CN207871966U - A kind of crystalline mother solution material recovering system - Google Patents

A kind of crystalline mother solution material recovering system Download PDF

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Publication number
CN207871966U
CN207871966U CN201820013668.3U CN201820013668U CN207871966U CN 207871966 U CN207871966 U CN 207871966U CN 201820013668 U CN201820013668 U CN 201820013668U CN 207871966 U CN207871966 U CN 207871966U
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China
Prior art keywords
mother solution
crystalline mother
solution tank
crystalline
pipeline
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CN201820013668.3U
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Chinese (zh)
Inventor
黄兆彪
庞博湛
叶强
李海平
孙春光
毕作鹏
熊昌武
孙东辉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lian Long (central Defender) New Material Co Ltd
Lian Long (zhuhai) New Materials Co Ltd
RIANLON Corp
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Lian Long (central Defender) New Material Co Ltd
Lian Long (zhuhai) New Materials Co Ltd
RIANLON Corp
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Application filed by Lian Long (central Defender) New Material Co Ltd, Lian Long (zhuhai) New Materials Co Ltd, RIANLON Corp filed Critical Lian Long (central Defender) New Material Co Ltd
Priority to CN201820013668.3U priority Critical patent/CN207871966U/en
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Abstract

The utility model provides a kind of crystalline mother solution material recovering system, the top side of crystalline mother solution tank is provided with feed inlet, it is provided with radial flow blender in the crystalline mother solution tank of bottom, the discharge port of recycling sticky material is provided on the crystalline mother solution pot sidewall of bottom, it recycles and is provided with transfering material pump on the first pipeline that sticky material discharge port is connected to retracting device, it is provided with mother liquor outlet on the crystalline mother solution pot sidewall of bottom, mother liquor outlet is connected to by the second pipeline with mother liquor rectifying column, and mother liquor delivery pump is provided on the second pipeline.The utility model is simple in sturcture, ingenious in design, can recycle high-content sticky material, is converted into product, improves production efficiency.

Description

A kind of crystalline mother solution material recovering system
Technical field
The utility model belongs to sticky material recovery technology field in crystalline mother solution, more particularly, to a kind of crystalline mother solution object Expect recovery system.
Background technology
In the centrifugation engineering of crystallized stock, understand solid material that some is crystallized out and undecomposed product with from Heart mother liquor enters in crystalline mother solution tank.Especially when crystallization effect is poor, has a large amount of solid material and enter crystalline mother solution In tank, product content is higher in this partial material, there is recovery value.
Common processing method is after crystalline mother solution is recycled recrystallisation solvent by rectifying, this expendable-limited-recoverable material into It is residual as low grade products sale to enter kettle.But this processing method has the disadvantage that, and first, do not make full use of in mother liquor Product causes yield to decline, and reduces production efficiency;Second, distillation process meeting consumption of calorie, waste of energy;Third, it is also necessary to people Power unlap low grade products, waste of manpower.
Invention content
In view of this, the utility model is directed to a kind of crystalline mother solution material recovering system, asked with solving above-mentioned technology Topic.
In order to achieve the above objectives, the technical solution of the utility model is realized in:
A kind of crystalline mother solution material recovering system, the top side of crystalline mother solution tank are provided with feed inlet, close to bottom It is provided with radial flow blender in crystalline mother solution tank, the sticky material discharging of recycling is provided on the crystalline mother solution pot sidewall of bottom Mouthful, it recycles and is provided with transfering material pump on the first pipeline that sticky material discharge port is connected to retracting device, the crystalline mother solution close to bottom Mother liquor outlet is provided on pot sidewall, mother liquor outlet is connected to by the second pipeline with mother liquor rectifying column, and mother is provided on the second pipeline Liquid delivery pump.
Further, the feed pipe at feed inlet is extend into inside the crystalline mother solution tank of crystalline mother solution pot bottom.
Further, the lower port of feed pipe is located at the one third height of crystalline mother solution tank inner cavity.
Further, height of the mother liquor outlet apart from crystalline mother solution pot bottom is crystallized higher than sticky material discharge port distance is recycled The height of mother liquor pot bottom.
Further, mother liquor delivery pump by triplate line respectively with the refluxing opening on mother liquor rectifying column, crystalline mother solution tank Connection.
Further, it is additionally provided with nitrogen inlet and offgas outlet at the top of crystalline mother solution tank, nitrogen inlet passes through pipeline It is connected to nitrogen pipeline, offgas outlet is connected to by pipeline with exhaust treatment system.
Further, the outside of crystalline mother solution tank is provided with thermometer and liquid level gauge.
Further, the motor of radial flow blender is located at the over top of crystalline mother solution tank.
Further, it is provided with filter on the second pipeline between mother liquor delivery pump and mother liquor outlet.
Compared with the existing technology, a kind of crystalline mother solution material recovering system described in the utility model has the advantage that:
(1) the utility model is simple in sturcture, ingenious in design, can recycle high-content sticky material, is converted into product, improves Production efficiency;
(2) the utility model uses radial flow blender, avoids sticky material axially movable;
(3) the utility model can effectively reduce the thermal losses in distillation process, save the energy;
(4) the utility model has effectively saved cost of human resources.
Description of the drawings
The attached drawing for constituting the part of the utility model is used to provide a further understanding of the present invention, this practicality is new The illustrative embodiments and their description of type are not constituted improper limits to the present invention for explaining the utility model. In attached drawing:
Fig. 1 is the structural schematic diagram of the prior art of the utility model embodiment;
Fig. 2 is the structural schematic diagram of the utility model embodiment.
Reference sign:
1, crystalline mother solution tank;101, feed inlet;102, sticky material discharge port is recycled;103, mother liquor outlet;104, refluxing opening; 105, nitrogen inlet;106, offgas outlet;107, discharge port;2, radial flow blender;201, motor;3, the first pipeline;4, turn Material pump;5, the second pipeline;6, mother liquor delivery pump;7, filter;8, thermometer;9, liquid level gauge;10, delivery pump;11, feed pipe.
Specific implementation mode
It should be noted that in the absence of conflict, the feature in the embodiments of the present invention and embodiment can To be combined with each other.
In the description of the present invention, it should be understood that term "center", " longitudinal direction ", " transverse direction ", "upper", "lower", The orientation or positional relationship of the instructions such as "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outside" is It is based on the orientation or positional relationship shown in the drawings, is merely for convenience of describing the present invention and simplifying the description, rather than indicate Or imply that signified device or element must have a particular orientation, with specific azimuth configuration and operation, therefore cannot understand For limitations of the present invention.In addition, term " first ", " second " etc. are used for description purposes only, and should not be understood as indicating Or it implies relative importance or implicitly indicates the quantity of indicated technical characteristic." first ", " second " etc. are defined as a result, Feature can explicitly or implicitly include one or more this feature.It is in the description of the present invention, unless another It is described, the meaning of " plurality " is two or more.
In the description of the present invention, it should be noted that unless otherwise clearly defined and limited, term " is pacified Dress ", " connected ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or integrally Connection;It can be mechanical connection, can also be electrical connection;Can be directly connected, can also indirectly connected through an intermediary, It can be the connection inside two elements.For the ordinary skill in the art, on being understood by concrete condition State the concrete meaning of term in the present invention.
The utility model will be described in detail below with reference to the accompanying drawings and embodiments.
As shown in Figure 1, crystalline mother solution tank 1 in the prior art include feed inlet 101 and discharge port 107, crystalline mother solution into Enter crystalline mother solution tank 1, the crystalline mother solution inside crystalline mother solution tank 1 enters mother liquor rectifying column by delivery pump 10.
As shown in Fig. 2, a kind of crystalline mother solution material recovering system, including crystalline mother solution tank 1, the top of crystalline mother solution tank 1 Side is provided with feed inlet 101.Feed pipe 11 at feed inlet 101 is extend into inside crystalline mother solution tank 1, the lower end of feed pipe 11 Mouth extend into the position close to 1 bottom of crystalline mother solution tank, it is preferred that the lower port of feed pipe 11 is located at 1 inner cavity of crystalline mother solution tank One third height at.The bottom middle position of crystalline mother solution tank 1 is provided with radial flow blender 2, radial flow blender 2 Motor 201 be located at the over top of crystalline mother solution tank 1.The sticky material of recycling is provided on 1 side wall of crystalline mother solution tank of bottom Discharge port 102 recycles and is provided with transfering material pump 4 on the first pipeline 3 that sticky material discharge port 102 is connected to retracting device.
Be provided with mother liquor outlet 103 on 1 side wall of crystalline mother solution tank of bottom, mother liquor outlet 103 by the second pipeline 5 with Mother liquor rectifying column is connected to.Mother liquor delivery pump 6 is provided on second pipeline 5, between mother liquor delivery pump 6 and mother liquor outlet 103 It is provided with filter 7 on two pipelines 5.Mother liquor delivery pump 6 by triplate line respectively on mother liquor rectifying column, crystalline mother solution tank 1 Refluxing opening 104 be connected to.Refluxing opening 104 is arranged at the top of crystalline mother solution tank 1.Mother liquor outlet 103 relatively recycles sticky material discharging Mouth 102 is high, and specific height is determined by material properties and reclaimed materials recycling frequency, ensures that mother liquor outlet 103 will not add up reclaimed materials.
The top of crystalline mother solution tank 1 is additionally provided with nitrogen inlet 105 and offgas outlet 106, and nitrogen inlet 105 passes through pipeline It is connected to nitrogen pipeline, offgas outlet 106 is connected to by pipeline with exhaust treatment system.The outside of crystalline mother solution tank 1 is provided with Thermometer 8 and liquid level gauge 9.
The operation principle of the utility model:
Crystalline mother solution is entered by the first pipeline 3 in crystalline mother solution tank 1, is recycled sticky material and is deposited in crystalline mother solution tank 1 Tank bottom.Crystalline mother solution gets to mother liquor rectifying column by mother liquor delivery pump 6.Reclaimed materials reaches certain thickness in 1 tank of crystalline mother solution tank Afterwards, start to squeeze into tank bottom recovered material toward recycling kettle.Mother liquor is switched to another crystalline mother solution tank 1, is no longer fed, it will 1 pot liquid of crystalline mother solution tank gets to mother liquor rectifying column by mother liquor delivery pump 6, and until liquid does not go out, it is defeated to close mother liquor Pump 6 is sent, transfering material pump 4 is started.Start radial flow blender 2, recycling discharging, reclaimed materials is pushed to enter recycling by transfering material pump 4 and fill It sets.Using radial flow blender 2, reclaimed materials radially flows discharging, can discharge to avoid the movement of reclaimed materials in the axial direction More thoroughly.
The above is only the preferred embodiment of the utility model only, is not intended to limit the utility model, all at this Within the spirit and principle of utility model, any modification, equivalent replacement, improvement and so on should be included in the utility model Protection domain within.

Claims (9)

1. a kind of crystalline mother solution material recovering system, it is characterised in that:Including crystalline mother solution tank (1), the top of crystalline mother solution tank (1) Portion side is provided with feed inlet (101), and radial flow blender (2) is provided in the crystalline mother solution tank (1) of bottom, the bottom of close to It is provided with the sticky material discharge port (102) of recycling on crystalline mother solution tank (1) side wall in portion, recycles sticky material discharge port (102) and recycling It is provided with transfering material pump (4) on the first pipeline (3) of device connection, mother liquor is provided on crystalline mother solution tank (1) side wall of bottom It exports (103), mother liquor outlet (103) is connected to by the second pipeline (5) with mother liquor rectifying column, and the second pipeline is provided with mother on (5) Liquid delivery pump (6).
2. crystalline mother solution material recovering system according to claim 1, it is characterised in that:Charging at feed inlet (101) The crystalline mother solution tank (1) that pipe (11) is extend into close to crystalline mother solution tank (1) bottom is internal.
3. crystalline mother solution material recovering system according to claim 2, it is characterised in that:The lower port position of feed pipe (11) At the one third height of crystalline mother solution tank (1) inner cavity.
4. crystalline mother solution material recovering system according to any one of claims 1 to 3, it is characterised in that:Mother liquor outlet (103) height apart from crystalline mother solution tank (1) bottom, which is higher than, recycles sticky material discharge port (102) apart from crystalline mother solution tank (1) bottom The height in portion.
5. crystalline mother solution material recovering system according to any one of claims 1 to 3, it is characterised in that:Mother liquor delivery pump (6) it is connected to respectively with the refluxing opening (104) on mother liquor rectifying column, crystalline mother solution tank (1) by triplate line.
6. crystalline mother solution material recovering system according to any one of claims 1 to 3, it is characterised in that:Crystalline mother solution tank (1) nitrogen inlet (105) and offgas outlet (106) are additionally provided at the top of, nitrogen inlet (105) passes through pipeline and nitrogen pipeline Connection, offgas outlet (106) are connected to by pipeline with exhaust treatment system.
7. crystalline mother solution material recovering system according to any one of claims 1 to 3, it is characterised in that:Crystalline mother solution tank (1) outside is provided with thermometer (8) and liquid level gauge (9).
8. crystalline mother solution material recovering system according to any one of claims 1 to 3, it is characterised in that:Radial flow stirs The motor (201) of device (2) is located at the over top of crystalline mother solution tank (1).
9. crystalline mother solution material recovering system according to any one of claims 1 to 3, it is characterised in that:Mother liquor delivery pump (6) it is provided with filter (7) on the second pipeline (5) between mother liquor outlet (103).
CN201820013668.3U 2018-01-04 2018-01-04 A kind of crystalline mother solution material recovering system Active CN207871966U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820013668.3U CN207871966U (en) 2018-01-04 2018-01-04 A kind of crystalline mother solution material recovering system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820013668.3U CN207871966U (en) 2018-01-04 2018-01-04 A kind of crystalline mother solution material recovering system

Publications (1)

Publication Number Publication Date
CN207871966U true CN207871966U (en) 2018-09-18

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820013668.3U Active CN207871966U (en) 2018-01-04 2018-01-04 A kind of crystalline mother solution material recovering system

Country Status (1)

Country Link
CN (1) CN207871966U (en)

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