CN208082483U - A kind of herbicide active compound synthesis reaction kettle - Google Patents

A kind of herbicide active compound synthesis reaction kettle Download PDF

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Publication number
CN208082483U
CN208082483U CN201820040172.5U CN201820040172U CN208082483U CN 208082483 U CN208082483 U CN 208082483U CN 201820040172 U CN201820040172 U CN 201820040172U CN 208082483 U CN208082483 U CN 208082483U
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CN
China
Prior art keywords
liquid pipe
autoclave body
annular liquid
active compound
inner cavity
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Expired - Fee Related
Application number
CN201820040172.5U
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Chinese (zh)
Inventor
王珩
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Harbin University of Science and Technology
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Harbin University of Science and Technology
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Priority to CN201820040172.5U priority Critical patent/CN208082483U/en
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Publication of CN208082483U publication Critical patent/CN208082483U/en
Expired - Fee Related legal-status Critical Current
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Abstract

The utility model discloses a kind of herbicide active compound synthesis reaction kettles, including autoclave body, No.1 fluid cylinder, No. two fluid cylinders, upper annular liquid pipe and lower annular liquid pipe, No.1 fluid cylinder and No. two fluid cylinders are respectively arranged on the upper lumen inner wall of autoclave body, it is both provided with piston in No.1 fluid cylinder and No. two fluid cylinders, the middle part of No.1 fluid cylinder and No. two fluid cylinders, which is connected to, is equipped with exhaust pipe, rotation axis is provided with by the rotation of bearing connection type in the inner cavity of autoclave body, the outer ring of rotation axis is installed with several stirring rods, the inner cavity lower part of autoclave body is provided with annular liquid pipe and lower annular liquid pipe respectively.The utility model is simple in structure, and the quality and efficiency for fully improving the synthesis of herbicide active compound are mixed between material, highly practical.

Description

A kind of herbicide active compound synthesis reaction kettle
Technical field
The utility model is related to reaction kettle, specifically a kind of herbicide active compound synthesis reaction kettle.
Background technology
The broad understanding of reaction kettle has the container physically or chemically reacted, is matched with parameter by the structure design to container It sets, realizes the mixture function of the heating of technological requirement, evaporation, cooling and low high speed.Reaction kettle be widely used in oil, chemical industry, Rubber, pesticide, dyestuff, medicine, food, for completing the pressure of the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation Force container.
Herbicide refers to that can make weeds that withered medicament, also known as herbicide thoroughly or selectively occur, eliminating or Inhibit a substance of plant growth.Sodium chlorate therein, borax, arsenate, trichloroacetic acid for any kind of plant all Play the role of it is withered, effect influenced by herbicide, plant and three factor of environmental condition;Herbicide active compound is in the synthesis process It needs to be sufficiently mixed material using reaction kettle.
And it is bad to the mixed effect of material for herbicide active compound synthesis reaction vessel in the prior art, storeroom mixes not The synthetic effect of herbicide active compound will fully be influenced.
Invention content
The purpose of this utility model is to provide a kind of herbicide active compound synthesis reaction kettles, to solve above-mentioned background technology The problem of middle proposition.
To achieve the above object, the utility model provides the following technical solutions:
A kind of herbicide active compound synthesis reaction kettle, including autoclave body, No.1 fluid cylinder, No. two fluid cylinders, upper annular liquid pipe and under Annular liquid pipe, is respectively arranged with No.1 fluid cylinder and No. two fluid cylinders on the upper lumen inner wall of the autoclave body, No.1 fluid cylinder and No. two Piston is both provided in fluid cylinder, two pistons are separately mounted to the bottom end of two telescopic rods;It is provided on the top plate of the autoclave body Two electric expansion cylinders, two electric expansion cylinders, which correspond to, drives two telescopic rods flexible;The No.1 fluid cylinder and No. two fluid cylinders Middle part, which is connected to, is equipped with exhaust pipe, and air bleeding valve is equipped on exhaust pipe;Turned by bearing connection type in the inner cavity of the autoclave body Dynamic to be provided with rotation axis, the outer ring of rotation axis is installed with several stirring rods;It is fixedly installed on the top plate of the autoclave body useful In the driving motor of driving rotation axis rotation;The inner cavity lower part of the autoclave body is provided with annular liquid pipe and lower annular liquid respectively Pipe;The intracavity bottom of the No.1 fluid cylinder is connected with one end of No.1 connecting pipeline;The inner cavity and one of the upper annular liquid pipe The other end of number connecting pipeline is connected;The intracavity bottom of No. two fluid cylinders is connected with one end of No. two connecting pipelines;Institute The inner cavity for stating lower annular liquid pipe is connected with the other end of No. two connecting pipelines.
As further program of the utility model:The end that the output shaft of the driving motor passes through shaft coupling and rotation axis Portion is drivingly connected.
As further program of the utility model:The upper annular liquid pipe is located at the surface of lower annular liquid pipe;It is described It is uniformly provided with and communicated with several No.1 nozzles in upper annular liquid pipe;It is uniformly provided with and communicated with several No. two in the lower annular liquid pipe Nozzle.
As further program of the utility model:The opening down setting of the No.1 nozzle;No. two nozzles Opening up setting.
As further program of the utility model:It is provided with and communicated with charge door on the inner cavity top plate of the autoclave body.
As further program of the utility model:The intracavity bottom of the autoclave body is that the high inclination in intermediate low both ends is set It sets, the intracavity bottom of autoclave body is provided with and communicated with drainage conduit, and blow-off valve is equipped in drainage conduit.
Compared with prior art, the utility model has the beneficial effects that:
The utility model is rotated using driving motor driving rotation axis, and the rotation axis of rotation drives stirring rod in autoclave body Inner cavity in move, to realize being sufficiently mixed for each material in autoclave body inner cavity, the electric expansion cylinder driving telescopic rod of setting is flexible, stretches Contracting bar driving piston moves in the inner cavity of No.1 fluid cylinder, and the partial material of autoclave body inner cavity enters upper annular by No.1 nozzle The inside of liquid pipe, it is spouting by No.1 nozzle later, in addition, the material of No. two fluid cylinder inner cavities is sprayed by No. two nozzles, The mutual convection current of material that the material that No. two nozzles spray is sprayed with No.1 nozzle, further improves the mixing of autoclave body inner cavity material Effect, promotes the combined coefficient of herbicide active compound, and the exhaust pipe of setting can balance No.1 fluid cylinder and No. two fluid cylinder inner cavities Pressure, it is highly practical convenient for remaining herbicide active compound discharge in No.1 fluid cylinder and No. two fluid cylinders.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model.
Fig. 2 is the upward view of upper annular liquid pipe in the utility model.
In figure:1- autoclave bodies, 2- No.1 fluid cylinders, 3- driving motors, 4- rotation axis, 5- stirring rods, 6- No.1 connecting pipelines, 7- No. two fluid cylinders, 8- pistons, 9- telescopic rods, 10- electric expansion cylinders, 11- charge doors, the upper annular liquid pipes of 12-, annular liquid pipe under 13-, No. bis- connecting pipelines of 14-, 15- drainage conduits, 16- blow-off valves, 17- exhaust pipes, 18- air bleeding valves, No. bis- nozzles of 19-, the spray of 20- No.1s Mouth.
Specific implementation mode
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work The every other embodiment obtained, shall fall within the protection scope of the present invention.
Please refer to Fig.1-2, in the utility model embodiment, a kind of herbicide active compound synthesis reaction kettle, including autoclave body 1, 2, No. two fluid cylinders 7 of No.1 fluid cylinder, upper annular liquid pipe 12 and lower annular liquid pipe 13, on the upper lumen inner wall of the autoclave body 1 respectively It is provided with No.1 fluid cylinder 2 and No. two fluid cylinders 7, piston 8 is both provided in No.1 fluid cylinder 2 and No. two fluid cylinders 7, two pistons 8 are distinguished Mounted on the bottom end of two telescopic rods 9;There are two electric expansion cylinder 10, two electric expansions for setting on the top plate of the autoclave body 1 Cylinder 10, which corresponds to, drives two telescopic rods 9 flexible;The No.1 fluid cylinder 2 is connected to the middle part of No. two fluid cylinders 7 and is equipped with exhaust pipe 17, Air bleeding valve 18 is installed on exhaust pipe 17.
Rotation axis 4 is provided with by the rotation of bearing connection type in the inner cavity of the autoclave body 1, the outer ring of rotation axis 4 is fixed Several stirring rods 5 are installed;Fixed setting is useful for the driving motor 3 that driving rotation axis 4 rotates on the top plate of the autoclave body 1, Wherein the output shaft of driving motor 3 is drivingly connected by the end of shaft coupling and rotation axis 4;The inner cavity lower part of the autoclave body 1 It is not provided with annular liquid pipe 12 and lower annular liquid pipe 13, upper annular liquid pipe 12 is located at the surface of lower annular liquid pipe 13;It is described It is uniformly provided with and communicated with several No.1 nozzles 20 in upper annular liquid pipe 12;If being uniformly provided with and communicated in the lower annular liquid pipe 13 Do No. two nozzles 19;The opening down setting of the No.1 nozzle 20;The opening up setting of No. two nozzles 19.
The intracavity bottom of the No.1 fluid cylinder 2 is connected with one end of No.1 connecting pipeline 6;The upper annular liquid pipe 12 Inner cavity is connected with the other end of No.1 connecting pipeline 6;The intracavity bottom of No. two fluid cylinders 7 and the one of No. two connecting pipelines 14 End is connected;The inner cavity of the lower annular liquid pipe 13 is connected with the other end of No. two connecting pipelines 14;The inner cavity of the autoclave body 1 Charge door 11 is provided with and communicated on top plate, the material for synthetic herbicide is added to by charge door 11 in the inner cavity of autoclave body 1; The intracavity bottom of the autoclave body 1, which is that intermediate low both ends are high, to be obliquely installed, and the intracavity bottom of autoclave body 1 is provided with and communicated with drainage conduit 15, blow-off valve 16 is installed in drainage conduit 15.
The operation principle of the utility model is:In use, by charge door 11 is passed through for the material of synthetic herbicide active compound It is added in the inner cavity of autoclave body 1, driving motor 3 is accessed into power supply, driving motor 3 drives rotation axis 4 to be rotated, and rotation turns Moving axis 4 drives stirring rod 5 to be moved in the inner cavity of autoclave body 1, to realize being sufficiently mixed for the autoclave body each material in 1 inner cavity, the electricity of setting Dynamic telescoping cylinder 10 drives telescopic rod 9 flexible, and when telescopic rod 9 shortens, telescopic rod 9 drives piston 8 in the inner cavity of No.1 fluid cylinder 2 It moves upwards, at this time the pressure change of 2 inner cavity of No.1 fluid cylinder, the partial material of 1 inner cavity of autoclave body is entered by No.1 nozzle 20 The inside of upper annular liquid pipe 12, the material of upper 12 inside of annular liquid pipe flow through No.1 connecting pipeline 6 and enter No.1 fluid cylinder 2 later Inner cavity in, when telescopic rod 9 extends, telescopic rod 9 drive piston 8 moved downward in the inner cavity of No.1 fluid cylinder 2, No.1 liquid The material of 2 inner cavities of cylinder is extruded, and spouting by No.1 nozzle 20, and similarly, the material of No. two 7 inner cavities of fluid cylinder passes through No. two Nozzle 19 sprays, and the mutual convection current of material that the material that No. two nozzles 19 spray is sprayed with No.1 nozzle 20 further improves kettle The mixed effect of 1 inner cavity material of body, promotes the combined coefficient of herbicide active compound, due to No.1 fluid cylinder 2 and No. two 7 inner cavities of fluid cylinder Herbicide be not easy to be discharged, open air bleeding valve 18, the exhaust pipe 17 of setting can balance No.1 fluid cylinder 2 and No. two 7 inner cavities of fluid cylinder Pressure, it is highly practical convenient for remaining herbicide active compound discharge in No.1 fluid cylinder 2 and No. two fluid cylinders 7.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this practicality is new in other specific forms Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this practicality is new The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing in the equivalent requirements of the claims will be fallen All changes in justice and range are embraced therein.Any reference numeral in claim should not be considered as limitation Involved claim.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiment being appreciated that.

Claims (6)

1. a kind of herbicide active compound synthesis reaction kettle, including autoclave body(1), No.1 fluid cylinder(2), No. two fluid cylinders(7), upper annular liquid Pipe(12)With lower annular liquid pipe(13), which is characterized in that the autoclave body(1)Upper lumen inner wall on be respectively arranged with No.1 liquid Cylinder(2)With No. two fluid cylinders(7), No.1 fluid cylinder(2)With No. two fluid cylinders(7)Inside it is both provided with piston(8), two pistons(8)Respectively Mounted on two telescopic rods(9)Bottom end, the autoclave body(1)Top plate on setting there are two electric expansion cylinder(10), two electricity Dynamic telescoping cylinder(10)Two telescopic rods of corresponding driving(9)It is flexible, the No.1 fluid cylinder(2)With No. two fluid cylinders(7)Middle part connect It is logical to be equipped with exhaust pipe(17), exhaust pipe(17)On air bleeding valve is installed(18), the autoclave body(1)Inner cavity in connected by bearing Mode, which rotates, is provided with rotation axis(4), rotation axis(4)Outer ring be installed with several stirring rods(5), the autoclave body(1)'s Fixed setting is useful for driving rotation axis on top plate(4)The driving motor of rotation(3), the autoclave body(1)Inner cavity lower part difference It is provided with annular liquid pipe(12)With lower annular liquid pipe(13), the No.1 fluid cylinder(2)Intracavity bottom and No.1 connecting pipeline (6)One end be connected, the upper annular liquid pipe(12)Inner cavity and No.1 connecting pipeline(6)The other end be connected, it is described No. two fluid cylinders(7)Intracavity bottom and No. two connecting pipelines(14)One end be connected, the lower annular liquid pipe(13)Inner cavity With No. two connecting pipelines(14)The other end be connected.
2. a kind of herbicide active compound synthesis reaction kettle according to claim 1, which is characterized in that the driving motor (3)Output shaft pass through shaft coupling and rotation axis(4)End be drivingly connected.
3. a kind of herbicide active compound synthesis reaction kettle according to claim 1, which is characterized in that the upper annular liquid pipe (12)Positioned at lower annular liquid pipe(13)Surface, the upper annular liquid pipe(12)On be uniformly provided with and communicated with several No.1 nozzles (20), the lower annular liquid pipe(13)On be uniformly provided with and communicated with several No. two nozzles(19).
4. a kind of herbicide active compound synthesis reaction kettle according to claim 3, which is characterized in that the No.1 nozzle (20)Opening down setting, No. two nozzles(19)Opening up setting.
5. a kind of herbicide active compound synthesis reaction kettle according to claim 1, which is characterized in that the autoclave body(1)'s It is provided with and communicated with charge door on the top plate of inner cavity(11).
6. a kind of herbicide active compound synthesis reaction kettle according to claim 1, which is characterized in that the autoclave body(1)'s Intracavity bottom, which is that intermediate low both ends are high, to be obliquely installed, autoclave body(1)Intracavity bottom be provided with and communicated with drainage conduit(15), drainage conduit (15)On blow-off valve is installed(16).
CN201820040172.5U 2018-01-10 2018-01-10 A kind of herbicide active compound synthesis reaction kettle Expired - Fee Related CN208082483U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820040172.5U CN208082483U (en) 2018-01-10 2018-01-10 A kind of herbicide active compound synthesis reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820040172.5U CN208082483U (en) 2018-01-10 2018-01-10 A kind of herbicide active compound synthesis reaction kettle

Publications (1)

Publication Number Publication Date
CN208082483U true CN208082483U (en) 2018-11-13

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112169746A (en) * 2020-09-30 2021-01-05 沈阳化工研究院有限公司 Device and method for continuously preparing azo compound
CN112169736A (en) * 2020-09-30 2021-01-05 沈阳化工研究院有限公司 Micro-collision flow stirring reactor

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112169746A (en) * 2020-09-30 2021-01-05 沈阳化工研究院有限公司 Device and method for continuously preparing azo compound
CN112169736A (en) * 2020-09-30 2021-01-05 沈阳化工研究院有限公司 Micro-collision flow stirring reactor
CN112169736B (en) * 2020-09-30 2022-01-07 沈阳化工研究院有限公司 Micro-collision flow stirring reactor
CN112169746B (en) * 2020-09-30 2022-04-15 沈阳化工研究院有限公司 Device and method for continuously preparing azo compound

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20181113

Termination date: 20200110