CN208018167U - Pigment waste acid concentrator - Google Patents

Pigment waste acid concentrator Download PDF

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Publication number
CN208018167U
CN208018167U CN201820126184.XU CN201820126184U CN208018167U CN 208018167 U CN208018167 U CN 208018167U CN 201820126184 U CN201820126184 U CN 201820126184U CN 208018167 U CN208018167 U CN 208018167U
Authority
CN
China
Prior art keywords
evaporator
heat exchanger
outlet
heater
waste acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201820126184.XU
Other languages
Chinese (zh)
Inventor
贺祝
潘文秀
王家雷
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xuzhou Murray Circle Environmental Technology Co Ltd
Original Assignee
Xuzhou Murray Circle Environmental Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xuzhou Murray Circle Environmental Technology Co Ltd filed Critical Xuzhou Murray Circle Environmental Technology Co Ltd
Priority to CN201820126184.XU priority Critical patent/CN208018167U/en
Application granted granted Critical
Publication of CN208018167U publication Critical patent/CN208018167U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

Include the preheater (1) being connect with spent acid input duct the utility model discloses a kind of pigment waste acid concentrator, the pipe outlet of the preheater (1) is connected to primary heater (2);The outlet of the primary heater (2) is connected to the first evaporator (3) by pump, first evaporator (3) is connected with secondary heater (4) by pipeline, and the pipeline is equipped with pressure reducing valve (5);The outlet of the secondary heater (4) is connected to the second evaporator (6), the outlet of second evaporator (6) is at the top of it, communicating pipe (7) is set, second evaporator (6) is connect with the sour pond (8) of storage, the inlet in the storage acid pond (8) is equipped with graphite heat exchanger (9).The utility model is by first preheating spent acid, then passes through two-step heating and twice evaporation respectively, and moisture content therein is recycled, the effect of concentration is further ensured.

Description

Pigment waste acid concentrator
Technical field
The utility model is related to a kind of environmental protection machinerys, are a kind of pigment waste acid concentrators specifically.
Background technology
Will produce a large amount of Waste Sulfuric Acid in many chemical products production process, these sulfuric acid generally diluted by water and Impurity is polluted, and the needs that these Waste Sulfuric Acids do not economize on resources still, the even more requirement of environmental protection are handled and regenerate.And it is current The obtained concentration of waste acid concentration technique sour quality it is unsatisfactory, cause concentration after sulfuric acid can not be recycled.
Utility model content
Purpose of utility model:The purpose of this utility model is to provide a kind of pigment waste acid concentrators.
Technical solution:The utility model is realized using following technological means:A kind of pigment waste acid concentrator, including with it is useless The preheater of sour input duct connection, the pipe outlet of the preheater are connected to primary heater;The level-one heating The outlet of device is connected to the first evaporator by pump, and first evaporator is connected with secondary heater by pipeline, described Pipeline be equipped with pressure reducing valve;The outlet of the secondary heater is connected to the second evaporator, second evaporator Communicating pipe is arranged at the top of it in outlet, the second evaporator is connect with the sour pond of storage, the inlet in the sour pond of the storage is equipped with graphite Heat exchanger;
The primary heater, level-one evaporator, secondary heater, secondary evaporimeter are connected with vacuum pump.
First evaporator and the second evaporator is connect with negative-pressure air fan.
The graphite heat exchanger is the cylindrical heat exchanger being set up in parallel, and the heat exchange of several vertical and horizontal is arranged thereon Pipe, the lateral heat exchanger tube and longitudinal heat exchanger tube are staggered, and are in the plane being mutually parallel.
The primary heater bottom is equipped with steam transfer passage, is heated by steam.
The utility model is by first preheating spent acid, then passes through two-step heating and twice evaporation respectively, will be therein Moisture content recycles, and further ensures the effect of concentration.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is the heat exchanger structure schematic diagram of the utility model.
Reference numeral:1- preheaters, 2- primary heaters, the first evaporators of 3-, 4- secondary heaters, 5- pressure reducing valves, 6- Second evaporator, 7- communicating pipes, the sour pond of 8- storages, 9- graphite heat exchangers, 10- vacuum pumps, 11- negative-pressure air fans, 12- heat exchanger tubes, 13- Steam transfer passage.
Specific implementation mode
In the utility model, evaporating column is commercially available.
The utility model is described in further detail with reference to the accompanying drawings of the specification:
Embodiment:
A kind of pigment waste acid concentrator, includes the preheater 1 being connect with spent acid input duct, and the pipe outlet of preheater 1 connects It is connected to primary heater 2;The outlet of primary heater 2 is connected to the first evaporator 3 by pump, and the first evaporator 3 adds with two level Hot device 4 is connected by pipeline, and pipeline is equipped with pressure reducing valve 5;The outlet of secondary heater 4 is connected to the second evaporator 6, and second steams The outlet of device 6 is sent out at the top of it, communicating pipe 7 is set, the second evaporator 6 is connect with storage acid pond 8, the inlet for storing up sour pond 8 is set There is graphite heat exchanger 9;
Primary heater 2, the first evaporator 3, secondary heater 4, the second evaporator 6 are connected with vacuum pump 10, vacuum Under state, the boiling point of acid solution can reduce, and the first evaporator 3 and the second evaporator 6 are connect with negative-pressure air fan 11, are evaporated Water vapour etc. is recycled to corresponding device by negative-pressure air fan and is collected.
Graphite heat exchanger 9 is the cylindrical heat exchanger being set up in parallel, and the heat exchanger tube 12 of several vertical and horizontal is arranged thereon, Lateral heat exchanger tube 12 and longitudinal heat exchanger tube 12 are staggered, and are in the plane being mutually parallel, such heat exchanger tube knot It when structure makes gas converting heat, will not be interfered with each other between each gas, improve the efficiency of heat exchange.2 bottom of primary heater is equipped with Steam transfer passage 13, is heated by steam.
Acid pickle is first passed through preheater and preheated by the utility model, here, preheater is commercially available plate type preheater, It enters back into primary heater and enters the first evaporator after being heated, water equal solvent therein is tentatively evaporated;It is laggard Enter in secondary heater and heated, enters the second evaporator afterwards, solvent therein is evaporated again;
This practicality carry out primary heater, the first evaporator, secondary heater, the second evaporator under vacuum conditions, The boiling point of acid reduces, and concentrated effect is more preferable.

Claims (4)

1. a kind of pigment waste acid concentrator, it is characterised in that:Include the preheater (1) being connect with spent acid input duct, described is pre- The pipe outlet of hot device (1) is connected to primary heater (2);The outlet of the primary heater (2) is connected to the by pump One evaporator (3), first evaporator (3) are connected with secondary heater (4) by pipeline, and the pipeline, which is equipped with, to be subtracted Pressure valve (5);The outlet of the secondary heater (4) is connected to the second evaporator (6), and the second evaporator (6) go out Communicating pipe (7) is arranged at the top of it in mouth, the second evaporator (6) is connect with the sour pond (8) of storage, the entrance in the storage acid pond (8) Place is equipped with graphite heat exchanger (9);
The primary heater (2), the first evaporator (3), secondary heater (4), the second evaporator (6) are and vacuum pump (10) it is connected.
2. pigment waste acid concentrator as described in claim 1, it is characterised in that:First evaporator (3) and the second evaporation Device (6) is connect with negative-pressure air fan (11).
3. pigment waste acid concentrator as described in claim 1, it is characterised in that:The graphite heat exchanger (9) is to be set up in parallel Cylindrical heat exchanger, the heat exchanger tube (12) of several vertical and horizontal is set thereon, the lateral heat exchanger tube (12) and longitudinal The heat exchanger tube (12) be staggered, and be in the plane being mutually parallel.
4. pigment waste acid concentrator as claimed in claim 2, it is characterised in that:Described primary heater (2) bottom, which is equipped with, steams Vapour transfer passage (13), is heated by steam.
CN201820126184.XU 2018-01-24 2018-01-24 Pigment waste acid concentrator Expired - Fee Related CN208018167U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820126184.XU CN208018167U (en) 2018-01-24 2018-01-24 Pigment waste acid concentrator

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820126184.XU CN208018167U (en) 2018-01-24 2018-01-24 Pigment waste acid concentrator

Publications (1)

Publication Number Publication Date
CN208018167U true CN208018167U (en) 2018-10-30

Family

ID=63903017

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820126184.XU Expired - Fee Related CN208018167U (en) 2018-01-24 2018-01-24 Pigment waste acid concentrator

Country Status (1)

Country Link
CN (1) CN208018167U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117815683A (en) * 2023-12-29 2024-04-05 安徽聚云环保设备制造有限责任公司 Low-temperature normal-pressure concentration recycling device for dilute phosphoric acid in iron phosphate preparation process

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117815683A (en) * 2023-12-29 2024-04-05 安徽聚云环保设备制造有限责任公司 Low-temperature normal-pressure concentration recycling device for dilute phosphoric acid in iron phosphate preparation process

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GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20181030

Termination date: 20210124