CN208008866U - A kind of anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer - Google Patents
A kind of anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer Download PDFInfo
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- CN208008866U CN208008866U CN201820389117.7U CN201820389117U CN208008866U CN 208008866 U CN208008866 U CN 208008866U CN 201820389117 U CN201820389117 U CN 201820389117U CN 208008866 U CN208008866 U CN 208008866U
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- oxidation
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- magnesium alloy
- iron
- prevention block
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Abstract
The utility model discloses a kind of anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer, the device includes vacuum glove box, heating furnace and iron crucible, heating furnace is located in vacuum glove box, iron crucible is located in heating furnace, iron crucible includes top blind flange, iron plate and bottom substrate, sample cell is set on iron plate, and top blind flange, iron plate and bottom substrate are fixedly connected sequentially from the top down.The magnesium base alloy material that the device can be synthesized disposably, device is simple and practical, and sample combined coefficient is high.
Description
Technical field
The utility model is related to a kind of synthesizers of rapid batch block magnesium alloy, and in particular to a kind of anti-oxidation, anti-
Volatilize block magnesium alloy batch synthesizer.
Background technology
Environmentally protective engineering material one of of the magnesium alloy as 21 century has become a research heat of academia in recent years
Point.But it is current, in magnesium alloy sample building-up process, while the problem of oxidation caused by by metal self property, volatilization,
It is difficult the magnesium alloy sample of a variety of proportionings of synthesis in the short time, is matched for screening high-quality.
Utility model content
The purpose of the utility model is to overcome the deficiencies in the prior art, provide a kind of anti-oxidation, volatilization prevention block magnesium conjunction
Golden batch synthesizer, specific technical solution are as follows：
A kind of anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer, which is characterized in that the device includes vacuum glove
Case, heating furnace and iron crucible, the vacuum glove box include babinet, toolroom, transfer chamber, purification system and vacuum pump, institute
The purification system stated is connected to the babinet, and the vacuum pump is connected to the transfer chamber and toolroom, and described adds
Hot stove is placed in the babinet of the vacuum glove box, and the iron crucible is placed in the heating furnace, the iron
Crucible includes top blind flange, iron plate and bottom substrate, and sample cell, the top blind flange, iron plate are provided on the iron plate
It is fixedly connected sequentially from the top down with bottom substrate.
Preferably, it is correspondingly provided with mounting hole on the top blind flange, iron plate and bottom substrate, three passes through fixation
Part achieves a fixed connection across mounting hole.
Preferably, the sample cell is uniformly distributed on the iron plate.
Preferably, protrusion corresponding with the sample cell on the iron plate is provided in the top blind flange.
Preferably, the fixing piece is screw and nut.
The utility model has the beneficial effects that：The device of the utility model is not only complete under conditions of anti-oxidation, volatilization prevention
At the synthesis of sample, but also the disposably magnesium base alloy of synthesis different ratio or certain is a series of using magnesium as the conjunction of matrix
Gold, device is simple and practical, and sample combined coefficient is high.
Description of the drawings
Fig. 1 is the structural schematic diagram of iron crucible；
Fig. 2 is anti-oxidation, the magnesium alloy batch synthesis of volatilization prevention block the device of the utility model；
Wherein, 1- top blind flanges, 2- iron plates, 3- bottom substrates, 4- sample cells, 5- screw holes, 6- screws, 7- nuts, 8- add
Hot stove, 9- vacuum glove boxes, 10- babinets, 11- transfer chambers, 12- pressure gauges, 13- toolrooms, 14- vacuum pumps, 15- purifications system
System.
Specific implementation mode
The utility model is described in detail below according to attached drawing and preferred embodiment, the purpose of this utility model and effect will become
It must be more clearly understood that, below in conjunction with drawings and examples, the present invention will be further described in detail.It should be appreciated that herein
Described specific embodiment is only used to explain the utility model, is not used to limit the utility model.
As shown in Figs. 1-2, a kind of anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer, which includes vacuum hand
Casing 9, heating furnace 8 and iron crucible, the vacuum glove box include babinet 10, toolroom 13, transfer chamber 11, purification system 15
With vacuum pump 14, purification system 15 is connected to babinet 10, and vacuum pump 14 is connected to transfer chamber 11 and toolroom 13, in toolroom 13
It is also equipped with pressure gauge 12, heating furnace 8 is placed in the babinet 10 of vacuum glove box, and iron crucible is placed in heating furnace 8, iron earthenware
Crucible includes top blind flange 1, iron plate 2 and bottom substrate 3, be provided on iron plate 2 more than 100 (each sample be more than 5 millimeters it is straight
Diameter) sample cell 4, screw hole 5 is correspondingly provided on top blind flange 1, iron plate 2 and bottom substrate 3, and three passes through screw 6, nut 7
It is fixedly connected sequentially from the top down across the realization of screw hole 5.
Sample cell on iron plate 2 is uniformly distributed on iron plate.
In order to improve the sealing performance of top blind flange and iron plate, prevent sample from volatilizing, it is preferable that be set in top blind flange 1
It is equipped with protrusion corresponding with the sample cell 4 on iron plate 2.
It is as follows that anti-oxidation, volatilization prevention block magnesium alloy operating process is prepared using device batch：
(1) use purification system 15 by the air purification in the babinet 10 of vacuum glove box；
(2) heating furnace 8 is sent by the transfer chamber 11 of vacuum glove box in babinet 10, and often opens a transfer chamber
11, transfer chamber 11 is vacuumized by vacuum pump 14 and pressure balance several times, ensure babinet 10 in vacuum environment；
(3) iron plate 2 is placed on bottom substrate 3, then sample is put into the sample cell 4 of iron plate of iron crucible, and the bottom of by
Portion's substrate 3, iron plate 2, top blind flange 1 and screw 6, nut 7 are put by toolroom 13 in babinet 10 together, and are often opened primary
Toolroom 13, toolroom 13 is vacuumized by vacuum pump 14 and pressure balance several times, ensure babinet 10 in vacuum ring
Border；
(4) bottom substrate 3, iron plate 2, the screw 6 of top blind flange 1, nut 7 are fixed by the gloves of vacuum glove box,
And it is positioned in heating furnace 8；
(5) according to the sample of different magnesium base alloys, different acid extractions is set to iron crucible, it is then natural
It is cooling, then take out iron crucible by toolroom 13 from the babinet 10 of vacuum glove box, fixed iron crucible is opened, that is, is obtained
Required sample.
By the device of the utility model, primary batch synthesizing block in the environment of anti-oxidation, volatilization prevention may be implemented
Magnesium base alloy, it is simple in structure, it is easy to operate, and sample combined coefficient is high.
It will appreciated by the skilled person that the foregoing is merely the preferred embodiments of utility model, and do not have to
In limitation utility model, although utility model is described in detail with reference to previous examples, for those skilled in the art
Member for, can still modify to the technical solution of aforementioned each case history, or to which part technical characteristic into
Row equivalent replacement.With within principle, modification, equivalent replacement for being made etc. should be included in practical new all spirit in utility model
Within the protection domain of type.
Claims (5)
1. a kind of anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer, which is characterized in that the device includes vacuum glove box
(9), heating furnace (8) and iron crucible, the vacuum glove box (9) include babinet (10), toolroom (13), transfer chamber (11),
Purification system (15) and vacuum pump (14), the purification system (15) are connected to the babinet (10), the vacuum pump
(14) it is connected to the transfer chamber (11) and toolroom (13), the heating furnace (8) is placed on the vacuum glove box
Babinet (10) in, the iron crucible is placed in the heating furnace (8), the iron crucible include top blind flange (1),
Iron plate (2) and bottom substrate (3), setting sample cell (4) on the iron plate (2), the top blind flange (1), iron plate (2) and
Bottom substrate (3) is fixedly connected sequentially from the top down.
2. anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer according to claim 1, which is characterized in that described
Top blind flange (1), be correspondingly provided with mounting hole on iron plate (2) and bottom substrate (3), three passes through installation by fixing piece
Hole achieves a fixed connection.
3. anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer according to claim 1, which is characterized in that described
Sample cell (4) be uniformly distributed on the iron plate (2).
4. anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer according to claim 1, which is characterized in that described
Top blind flange (1) on be provided with protrusion corresponding with sample cell (4) on the iron plate (2).
5. anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer according to claim 2, which is characterized in that described
Fixing piece be screw (6) and nut (7).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820389117.7U CN208008866U (en) | 2018-03-21 | 2018-03-21 | A kind of anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820389117.7U CN208008866U (en) | 2018-03-21 | 2018-03-21 | A kind of anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208008866U true CN208008866U (en) | 2018-10-26 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820389117.7U Active CN208008866U (en) | 2018-03-21 | 2018-03-21 | A kind of anti-oxidation, volatilization prevention block magnesium alloy batch synthesizer |
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| CN (1) | CN208008866U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108546833A (en) * | 2018-03-21 | 2018-09-18 | 浙江大学 | Anti-oxidation, the volatilization prevention block magnesium alloy batch synthesizer of one kind and synthetic method |
-
2018
- 2018-03-21 CN CN201820389117.7U patent/CN208008866U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108546833A (en) * | 2018-03-21 | 2018-09-18 | 浙江大学 | Anti-oxidation, the volatilization prevention block magnesium alloy batch synthesizer of one kind and synthetic method |
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