CN207987115U - A kind of hydrogenation plant for waste lubricant oil regeneration - Google Patents
A kind of hydrogenation plant for waste lubricant oil regeneration Download PDFInfo
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- CN207987115U CN207987115U CN201721410584.5U CN201721410584U CN207987115U CN 207987115 U CN207987115 U CN 207987115U CN 201721410584 U CN201721410584 U CN 201721410584U CN 207987115 U CN207987115 U CN 207987115U
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- reactor
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- fractionating column
- separator
- collector
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Abstract
A kind of hydrogenation plant for waste lubricant oil regeneration, mainly it is made of separator, reactor and fractionating column, it is equipped with waste lubricating oil oil inlet and auxiliary agent adding mouth on separator, in oil product component into catalyst is added before reactor, blow-off pipe is equipped in the bottom of reactor;Hydrogen inlet is equipped on reactor;It is equipped with naphtha collector at the top of fractionating column, diesel oil collector is equipped at the middle part of fractionating column, lube cut oil interceptor is equipped in the lower part of fractionating column, heavy component collector is equipped in the bottom of fractionating column.In addition to reactor top is provided with the gas-phase space of certain altitude, rest part is in liquid phase state, keep the temperature in reactor substantially balanced, it not will produce the high phenomenon of local temperature, so, percussion flow hydrogenation reactor is not easy green coke, tailings discharge capacity is lacked etc., its distillate yield is up to 85% or more, also has many advantages, such as superior product quality, automatic controlling level is high, has wide popularizing application prospect.
Description
Technical field:
The present invention relates to a kind of hydrogenation plant for waste lubricant oil regeneration, belong to the processing modification essence to regenerative resource
Process field processed.
Background technology:
With the development of economy, the application of lubricating oil is increasingly extensive, lubricating oil in use for some time, performance indicator
Decline and need replacing, to generate a large amount of waste.Since waste lubricating oil is after refined and modifying process, additionally it is possible to
Recycling, therefore more and more important has been become to waste lubricating oil recovery and reusing and recycling, it both economized on resources, turned waste into wealth, again
It can reduce and prevent the pollution of the environment, there is very considerable economic benefit and social benefit.
Currently, China's process for regeneration of waste lubricating oil, still in relatively primitive state, traditional processing technology routine also takes up
Leading position, and traditional waste lubricating oil recycles mixed hydrogenation treatment process, complex steps, the waste of generation be more, oneself
The low, poor quality of properties of product etc. that dynamicization degree is low, produces.
Utility model content:
The utility model in order to make up for the deficiencies of the prior art, provide it is a kind of for waste lubricant oil regeneration plus hydrogen dress
It sets, is especially suitable for processing waste lubricating oil material inferior, it can be can only be handled refined as the waste that fuel uses originally
It by re-effective is utilized for the high raw material of lubricating oil oil product, advantageously reduces pollution, the renewable cycle of the energy is promoted to make
With solving problems of the prior art.
Used technical solution is the utility model to solve above-mentioned technical problem:
A kind of hydrogenation plant for waste lubricant oil regeneration is mainly made of separator, reactor and fractionating column, is being detached
Device is equipped with waste lubricating oil oil inlet and auxiliary agent adding mouth, in oil product component into catalyst is added before reactor, in reactor
Bottom is equipped with blow-off pipe;Hydrogen inlet is equipped on reactor;It is equipped with naphtha collector at the top of fractionating column, is being fractionated
The middle part of tower is equipped with diesel oil collector, is equipped with lube cut oil interceptor in the lower part of fractionating column, is set in the bottom of fractionating column
There is heavy component collector.
The separator is hypergravity separator.
The reactor is impact flow reactor.
The catalyst is to contain the two or more mixtures in molybdenum, cobalt, iron, zinc, copper.
The auxiliary agent is the mixture of demulsifier and flocculant.
The mode that the utility model reactor is fed respectively using liquid, gas reaches the feedstock oil of certain temperature
Enter from the lower part of reactor after mixed catalyst, is sprayed upwards by raw material nozzle component;Hydrogen enters the middle part of reactor
Nozzle assembly flows downward, and the feedstock oil counter current contacting from reactor lower part, and reacts.Counter current contacting can be strengthened
The mass transfer of gas and two kinds of materials of liquid expands contact area, achievees the purpose that fast reaction;Lower reactor is empty simultaneously
Speed, also helps the sundries such as the metal in raw material, colloid, asphalitine and the catalyst for refining reaction slowly concentrates on instead
The bottom for answering device is provided with oil circulating pump, the cycle stock nozzle in the middle part of Returning reactor in reactor bottom.From entirety, remove
Reactor top is provided with outside the gas-phase space of certain altitude, and rest part is in liquid phase state, makes the temperature in reactor
It is substantially balanced, it not will produce the high phenomenon of local temperature, so, percussion flow hydrogenation reactor is not easy green coke, tailings discharge
The advantages that amount waits less, distillate yield is up to 85% or more, also has superior product quality, automatic controlling level height etc. excellent
Point has wide popularizing application prospect.
Description of the drawings:
Fig. 1 is the structural schematic diagram of the utility model.
In figure, 1, separator, 2, reactor, 3, fractionating column, 4, waste lubricating oil oil inlet, 5, auxiliary agent adding mouth, 6, blowdown
Pipe, 7, hydrogen inlet, 8, naphtha collector, 9, diesel oil collector, 10, lube cut oil interceptor, 11, heavy component
Collector, 12, catalyst.
Specific implementation mode:
In order to clarify the technical characteristics of the invention, below by specific implementation mode, and its attached drawing is combined, to this reality
It is described in detail with novel.
As shown in Figure 1, a kind of hydrogenation plant for waste lubricant oil regeneration, mainly by separator 1, reactor 2 and fractionation
Tower 3 forms, and waste lubricating oil oil inlet 4 and auxiliary agent adding mouth 5 are equipped on separator 1, in oil product component into being added before reactor 2
Catalyst 12 is equipped with blow-off pipe 6 in the bottom of reactor 2;Hydrogen inlet 7 is equipped on reactor 2;On the top of fractionating column 3
Portion is equipped with naphtha collector 8, and diesel oil collector 9 is equipped at the middle part of fractionating column 3, and lubricating oil is equipped in the lower part of fractionating column 3
Fraction oil interceptor 10 is equipped with heavy component collector 11 in the bottom of fractionating column 3.
The separator 1 is hypergravity separator 1;The moisture content in waste lubricating oil is taken off using mechanical means by density contrast
It removes, obtains relatively pure oil product component, while the ingredients such as part metals, impurity can also be removed.
The reactor 2 is impact flow reactor 2;Under the effect of the catalyst with hydrogen counter current contacting, carries out plus hydrogen is smart
System reaction, and remove demetalization, Jiao Zhi, asphalitine and a variety of harmful components again.
The catalyst 12 is to contain the two or more mixtures in molybdenum, cobalt, iron, zinc, copper.
The auxiliary agent is the mixture of demulsifier and flocculant.
When operation, the heavy ingredients such as raw material is tangentially sent into the internal layer of hypergravity separator 1 by high speed, and moisture, machine are miscellaneous by
It gradually flows downward, oil product component flows upwards out, and percussion flow hydrogenation reactor 2 is removed after heating.The method handle detached by hypergravity
Moisture content removing is fallen in waste lubricating oil, obtains relatively pure oil product component, at the same also remove part metals, mechanical admixture etc. at
Point;By oil product component under the effect of the catalyst enter percussion flow hydrogenation reactor 2, carry out hydrofining reaction, removing metal,
The a variety of harmful components of Jiao Zhi, asphalitine etc.;Reaction product enters separator 1, and gas-liquid separation is carried out by high score, separation
Gas is used for hydrogenation reaction as recycle hydrogen, and isolated liquid enters fractionating column 3 and detached;It is obtained at 3 top of fractionating column
To naphtha, 3 middle part side line of fractionating column obtains diesel component, and 3 lower part side line of fractionating column obtains lube cut, and tower bottom obtains
Heavy component;The heavy component of 3 bottom of fractionating column comes back for freshening operation, can also be as byproduct.
Place is not described in detail for the utility model, is the known technology of those skilled in the art of the present technique.
Claims (3)
1. a kind of hydrogenation plant for waste lubricant oil regeneration, it is characterised in that:Mainly by separator, reactor and fractionating column group
At, waste lubricating oil oil inlet and auxiliary agent adding mouth are equipped on separator, in oil product component into catalyst is added before reactor,
The bottom of reactor is equipped with blow-off pipe;Hydrogen inlet is equipped on reactor;It is collected equipped with naphtha at the top of fractionating column
Device, diesel oil collector is equipped at the middle part of fractionating column, lube cut oil interceptor is equipped in the lower part of fractionating column, in fractionating column
Bottom be equipped with heavy component collector.
2. a kind of hydrogenation plant for waste lubricant oil regeneration according to claim 1, it is characterised in that:The separator
For hypergravity separator.
3. a kind of hydrogenation plant for waste lubricant oil regeneration according to claim 1, it is characterised in that:The reactor
For impact flow reactor.
Priority Applications (1)
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CN201721410584.5U CN207987115U (en) | 2017-10-27 | 2017-10-27 | A kind of hydrogenation plant for waste lubricant oil regeneration |
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CN201721410584.5U CN207987115U (en) | 2017-10-27 | 2017-10-27 | A kind of hydrogenation plant for waste lubricant oil regeneration |
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CN207987115U true CN207987115U (en) | 2018-10-19 |
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CN201721410584.5U Expired - Fee Related CN207987115U (en) | 2017-10-27 | 2017-10-27 | A kind of hydrogenation plant for waste lubricant oil regeneration |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110194968A (en) * | 2019-04-30 | 2019-09-03 | 武汉金中石化工程有限公司 | A kind of waste lubricating oil full constituent floating bed hydrogenation regeneration technology |
-
2017
- 2017-10-27 CN CN201721410584.5U patent/CN207987115U/en not_active Expired - Fee Related
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110194968A (en) * | 2019-04-30 | 2019-09-03 | 武汉金中石化工程有限公司 | A kind of waste lubricating oil full constituent floating bed hydrogenation regeneration technology |
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CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20181019 Termination date: 20211027 |