of the main body of reactor of the invention.
Fig. 3 is the schematic perspective view of the frame of reactor of the invention.
Fig. 4 is the structural schematic diagram of the reaction sphere mill chamber of reactor of the invention.
Wherein：1 be center central siphon, 2 be reaction sphere mill chamber, 3 be rotating top plate, 4 be planetary gear, 5 be conveying tube bank, 6
It is counterweight for center gear, 7,8 be vertical columns, 9 be taper rotating drum, 10 be variable-frequency motor, 11 be discharge nozzle, 12 is set
Pipe, 13 be belt pulley, 14 be bottom plate, 15 be middle plate, 16 be column, 17 be top plate, 18 be upper bearing (metal), 19 be lower bearing, 2-1 is
Circular cylindrical cavity, 2-2 are upper conical end socket, 2-3 is inferior pyramidal end socket, 2-4 is inlet tube, 2-5 is outlet, 2-6 is collet
Layer, 2-7 are separation sieve plate, 2-8 is distribution cavity, 2-9 is reaction member, 2-10 is material collection chamber, 2-11 is temp probe, 2-
12 be pressure measuring chamber, 2-13 is abrasive media ball.
Specific embodiment
With reference to the accompanying drawing 1,2,3 and 4, by embodiment, present invention is further described in detail.
Embodiment 1
A kind of synchronous planet mechanico-chemical reaction system of continous way include reactor, cyclone separator, blower, condenser,
Dissolution kettle, solvent recovery kettle, crystallization kettle, first filter, the second filter, liquid pump, helicoidal pump, air pump；Reactor is by main body
It is constituted with frame；The structure of main body is as follows：Discharge nozzle（11）For one section of right-angle elbow pipe, one end is vertically arranged；Central shaft tube（1）
Also vertically fixed and from discharge nozzle（11）The center for being vertically arranged one end passes through and runs through discharge nozzle（11）；Discharge nozzle（11）It is another
One end is the product exit of reactor；Taper rotating drum（9）Conehead position and casing（12）Connection, belt pulley（13）It is fixed
In casing（12）On, taper rotating drum（9）Circular bottom surface and rotating top plate（3）Pass through vertical columns（8）It is fixed, so that cone
Shape rotating drum（9）, casing（12）, belt pulley（13）, rotating top plate（3）And vertical columns（8）Form a rigid rotating body；
Rigid rotating body is mounted on central shaft tube by bearing support（1）On；Reaction sphere mill chamber（2）And counterweight（7）Through bearing in
Central spindle tube（1）Axisymmetricly it is mounted on taper rotating drum（9）Bottom surface and rotating top plate（3）Between, counterweight（7）Balance is played to make
With；Reaction sphere mill chamber（2）And counterweight（7）In rotating top plate（3）Above section Gu Dingshezhi not a central gear（6）With one
Planetary gear（4）, close to taper rotating drum（9）Bottom surface also respectively be fixedly installed a central gear（6）With a planet
Gear（4）；Conveying tube bank（5）Inside it is installed with liquid delivery tube, powder conveying pipe, gas conveying, chuck layer inlet pipe, chuck layer go out
Pipe, temperature signal line, pressure signal line, such as same root " seven core conducting wires "；Conveying tube bank（5）One end run through reaction sphere mill chamber
（2）The planetary gear of upper end（4）With reaction sphere mill chamber（2）Inside connection, and and planetary gear（4）It is fixed；Conveying tube bank（5）
The other end run through central shaft tube（1）The central gear of upper end（6）, central shaft tube is passed through afterwards（1）Inside is being lower than discharge nozzle
（11）Position from central shaft tube（1）Side is pierced by, and conveys tube bank（5）With central gear（6）And central shaft tube（1）It is fixed,
This one end is the tube bank import of reactor；Discharge nozzle（11）Internal diameter is greater than taper rotating drum（9）Casing（12）Outer diameter, because
And casing（12）With stationary discharge nozzle（11）Between have certain annular space；Planetary gear（4）And central gear（6）Size
Unanimously, it is intermeshed, works as variable-frequency motor in this way（10）Drive belt pulley（13）Make rigid rotating body around central shaft tube（1）Rotation
When, reaction sphere mill chamber can be made（2）Around central shaft tube（1）Make the same direction, equal angular around central axis while revolution
Rotation i.e. " synchronous planetary motion " conveying is avoided to restrain（5）Winding fractures.The structure of frame is as follows：Bottom plate（14）, middle plate
（15）And top plate（17）Pass through column（16）It is fixed as a frame；The central shaft tube of the main body（1）It supports and is fixed on bottom
Plate（14）On, rotating top plate（3）Pass through upper bearing (metal)（18）With top plate（17）Contact, taper rotating drum（9）Circular bottom surface pass through under
Bearing（19）With middle plate（15）Contact.Reaction sphere mill chamber（2）By circular cylindrical cavity（2-1）, conehead be equipped with inlet tube（2-4）It is upper
Conical head（2-2）Outlet is equipped with conehead（2-5）Inferior pyramidal end socket（2-3）It constitutes；The circular cylindrical cavity（2-1）Outside
Equipped with chuck layer（2-6）, inside it is equipped with 4 pieces of separation sieve plates（2-7）Separate the cavity into 5 Cavity units, on first chamber down
Body unit is distribution cavity（2-8）, the 2nd to 4 Cavity unit is reaction member（2-9）, the 5th Cavity unit is material collection chamber
（2-10）；Temp probe is equipped in the separation sieve plate（2-11）；Each reaction member（2-9）Side be equipped with pressure measuring chamber（2-
12）, pressure measuring chamber（2-12）Across chuck layer（2-6）Pass through 4 pores and reaction member（2-9）Inside connection, the reaction are single
Member（2-9）It is provided with abrasive media ball（2-13）.
Cyclone separator is equipped with import, solid outlet, gas vent；Dissolution kettle is equipped with feed inlet, solvent inlet and discharging
Mouthful；First filter and the second filter are equipped with respective import, solid outlet and liquid outlet；Solvent recovery kettle be equipped with into
Mouth, gas vent, liquid outlet；Condenser is shell-and-tube heat exchanger, is equipped with tube side import and tube side exports；Crystallization kettle is equipped with original
Liquid inlet and outlet is applied in material import；The outlet of liquid pump is connected to one end of liquid delivery tube, and the other end of liquid delivery tube is worn
Enter to restrain import；The outlet of helicoidal pump is connected to one end of powder conveying pipe, and the other end of powder conveying pipe penetrates tube bank import；
The outlet of air pump is connected to one end of air shooter, and the other end of air shooter penetrates tube bank import；The product of reactor
The inlet communication of outlet and cyclone separator, the gas vent of cyclone separator and the inlet communication of blower；Cyclone separator
Solid outlet is connected to the feed inlet of the dissolution kettle, the discharge port of dissolution kettle and the inlet communication of first filter；First mistake
The liquid outlet of filter and the inlet communication of solvent recovery kettle；The tube side import of the gas vent and condenser of solvent recovery kettle connects
Logical, the tube side outlet of condenser is connected to the solvent inlet of dissolution kettle；The liquid outlet of solvent recovery kettle and the raw material of crystallization kettle
Inlet communication；The outlet of crystallization kettle and the inlet communication of the second filter；The liquid outlet of second filter and the set of crystallization kettle
With liquid inlet communication.
A kind of course of work of the synchronous planet mechanico-chemical reaction system of continous way of the invention：Liquid charging stock, solid are former
Material and gas raw material pass through liquid pump respectively, helicoidal pump passes through conveying tube bank（5）It is continuously conveyed to reaction sphere mill chamber（2）It is interior.Frequency conversion
Motor（10）Belt pulley is driven by belt（13）Make rigid rotating body around central shaft tube（1）Rotation makes reaction sphere mill chamber（2）?
Around central shaft tube（1）Make the rotation of the same direction, equal angular, i.e. " synchronization line luck while revolution around central axis
It is dynamic ", avoid conveying from restraining（5）Winding fractures.Into reaction sphere mill chamber（2）Material pass through distribution cavity（2-8）Into first
Reaction member（2-9）, abrasive media ball shears reactant by the effect of " synchronous planet " movement, rubbed, impacted, squeezed
Pressure is allowed to occur mechanico-chemical reaction, and by the effect of rolling of abrasive media ball by the material of the reaction member ground sieve plate into
Enter second reaction member（2-9）, pass through third reaction member again in this way（2-9）, reaction product enters material collection chamber（2-
10）, after fall into taper rotating drum（9）It is interior, then pass through taper rotating drum（9）Casing（12）With central shaft tube（1）Between ring
Gap goes cyclone separator to be separated, and solid and liquid enter dissolution kettle from the solid outlet of cyclone separator, and gas passes through wind
Machine discharge becomes tail gas；The solvent come from condenser, which enters dissolution kettle, dissolve to the next solid of cyclone separator and liquid
To solution, solution is discharged into first filter from the bottom of dissolution kettle, and filtered filtrate enters solvent recovery kettle, and filter cake is made
For waste residue discharge；Filtrate is concentrated in solvent recovery kettle vaporized in part, and steam enters condenser and is condensed into solvent, and concentrate enters
Crystallization kettle crystallisation by cooling obtains crystal solution, and crystal solution obtains product and mother liquor by the second filter, and mother liquor returns crystallization kettle.
Claims (4)
1. a kind of synchronous planet mechanico-chemical reaction system of continous way, it is characterised in that：The reaction system includes reactor, rotation
Wind separator, blower, condenser, dissolution kettle, solvent recovery kettle, crystallization kettle, first filter, the second filter, liquid pump, spiral
Pump, air pump；
The reactor is equipped with tube bank import and product exit；The cyclone separator goes out equipped with import, solid outlet, gas
Mouthful；The dissolution kettle is equipped with feed inlet, solvent inlet and discharge port；The first filter and the second filter are equipped with respectively
Import, solid outlet and liquid outlet；The solvent recovery kettle is equipped with import, gas vent, liquid outlet；The condenser
For shell-and-tube heat exchanger, it is equipped with tube side import and tube side exports；The crystallization kettle is equipped with material inlet, applies liquid import and go out
Mouthful；
The outlet of the liquid pump is connected to one end of liquid delivery tube, and the other end of liquid delivery tube penetrates tube bank import；It is described
The outlet of helicoidal pump is connected to one end of powder conveying pipe, and the other end of powder conveying pipe penetrates tube bank import；The air pump
Outlet is connected to one end of air shooter, and the other end of air shooter penetrates tube bank import；The product of the reactor goes out
The inlet communication of mouth and cyclone separator, the gas vent of the cyclone separator and the inlet communication of blower；The whirlwind point
It is connected to from the solid outlet of device with the feed inlet of the dissolution kettle, the discharge port of dissolution kettle and the inlet communication of first filter；
The liquid outlet of the first filter and the inlet communication of solvent recovery kettle；The gas vent of the solvent recovery kettle and condensation
The tube side outlet of the tube side inlet communication of device, condenser is connected to the solvent inlet of dissolution kettle；The liquid of the solvent recovery kettle
Outlet is connected to the material inlet of crystallization kettle；The outlet of the crystallization kettle and the inlet communication of the second filter；Second mistake
The liquid outlet of filter and crystallization kettle apply liquid inlet communication.
2. reaction system according to claim 1, it is characterised in that：The reactor is made of main body and frame；It is described
The structure of main body is as follows：Discharge nozzle（11）For one section of right-angle elbow pipe, one end is vertically arranged；Central shaft tube（1）Also vertical fixed
And from discharge nozzle（11）The center for being vertically arranged one end passes through and runs through discharge nozzle（11）；The discharge nozzle（11）The other end be
For the product exit of reactor；Taper rotating drum（9）Conehead position and casing（12）Connection, belt pulley（13）It is fixed on casing
（12）On, taper rotating drum（9）Circular bottom surface and rotating top plate（3）Pass through vertical columns（8）It is fixed, so that taper rotation
Chamber（9）, casing（12）, belt pulley（13）, rotating top plate（3）And vertical columns（8）Form a rigid rotating body；It is described rigid
Property rotary body is mounted on central shaft tube by bearing support（1）On；Reaction sphere mill chamber（2）And counterweight（7）Pass through bearing and center
Central siphon（1）Axisymmetricly it is mounted on taper rotating drum（9）Bottom surface and rotating top plate（3）Between, counterweight（7）Balance is played to make
With；Reaction sphere mill chamber（2）And counterweight（7）In rotating top plate（3）Above section Gu Dingshezhi not a central gear（6）With one
Planetary gear（4）, close to taper rotating drum（9）Bottom surface also respectively be fixedly installed a central gear（6）With a planet
Gear（4）；Conveying tube bank（5）One end run through reaction sphere mill chamber（2）The planetary gear of upper end（4）With reaction sphere mill chamber（2）It is interior
Portion's connection, and and planetary gear（4）It is fixed；Conveying tube bank（5）The other end run through central shaft tube（1）The central gear of upper end
（6）, central shaft tube is passed through afterwards（1）Inside is being lower than discharge nozzle（11）Position from central shaft tube（1）Side is pierced by, and delivery pipe
Beam（5）With central gear（6）And central shaft tube（1）Fixed, this one end is the tube bank import of reactor；The discharge nozzle（11）
Internal diameter is greater than taper rotating drum（9）Casing（12）Outer diameter, thus casing（12）With stationary discharge nozzle（11）Between
There is certain annular space；Planetary gear（4）And central gear（6）In the same size, variable-frequency motor is worked as in intermeshing in this way（10）It drives
Belt pulley（13）Make rigid rotating body around central shaft tube（1）When rotation, reaction sphere mill chamber can be made（2）Around central shaft tube（1）It is public
Make the rotation of the same direction, equal angular while turning around central axis, i.e. " synchronous planetary motion ", conveying is avoided to restrain
（5）Winding fractures；
The structure of the frame is as follows：Bottom plate（14）, middle plate（15）And top plate（17）Pass through column（16）It is fixed as a frame；
The central shaft tube of the main body（1）It supports and is fixed on bottom plate（14）On, rotating top plate（3）Pass through upper bearing (metal)（18）With top plate
（17）Contact, taper rotating drum（9）Circular bottom surface pass through lower bearing（19）With middle plate（15）Contact.
3. reaction system according to claim 2, it is characterised in that：The reaction sphere mill chamber（2）By circular cylindrical cavity（2-
1）, conehead be equipped with inlet tube（2-4）Upper conical end socket（2-2）Outlet is equipped with conehead（2-5）Inferior pyramidal end socket（2-3）
It constitutes；The circular cylindrical cavity（2-1）It is externally provided with chuck layer（2-6）, inside it is equipped with 4 pieces of separation sieve plates（2-7）Separate the cavity into 5
A Cavity unit, on down first Cavity unit be distribution cavity（2-8）, the 2nd to 4 Cavity unit is reaction member（2-9）,
5th Cavity unit is material collection chamber（2-10）；Temp probe is equipped in the separation sieve plate（2-11）；Each reaction
Unit（2-9）Side be equipped with pressure measuring chamber（2-12）, pressure measuring chamber（2-12）Across chuck layer（2-6）By 4 pores with react
Unit（2-9）Inside connection, the reaction member（2-9）It is provided with abrasive media ball（2-13）.
4. reaction system according to claim 2, it is characterised in that：The conveying tube bank（5）Inside be installed with liquid delivery tube,
Powder conveying pipe, gas conveying, chuck layer inlet pipe, chuck layer outlet pipe, temperature signal line, pressure signal line, such as same root " seven cores
Conducting wire ".
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820364263.4U CN208161578U (en) | 2018-03-18 | 2018-03-18 | A kind of continous way synchronization planet mechanico-chemical reaction system |
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| CN201820364263.4U CN208161578U (en) | 2018-03-18 | 2018-03-18 | A kind of continous way synchronization planet mechanico-chemical reaction system |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108295788A (en) * | 2018-03-18 | 2018-07-20 | 宁波工程学院 | A kind of continous way synchronization planet mechanico-chemical reaction system |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108295788A (en) * | 2018-03-18 | 2018-07-20 | 宁波工程学院 | A kind of continous way synchronization planet mechanico-chemical reaction system |
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