CN208145968U - A kind of turbulent device of organic silicon emulsion reaction - Google Patents
A kind of turbulent device of organic silicon emulsion reaction Download PDFInfo
- Publication number
- CN208145968U CN208145968U CN201820398173.7U CN201820398173U CN208145968U CN 208145968 U CN208145968 U CN 208145968U CN 201820398173 U CN201820398173 U CN 201820398173U CN 208145968 U CN208145968 U CN 208145968U
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- Prior art keywords
- turbulent
- thermowell
- main shaft
- blade
- stirring main
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 34
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 title claims abstract description 16
- 229910052710 silicon Inorganic materials 0.000 title claims abstract description 16
- 239000010703 silicon Substances 0.000 title claims abstract description 16
- 239000000839 emulsion Substances 0.000 title claims abstract description 15
- 238000003756 stirring Methods 0.000 claims abstract description 82
- 238000007790 scraping Methods 0.000 claims description 27
- 230000008878 coupling Effects 0.000 claims description 19
- 238000010168 coupling process Methods 0.000 claims description 19
- 238000005859 coupling reaction Methods 0.000 claims description 19
- 239000007788 liquid Substances 0.000 claims description 16
- 238000002347 injection Methods 0.000 claims description 9
- 239000007924 injection Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 238000003825 pressing Methods 0.000 claims description 6
- 238000009434 installation Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 238000007720 emulsion polymerization reaction Methods 0.000 abstract description 3
- 239000000243 solution Substances 0.000 description 12
- 239000012530 fluid Substances 0.000 description 11
- 230000000694 effects Effects 0.000 description 4
- 238000002156 mixing Methods 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000005452 bending Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
Landscapes
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model provides a kind of turbulent device of organic silicon emulsion reaction,Including autoclave body and upper cover,Upper tops are equipped with driving motor,Agitating paddle is equipped in autoclave body,Agitating paddle includes stirring main shaft and blade,Blade is fixedly connected on the lower end of stirring main shaft,Upper cover is equipped with thermometer mounting base,Mounting base is equipped with thermowell,The lower ending opening of thermowell,The outside of thermowell is equipped with the first turbulent structure,The lower section of first turbulent structure is equipped with the second turbulent structure,First turbulent structure includes the first turbulent inclined plate for being fixedly connected on thermowell side and the second turbulent inclined plate for being fixedly connected on the thermowell other side,First turbulent inclined plate and the second turbulent inclined plate arranged crosswise,Second turbulent structure includes the circumferentially uniformly distributed turbulent straight panel along thermowell,Turbulent straight panel is consistent with the length direction of thermowell.The utility model is suitable for the emulsion polymerization of organosilicon, can be improved production efficiency, Improving The Quality of Products.
Description
Technical field
The utility model relates in organic silicon production process consersion unit more particularly to organic silicon emulsion polymerization reaction set
Turbulent device in standby.
Background technique
Usually, the emulsion reaction of organosilicon needs to carry out in heating reaction kettle, stirs while reacting, still
Due to the particular/special requirement of organosilicon material, in the reaction, there are very high requirement, common reaction kettle to the mixability of reaction material
It is unable to satisfy the production requirement of organosilicon.
Summary of the invention
The technical problem to be solved by the utility model is to provide a kind of turbulent devices of organic silicon emulsion reaction, are suitable for
The emulsion polymerization of organosilicon can generate turbulence effect in the reaction solution of stirring, improve production efficiency, promote product matter
Amount.
The utility model technical scheme applied to solve the technical problem is：
A kind of turbulent device of organic silicon emulsion reaction, including autoclave body and upper cover, the top of upper cover are equipped with driving motor, kettle
It is equipped with agitating paddle in vivo, autoclave body is fixedly connected with upper cover by flange, and the side of upper cover is equipped with loading hopper, and the other side is equipped with temperature
Degree meter, agitating paddle include stirring main shaft and blade, and blade is fixedly connected on the lower end of stirring main shaft, and the outer surface of upper cover is equipped with temperature
Degree meter mounting base, mounting base are equipped with and protrude into the intracorporal thermowell of kettle, the lower ending opening of thermowell, thermometer
It is arranged in thermowell, the outside of thermowell is equipped with the first turbulent structure, sets below the first turbulent structure
There is the second turbulent structure, the first turbulent structure includes being fixedly connected on the first turbulent inclined plate of thermowell side and consolidating
Surely it is connected to the second turbulent inclined plate of the thermowell other side, the first turbulent inclined plate and the second turbulent inclined plate arranged crosswise,
Second turbulent structure includes the circumferentially uniformly distributed turbulent straight panel along thermowell, the length of turbulent straight panel and thermowell
It is consistent to spend direction.
Further, the middle part of turbulent straight panel is equipped with square hole, and shaft is equipped in square hole, and shaft is equipped with blade.
Further, blade is uniformly distributed along the circumferential direction of stirring main shaft, and the outside of blade is bent up upwards.
Further, stirring countershaft is equipped in stirring main shaft, stirs the lower end connection liquid scraping device of countershaft, stirring main shaft and
Stirring countershaft is driven by driving motor, and the bottom of reaction kettle is equipped with liquid outlet.
Further, liquid scraping device includes connecting rod, and connecting rod is consistent with the bottom shape of reaction kettle, the both ends of connecting rod
It is bent upwards and connects the scraping blade for being adjacent to reaction kettle side wall.
Further, collet is equipped on the outside of autoclave body, the side of collet is equipped with inlet, and the other side is equipped with liquid outlet.
Further, stirring main shaft is hollow shaft, and the upper end of stirring main shaft is equipped with water injection hole, and blade is groomed oar, blade
Outside be equipped with apopore, the hollow parts of stirring main shaft be connected tos with the hollow parts of blade, and water injection hole and apopore, which pass through, to be stirred
The hollow parts for mixing main shaft are connected to the hollow parts of blade.
Further, the top of upper cover is equipped with driving motor mounting rack, and stirring main shaft and the upper end for stirring countershaft are protruded into
Into driving motor mounting rack, shaft coupling switch is equipped in driving motor mounting rack, be equipped in shaft coupling switch for stirring
The first linkage section that main shaft upper end is fastenedly connected and the second linkage section for being fastenedly connected with stirring countershaft upper end, the first connection
Section is located at below the second linkage section, and shaft coupling switch top is equipped with pressing plate, and shaft coupling switch lower part is equipped with reset spring.
The utility model has the beneficial effects that：
(1) the utility model is provided with thermometer mounting base on upper lid, and thermometer can be inserted and monitor reaction solution at any time
Temperature, prevent from being subcooled heat affecting properties of product, thermometer is arranged in protection pipe, protects thermometer not to be stirred in this way
In liquid smash, thermowell be equipped with turbulent structure, can form turbulent flow in the liquid being stirred, allow stir more
Add sufficiently, promotes the efficiency of stirring and the performance of product.
(2) agitating paddle being bent upwards is equipped in the reaction kettle of the utility model, it can be in the bending part shape of agitating paddle
At inner eddy flow, equivalent to increase the stirring extent inside reaction kettle, so as to promote stirring efficiency.
(3) agitating paddle of the utility model is hollow structure, and upper part is equipped with water injection hole, and lower part is equipped with apopore, can
Entire agitating paddle inside is adequately cleaned.
(4) the utility model is provided with and the coaxial stirring countershaft of agitating paddle, stirring countershaft can drive setting reacting
Scraping blade on kettle inner wall, the reaction solution being splashed on reaction kettle inner wall when by stirring scrape off, it is ensured that the complete degree of stirring.
(5) the stirring countershaft of the utility model can be stirred using the form that is separated with stirring main shaft, compartment of terrain and
Scraping fluid avoids stirring and scraping fluid from influencing each other.
Detailed description of the invention
Fig. 1 is the overall structure figure of the utility model.
Fig. 2 is the schematic diagram of agitating paddle.
Fig. 3 is the schematic diagram of scraping blade.
Fig. 4 is the cross-sectional view of shaft coupling switch.
Fig. 5 is the enlarged drawing of thermowell.
Figure label：Thermometer mounting base 1, agitating paddle 2, autoclave body 3, upper cover 4, flange 5, loading hopper 6, thermometer 7 drive
Dynamic motor 8, stirring main shaft 9, blade 10 stir countershaft 11, liquid scraping device 12, leakage fluid dram 13, connecting rod 14, scraping blade 15, connection
Piece 16, flexible scraping article 17, fixinig plate 18, collet 19, inlet 20, liquid outlet 21, water injection hole 22, apopore 23, driving motor
Mounting rack 24, shaft coupling switch 25, the first linkage section 26, the second linkage section 27, pressing plate 28, reset spring 29, thermometer protection
Pipe 30, the first turbulent inclined plate 31, the second turbulent inclined plate 32, turbulent straight panel 33, square hole 34, turbulent shaft 35, blade 36.
Specific embodiment
It is described in further details below in conjunction with specific embodiment of the attached drawing to the utility model, it is noted that
Embodiment is only specifically described the utility model, is not construed as the restriction to the utility model.
As shown, the utility model provides a kind of turbulent device of organic silicon emulsion reaction, including autoclave body 3 and upper cover 4,
Autoclave body 3 is fixedly connected with upper cover 4 by flange 5, and the side of upper cover 4 is equipped with loading hopper 6, and the other side is equipped with thermometer 7, autoclave body
Agitating paddle 2 is equipped in 3, agitating paddle 2 includes stirring main shaft 8 and blade 10, and blade 10 is fixedly connected on the lower end of stirring main shaft 9,
The outer surface of upper cover 4 is equipped with thermometer mounting base 1, and thermometer mounting base 1 is equipped with the thermowell protruded into autoclave body 3
30, the damage of liquid when avoiding being stirred in thermowell 30 is arranged in 30 lower ending openings of thermowell, thermometer 7
Bad, the outside of thermowell 30 is equipped with the first turbulent structure, and the lower section of the first turbulent structure is equipped with the second turbulent structure, the
One turbulent structure includes being fixedly connected on the first turbulent inclined plate 31 of thermowell side and being fixedly connected on thermometer
The turbulent inclined plate 32 of the second of the protection pipe other side, the first turbulent inclined plate 31 and the second 32 arranged crosswise of turbulent inclined plate, the first turbulent flow
Inclined plate 31 and the second turbulent inclined plate 32 are in respectively 15-30 ° of angle with thermowell 30, and the second turbulent structure includes along temperature
Count the circumferentially uniformly distributed turbulent straight panel 33 of protection pipe 30, the first turbulent inclined plate 32 of turbulent inclined plate 31, second and 33 energy of turbulent inclined plate
It enough generates turbulence effect at various height respectively, improves stirring efficiency.
As a preferred solution, turbulent straight panel 33 is consistent with the length direction of thermowell 30, turbulent straight panel
33 middle part is equipped with square hole 34, turbulent shaft 35 is equipped in square hole 34, turbulent shaft 35 is equipped with blade 36, such as Fig. 5 institute
Show, turbulent straight panel can be set it is multiple, it is preferably uniformly distributed along the circumferential direction of thermowell 30, also set inside the second turbulent structure
Further turbulent structure is set, turbulent shaft 35 can be freely rotated, and when there is fluid to touch, push blade 36 just
Turbulent shaft 35 can be driven to rotate, turbulent flow is further generated in a small range, improve stirring efficiency.
As a preferred solution, stirring countershaft 11 is equipped in stirring main shaft 9, the lower end of stirring countershaft 10 connects scraping fluid
Device 12, stirring main shaft 9 and stirring countershaft 11 are driven by driving motor 8, and the bottom of autoclave body 3 is equipped with leakage fluid dram 13.
As a preferred solution, blade 10 is uniformly distributed along the circumferential direction of stirring main shaft 9, and the outside of blade 10 is bent up upwards,
The lower end of temperature and protection pipe 30, so that it may extend into this gap, cause turbulent flow in the reaction solution in gap.
As a preferred solution, liquid scraping device 12 includes connecting rod 14, the bottom shape of connecting rod 14 and reaction kettle 1
Unanimously, in this way, the both ends of 14 connecting rod of connecting rod are bent upwards and connect the scraping blade 15 for being adjacent to reaction kettle side wall.
As a preferred solution, scraping blade 15 includes connection sheet 16, as shown in figure 3, connection sheet 16 is scraped equipped with flexibility
Item 17, flexible scraping article 17 are the inner wall surfaces of direct effect and autoclave body 3, and in general, the side of flexible scraping article 17 is pasted
The inner wall of tight autoclave body 3, the outside of flexible scraping article 17 are equipped with fixinig plate 18, and fixinig plate 18, flexible scraping article 17 and connection sheet 16 pass through
Fastener is fixed together, and the side that flexible scraping article 17 is adjacent to 3 inner wall of autoclave body has smooth shaving.
As a preferred solution, collet 19 is equipped on the outside of autoclave body 3,19 sides of collet are equipped with inlet 20, another
Side is equipped with liquid outlet 21, and the temperature that autoclave body can be heated or cooled by way of heat exchange is adjusted.
As a preferred solution, stirring main shaft 9 is hollow shaft, and the upper end of stirring main shaft 9 is equipped with water injection hole 22, blade
10 be groomed oar, and the outside of blade 10 is equipped with apopore 23, and the hollow parts of stirring main shaft 9 and the hollow parts of blade 10 connect
Logical, water injection hole 22 is connected to by the hollow parts of stirring main shaft 9 with the hollow parts of blade 10 with apopore 23, since stirring is led
Axis be it is hollow, stirring when necessarily have feed liquid enter wherein, it is therefore desirable to cleaning or cleaning, can be infused by flushing liquor
Enter water injection hole 22, then rinses the hollow parts of stirring main shaft 9 and the hollow parts of blade 10, gone out from apopore 23, to stirring
The inside for mixing paddle is cleaned.
As a preferred solution, stirring main shaft 9 and stirring countershaft 11 can be relatively independent, and respectively by driving
Dynamic motor is driven, because not needing ceaselessly to carry out scraping fluid while agitating sometimes, too frequent scraping fluid
The effect that stirring may be will affect instead, when this, it is necessary to stirring and scraping fluid are carried out respectively, in this case, on
Driving motor mounting rack 24 is arranged in the top of lid 4, and stirring main shaft 9 and the upper end for stirring countershaft 11 extend into driving motor installation
In frame 24, shaft coupling switch 25 is equipped in driving motor mounting rack 24, as shown in figure 4, be equipped in shaft coupling switch 25 for
The first linkage section 26 that 9 upper end of stirring main shaft is fastenedly connected and the second linkage section for being fastenedly connected with stirring 11 upper end of countershaft
27, the first linkage section 26 and the second linkage section 27 can be threaded connection sections, using the form of internal screw thread, in stirring main shaft 9
It is respectively equipped with matching external screw thread with the upper end of stirring countershaft 11, other dismountable connection types can also be used,
Also, in view of stirring main shaft 9 is thicker than stirring countershaft 11, therefore, the first linkage section 26 is located at the lower section of the second linkage section 27, stirs
Mixing countershaft 11 can connect across the first linkage section 26 with the second linkage section 27, on the contrary then not all right, in addition, on shaft coupling switch 25
Portion is equipped with pressing plate 28, and 25 lower part of shaft coupling switch is equipped with reset spring 29, when needing to switch to scraping fluid operation, unclamps shaft coupling and cuts
The connection of parallel operation 25 and stirring main shaft 9, pushing pressing plate 28 makes shaft coupling switch 25 be displaced downwardly to the second linkage section 27 and stirring countershaft
11 upper end cooperation, stirring countershaft 11 and shaft coupling switch 25 are fastenedly connected, scraping fluid operation is carried out, conversely, it is secondary to unclamp stirring
Axis 11 and shaft coupling switch 25 discharge pressing plate 28, and reset spring 29 jacks up shaft coupling switch 25 upwards to be resetted, at this time again can be into
The connection of row stirring cooperates.
Claims (8)
1. a kind of turbulent device of organic silicon emulsion reaction, including autoclave body and upper cover, the top of upper cover are equipped with driving motor, autoclave body
Interior to be equipped with agitating paddle, autoclave body is fixedly connected with upper cover by flange, and the side of upper cover is equipped with loading hopper, and the other side is equipped with temperature
Meter, characterized in that agitating paddle includes stirring main shaft and blade, and blade is fixedly connected on the lower end of stirring main shaft, the appearance of upper cover
Face is equipped with thermometer mounting base, and mounting base is equipped with and protrudes into the intracorporal thermowell of kettle, and the lower end of thermowell is opened
Mouthful, thermometer is arranged in thermowell, and the outside of thermowell is equipped with the first turbulent structure, the first turbulent structure
Lower section be equipped with the second turbulent structure, the first turbulent structure include be fixedly connected on thermowell side first turbulent flow tiltedly
Plate and the second turbulent inclined plate for being fixedly connected on the thermowell other side, the first turbulent inclined plate and the second turbulent inclined plate are handed over
Fork arrangement, the second turbulent structure include the circumferentially uniformly distributed turbulent straight panel along thermowell, and turbulent straight panel and thermometer are protected
The length direction of pillar is consistent.
2. a kind of turbulent device of organic silicon emulsion reaction according to claim 1, characterized in that the middle part of turbulent straight panel
Equipped with square hole, shaft is equipped in square hole, shaft is equipped with blade.
3. a kind of turbulent device of organic silicon emulsion reaction according to claim 1, characterized in that blade is along stirring main shaft
Circumferential direction it is uniformly distributed, the outside of blade is bent up upwards.
4. a kind of turbulent device of organic silicon emulsion reaction according to claim 1, characterized in that be equipped in stirring main shaft
Countershaft is stirred, the lower end connection liquid scraping device of countershaft is stirred, stirring main shaft and stirring countershaft are driven by driving motor, reaction kettle
Bottom be equipped with liquid outlet.
5. a kind of turbulent device of organic silicon emulsion reaction according to claim 4, characterized in that liquid scraping device includes connecting
Extension bar, connecting rod is consistent with the bottom shape of reaction kettle, and the both ends of connecting rod, which are bent upwards and connect, is adjacent to reaction kettle side wall
Scraping blade.
6. a kind of turbulent device of organic silicon emulsion reaction according to claim 1, characterized in that be equipped with folder on the outside of autoclave body
Set, the side of collet are equipped with inlet, and the other side is equipped with liquid outlet.
7. a kind of turbulent device of organic silicon emulsion reaction according to claim 1, characterized in that stirring main shaft is hollow
Axis, the upper end of stirring main shaft are equipped with water injection hole, and blade is groomed oar, and the outside of blade is equipped with apopore, stirring main shaft it is hollow
Part is connected to the hollow parts of blade, and water injection hole and apopore pass through the hollow parts of stirring main shaft and the hollow parts of blade
Connection.
8. a kind of turbulent device of organic silicon emulsion reaction according to claim 1, characterized in that the top of upper cover is equipped with
The upper end of driving motor mounting rack, stirring main shaft and stirring countershaft is extend into driving motor mounting rack, driving motor installation
It is equipped with shaft coupling switch in frame, the first linkage section and use for being fastenedly connected with stirring main shaft upper end are equipped in shaft coupling switch
In the second linkage section being fastenedly connected with stirring countershaft upper end, the first linkage section is located at below the second linkage section, shaft coupling switch
Top is equipped with pressing plate, and shaft coupling switch lower part is equipped with reset spring.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820398173.7U CN208145968U (en) | 2018-03-23 | 2018-03-23 | A kind of turbulent device of organic silicon emulsion reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820398173.7U CN208145968U (en) | 2018-03-23 | 2018-03-23 | A kind of turbulent device of organic silicon emulsion reaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208145968U true CN208145968U (en) | 2018-11-27 |
Family
ID=64392687
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820398173.7U Expired - Fee Related CN208145968U (en) | 2018-03-23 | 2018-03-23 | A kind of turbulent device of organic silicon emulsion reaction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208145968U (en) |
-
2018
- 2018-03-23 CN CN201820398173.7U patent/CN208145968U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20181127 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |