CN207951448U - A kind of chlorinating container for medicine intermediate - Google Patents
A kind of chlorinating container for medicine intermediate Download PDFInfo
- Publication number
- CN207951448U CN207951448U CN201820186611.3U CN201820186611U CN207951448U CN 207951448 U CN207951448 U CN 207951448U CN 201820186611 U CN201820186611 U CN 201820186611U CN 207951448 U CN207951448 U CN 207951448U
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- China
- Prior art keywords
- reaction kettle
- fixed
- driving motor
- case
- tube
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Abstract
The utility model discloses a kind of chlorinating containers for medicine intermediate, including reaction kettle case, driving motor, feed inlet and power supply panel, the driving motor is located at the top of reaction kettle case, the feed inlet is located at driving motor side and is conducted with reaction kettle case, the power supply panel is fixed on reaction kettle case side, the reaction kettle envelope surface is connected with heating mantle, the driving motor bottom is fixedly connected with agitating shaft, the reaction kettle case inner cavity top is fixed with manograph, the manograph side is fixed with relief valve, the conducting of reaction kettle casing base side is connected with drainage conduit, the shaft bottom is fixedly connected with U-tube.The utility model is designed reasonably is novel, easy to operate and use, and reaction kettle combines stirring, chlorination, heating, cleaning and increase light source to be integrated, and can effectively increase the efficiency of pharmaceutical intermediate chlorination, have higher practicability, be suitble to be widely popularized and use.
Description
Technical field
The utility model is related to a kind of reaction kettles, more particularly to a kind of chlorinating container for medicine intermediate.
Background technology
Chlorination reaction refers generally to the reaction being introduced into chlorine element in compound.In organic chemical reactions, chlorination reaction one
As include displacement chlorination, addition chlorination and oxidation chlorination；In metallurgical industry, certain metals are refined using chlorine or chloride
Claim chlorination；In water throw chlorine or containing oxychloride with reach oxidation and disinfection the purpose of process be also referred to as chlorination.
During chlorination production, often there are many drawbacks, the utilization rate such as chlorine is low, the mixing effect of chlorine and material
Fruit is poor and causes reaction efficiency relatively low.In addition, the cleaning inside reaction kettle is very troublesome, generally requires and dismantle reaction kettle
It is cleaned again, needs to expend more manpower and materials.For this purpose, it is proposed that a kind of chlorination reaction for medicine intermediate
Kettle.
Utility model content
The main purpose of the utility model is to provide a kind of chlorinating containers for medicine intermediate, can effectively solve
Certainly the problems in background technology.
To achieve the above object, the technical solution that the utility model is taken is：
A kind of chlorinating container for medicine intermediate, including reaction kettle case, driving motor, feed inlet and power supply face
Plate, the driving motor are located at the top of reaction kettle case, the feed inlet be located at driving motor side and with reaction kettle case phase
Conducting, the power supply panel are fixed on reaction kettle case side, and the reaction kettle envelope surface is connected with heating mantle, described
Driving motor bottom is fixedly connected with agitating shaft, and the reaction kettle case inner cavity top is fixed with manograph, the manograph one
Side is fixed with relief valve, and the conducting of reaction kettle casing base side is connected with drainage conduit, and the shaft bottom is fixedly connected
There are U-tube, the U-tube side to be fixedly connected with seal glass cover, the U-tube bottom side is connected with gas supply by bearing seal
Pipe, air supply pipe one end conducting are connected with chlorine pot.
Further, the side is fixed with electromagnet, and the electromagnet side is fixed with power supply case.
Further, seal glass cover inner cavity is fixedly connected with ultraviolet lamp tube.
Further, the air supply pipe side is connected with feed pipe by valve conducting, and feed pipe one end conducting connects
It is connected to water supply pump.
Further, the chlorine pot side is fixed with booster pump, and the U-tube surface is fixed with gas vent.
Compared with prior art, the utility model has the advantages that：
1. this kind is used for the chlorinating container of medicine intermediate, by feed inlet into reaction kettle case inner cavity injection medicine
Mesosome raw material is in series by power supply panel with driving motor, and then so that driving motor is powered and run, and agitating shaft and U-tube are driven
It is rotated, while U-tube bottom is connected with air supply pipe by bearing, and chlorine pot side is fixed with booster pump, utilizes supercharging
Pump carries out pressure testing to chlorine pot inside, so that internal chlorine is passed through air supply pipe and arranges to U-tube inner cavity, U-tube surface is fixed with row
Stomata accelerates the mixing efficiency for removing pharmaceutical intermediate, while utilizing sealing glass so that chlorine is released in whipping process
The ultraviolet lamp tube of glass cover inner cavity, which is powered, to be irradiated, and then the efficiency of quickening chlorination, more practical.
2. in reaction temperature deficiency, heating mantle can be fixed by electromagnet, heating mantle is made to be fixed on reaction
Kettle envelope surface, the making of the thermal insulation material with heating wire can be used in heating mantle, and is carried out to electromagnet using power supply case
Power supply, makes the external supply line of heater strip heat reaction kettle case, to improve the efficiency of chlorination reaction, more
It is practical.
3. the later stage needs to clean reaction kettle inside, feed pipe can be utilized by the external watering of water supply pump
Water source is injected to U-tube inner cavity, and then reaction kettle inner wall and agitating shaft surface are cleared up in whipping process, avoids drug
Residual, the later stage can by drainage conduit by after the completion of chlorination liquid or cleaning water discharge.
Description of the drawings
Fig. 1 is overall structure diagram of the utility model for the chlorinating container of medicine intermediate.
Fig. 2 is internal structure schematic diagram of the utility model for the chlorinating container of medicine intermediate.
In figure：1, reaction kettle case；2, driving motor；3, feed inlet；4, power supply panel；5, heating mantle；6, electromagnet；7、
Power supply case；8, agitating shaft；9, manograph；10, relief valve；11, drainage conduit；12, U-tube；13, seal glass cover；14, ultraviolet lamp
Pipe；15, air supply pipe；16, chlorine pot；17, feed pipe；18, water supply pump.
Specific implementation mode
To make the technical means, creative features, achievement of purpose, and effectiveness of the utility model be easy to understand, below
In conjunction with specific implementation mode, the utility model is expanded on further.
As shown in Figs. 1-2, a kind of chlorinating container for medicine intermediate, including reaction kettle case 1, driving motor 2,
Feed inlet 3 and power supply panel 4, the driving motor 2 are located at 1 top of reaction kettle case, and the feed inlet 3 is located at driving motor 2
It side and is conducted with reaction kettle case 1, the power supply panel 4 is fixed on 1 side of reaction kettle case, the reaction kettle case 1
Surface activity is connected with heating mantle 5, and 2 bottom of the driving motor is fixedly connected with agitating shaft 8,1 inner cavity of reaction kettle case
Top is fixed with manograph 9, and 9 side of the manograph is fixed with relief valve 10, and 1 bottom side of the reaction kettle case conducting connects
It is connected to drainage conduit 11,8 bottom of the agitating shaft is fixedly connected with U-tube 12, and 12 side of the U-tube is fixedly connected with sealing glass
Glass cover 13,12 bottom side of the U-tube are connected with air supply pipe 15 by bearing seal, and the conducting of 15 one end of the air supply pipe is connected with chlorine
Gas tank 16.
Wherein, the side is fixed with electromagnet 6, and 6 side of the electromagnet is fixed with power supply case 7.
Wherein, 13 inner cavity of seal glass cover is fixedly connected with ultraviolet lamp tube 14.
Wherein, 15 side of the air supply pipe is connected with feed pipe 17, the conducting of 17 one end of the feed pipe by valve conducting
It is connected with water supply pump 18.
Wherein, 16 side of the chlorine pot is fixed with booster pump, and 12 surface of the U-tube is fixed with gas vent.
It should be noted that the utility model is a kind of chlorinating container for medicine intermediate, when work, by into
Material mouth 3 injects medicine intermediate raw material to 1 inner cavity of reaction kettle case, is in series by power supply panel 4 and driving motor 2, and then make
Driving motor 2, which is powered, to be run, and drives agitating shaft 8 and U-tube 12 to be rotated, while 12 bottom of U-tube is connected with by bearing
Air supply pipe 15, and 16 side of chlorine pot is fixed with booster pump, carries out pressure testing to 16 inside of chlorine pot using booster pump, makes internal chlorine
Gas is by 15 row of air supply pipe to 12 inner cavity of U-tube, and 12 surface of U-tube is fixed with gas vent, so that chlorine is stirred
It is released in journey, accelerates the mixing efficiency for removing pharmaceutical intermediate, while logical using the ultraviolet lamp tube 14 of 13 inner cavity of seal glass cover
Electricity irradiation, and then accelerate the efficiency of chlorination, it is more practical, it, can be by electromagnet 6 to heating mantle 5 in reaction temperature deficiency
It is fixed, heating mantle 5 is made to be fixed on 1 surface of reaction kettle case, the thermal insulation material system with heating wire can be used in heating mantle 5
Make, and electromagnet 6 is powered using power supply case 7, the external supply line of heater strip is made to heat reaction kettle case 1
Processing, it is more practical to improve the efficiency of chlorination reaction, when the later stage needs to clean reaction kettle inside, it can pass through
18 external watering of water supply pump injects water source using feed pipe 17 to 12 inner cavity of U-tube, and then to reaction kettle in whipping process
Inner wall and 8 surface of agitating shaft are cleared up, and avoid medicament residue, and the later stage can be by drainage conduit 11 by the liquid after the completion of chlorination
Or cleaning water discharge.
The advantages of basic principles and main features and the utility model of the utility model have been shown and described above.One's own profession
The technical staff of industry is it should be appreciated that the present utility model is not limited to the above embodiments, described in above embodiments and description
Only illustrate the principles of the present invention, on the premise of not departing from the spirit and scope of the utility model, the utility model is also
It will have various changes and improvements, these various changes and improvements fall within the scope of the claimed invention.The utility model
Claimed range is defined by the appending claims and its equivalent thereof.
Claims (5)
1. a kind of chlorinating container for medicine intermediate, including reaction kettle case (1), driving motor (2), feed inlet (3)
With power supply panel (4), the driving motor (2) is located at the top of reaction kettle case (1), and the feed inlet (3) is located at driving motor
(2) it side and is conducted with reaction kettle case (1), the power supply panel (4) is fixed on reaction kettle case (1) side, feature
It is：Reaction kettle case (1) surface activity is connected with heating mantle (5), and driving motor (2) bottom, which is fixedly connected with, to be stirred
Axis (8) is mixed, reaction kettle case (1) inner cavity top is fixed with manograph (9), and manograph (9) side is fixed with pressure release
Valve (10), reaction kettle case (1) the bottom side conducting are connected with drainage conduit (11), and agitating shaft (8) bottom, which is fixed, to be connected
It is connected to U-tube (12), U-tube (12) side is fixedly connected with seal glass cover (13), and U-tube (12) bottom side passes through
Bearing seal is connected with air supply pipe (15), and air supply pipe (15) one end conducting is connected with chlorine pot (16).
2. a kind of chlorinating container for medicine intermediate according to claim 1, it is characterised in that：The side is solid
There are electromagnet (6), electromagnet (6) side to be fixed with power supply case (7) surely.
3. a kind of chlorinating container for medicine intermediate according to claim 1, it is characterised in that：The sealing glass
Glass cover (13) inner cavity is fixedly connected with ultraviolet lamp tube (14).
4. a kind of chlorinating container for medicine intermediate according to claim 1, it is characterised in that：The air supply pipe
(15) side is connected with feed pipe (17) by valve conducting, and feed pipe (17) one end conducting is connected with water supply pump (18).
5. a kind of chlorinating container for medicine intermediate according to claim 1, it is characterised in that：The chlorine pot
(16) side is fixed with booster pump, and U-tube (12) surface is fixed with gas vent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820186611.3U CN207951448U (en) | 2018-02-02 | 2018-02-02 | A kind of chlorinating container for medicine intermediate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820186611.3U CN207951448U (en) | 2018-02-02 | 2018-02-02 | A kind of chlorinating container for medicine intermediate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207951448U true CN207951448U (en) | 2018-10-12 |
Family
ID=63737055
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820186611.3U Expired - Fee Related CN207951448U (en) | 2018-02-02 | 2018-02-02 | A kind of chlorinating container for medicine intermediate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207951448U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113912644A (en) * | 2021-09-29 | 2022-01-11 | 封丘县龙润精细化工有限公司 | Novel green synthesis process and device for pharmaceutical-grade ethyl chloride |
-
2018
- 2018-02-02 CN CN201820186611.3U patent/CN207951448U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113912644A (en) * | 2021-09-29 | 2022-01-11 | 封丘县龙润精细化工有限公司 | Novel green synthesis process and device for pharmaceutical-grade ethyl chloride |
| CN113912644B (en) * | 2021-09-29 | 2022-09-09 | 河南嘉颖生物科技有限公司 | Pharmaceutical-grade ethyl chloride synthesis process and device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20181012 Termination date: 20220202 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |