CN207857481U - The batch cleaning device of nuclear magnetic tube - Google Patents
The batch cleaning device of nuclear magnetic tube Download PDFInfo
- Publication number
- CN207857481U CN207857481U CN201721843245.6U CN201721843245U CN207857481U CN 207857481 U CN207857481 U CN 207857481U CN 201721843245 U CN201721843245 U CN 201721843245U CN 207857481 U CN207857481 U CN 207857481U
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- CN
- China
- Prior art keywords
- nuclear magnetic
- washer
- magnetic tube
- cleaning device
- liquid receptacle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000004140 cleaning Methods 0.000 title claims abstract description 67
- 239000007788 liquid Substances 0.000 claims abstract description 71
- 230000000740 bleeding effect Effects 0.000 claims abstract description 19
- 239000002699 waste material Substances 0.000 claims abstract description 4
- 239000002904 solvent Substances 0.000 claims description 42
- 238000005192 partition Methods 0.000 claims description 24
- 239000000284 extract Substances 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 238000012545 processing Methods 0.000 claims description 3
- 238000005086 pumping Methods 0.000 claims 1
- 230000005311 nuclear magnetism Effects 0.000 description 8
- 238000000034 method Methods 0.000 description 7
- 239000000463 material Substances 0.000 description 4
- 230000006378 damage Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000005481 NMR spectroscopy Methods 0.000 description 1
- 230000004308 accommodation Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 210000001550 testis Anatomy 0.000 description 1
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- Cleaning By Liquid Or Steam (AREA)
Abstract
The utility model provides a kind of batch cleaning device of nuclear magnetic tube, which includes：The liquid receptacle of cleaning waste liquid is received, and the washer being arranged on liquid receptacle；Liquid receptacle and washer integrated setting；Liquid receptacle includes bleeding point；Washer includes the first inlet, and the first communicating pipe in the first inlet, and the second communicating pipe of connection washer and liquid receptacle is arranged.The batch cleaning device of nuclear magnetic tube described in the utility model has the advantages that quick, efficient, batch cleaning nuclear magnetic tube.
Description
Technical field
The utility model is related to chemical apparatuses fields, and the cleaning device of more particularly to chemical apparatuses, are exactly specifically
A kind of batch cleaning device of nuclear magnetic tube.
Background technology
In the relevant research work of chemical classes, nuclear magnetic resonance technique is a kind of widely applied measuring technology, and nuclear-magnetism is total
The technology of shaking is that the nuclear magnetic tube equipped with sample is placed in magnet to be detected, very heavy to be provided for the structure elucidation of compound
The information wanted.After detection, need to clean nuclear magnetic tube, but nuclear magnetic tube pipe range, bore is small, and wall is thin frangible, clear
It is highly difficult when washing, and if cleaning is not thorough or cleaning way is improper, experimental result can all be had an impact.
Currently, the cleaning common method of nuclear magnetic tube is：One, Manual-cleaning, directly with solvent swab stick or brush insert
Enter in nuclear magnetic tube and is cleaned.This method is time-consuming and laborious, and is very easy to scratch nuclear magnetic tube；Two, it is cleaned by ultrasonic, nuclear-magnetism
Pipe is put into cleaning solution, is cleaned in ultrasonic cleaners, and this method cleaning is fast, but ultrasonic wave is be easy to cause to nuclear magnetic tube quartz
The destruction of lattice, long-time service can be such that nuclear magnetic tube damages, and influence nuclear magnetic tube testing result；Three, it is cleaned using existing nuclear magnetic tube
Device cleans, and cumbersome, washer itself needs to clean, and can only wash one or five nuclear magnetic tubes every time, time-consuming and laborious, and price is high
It is expensive.
There is an urgent need for research and development one kind not to damage nuclear magnetic tube by those skilled in the art, and efficiently, quickly, nuclear magnetic tube can be cleaned in batches
Cleaning device.
Invention content
To solve the above-mentioned problems, the utility model provides a kind of batch cleaning device of nuclear magnetic tube, the cleaning device packet
It includes：The liquid receptacle of cleaning waste liquid is received, and the washer on the liquid receptacle is set；The liquid receptacle and the cleaning
Device integrated setting；The liquid receptacle includes bleeding point；The washer includes the first inlet, is arranged in first feed liquor
First communicating pipe of mouth, and it is connected to the second communicating pipe of the washer and the liquid receptacle；Wherein, first communicating pipe
The washer can be connected to and be stored with the solvent bottle of solvent；The gas in the liquid receptacle is extracted by the bleeding point, from
And negative pressure is formed in the liquid receptacle and the washer, so that the solvent in the solvent bottle passes through first communicating pipe
Into the washer, the multiple nuclear magnetic tubes placed in the washer are cleaned.
In some embodiments, in the batch cleaning device of the nuclear magnetic tube, the washer further includes that top is opened
The lid of the tube body of mouth and the opening for being covered in the tube body.
In some embodiments, in the batch cleaning device of the nuclear magnetic tube, the tube body is contacted with the lid
Face is the contact surface of frosted processing.
In some embodiments, in the batch cleaning device of the nuclear magnetic tube, the washer further includes：Level is set
The partition board in the tubular body is set, multiple through-holes are offered on the partition board；Correspondence is fixed on the through-hole and sets the multiple of place
Hollow tube, for extracting solvent washing nuclear magnetic tube from the solvent bottle 1；Wherein, first inlet, the through-hole and described
Hollow tube is connected.
In some embodiments, in the batch cleaning device of the nuclear magnetic tube, the partition board upper surface and the lid
Height value of the value more than nuclear magnetic tube the distance between at the top of body；The height value of the hollow tube is more than the height value of nuclear magnetic tube.
In some embodiments, in the batch cleaning device of the nuclear magnetic tube, the partition board is interior with the tube body
Wall fitting setting.
In some embodiments, in the batch cleaning device of the nuclear magnetic tube, second communicating pipe is fixed on institute
The upper surface flush of one end and the partition board of washer is stated, the other end that second communicating pipe is fixed on the liquid receptacle is stretched
Enter inside the liquid receptacle.
In some embodiments, in the batch cleaning device of the nuclear magnetic tube, the other end of second communicating pipe
Extend to the lower part of the liquid receptacle.
In some embodiments, in the batch cleaning device of the nuclear magnetic tube, first is provided at the bleeding point
Vacuum cock；The bleeding point is opened in the top of the liquid receptacle.
In some embodiments, in the batch cleaning device of the nuclear magnetic tube, the lower part of the liquid receptacle also opens up
The the second vacuum cock for having the first liquid outlet and being arranged at first liquid outlet.
Advantageous effect：
1. in the batch cleaning device of nuclear magnetic tube described in the utility model, can be fixed on the lead to the hole site of partition board more
A nuclear magnetic tube can once clean more than ten even tens nuclear magnetic tubes, fast and efficiently batch cleaning nuclear magnetic tube simultaneously.
2. in the batch cleaning device of nuclear magnetic tube described in the utility model, in the operation that bleeding point is evacuated, utilizing
Negative pressure makes solvent flow and flush clean nuclear magnetic tube, and the batch cleaning device of nuclear magnetic tube described in the utility model, which has, not to be damaged
Hinder the high advantage of nuclear-magnetism tube wall, cleaning degree.
3. the batch cleaning device of nuclear magnetic tube described in the utility model is cheap, simple in structure, easy to operate, economical
Durable, cleaning efficiency is high, being capable of effectively auxiliary kernel Magnetic testi.
Description of the drawings
Fig. 1 is that the first structure of the batch cleaning device of the nuclear magnetic tube described in the one of embodiment of the utility model is shown
It is intended to；
Fig. 2 is the second structure in the batch cleaning device of the nuclear magnetic tube described in the one of embodiment of the utility model
Schematic diagram；
Fig. 3 is washer described in the batch cleaning device of the nuclear magnetic tube described in the one of embodiment of the utility model
The structural schematic diagram of middle partition board.
Reference sign
1 represents solvent bottle, and 2 represent liquid receptacle, and 22 represent bleeding point, and 23 represent the first vacuum cock, and 24, which represent first, goes out
Liquid mouth, 25 represent the second vacuum cock, and 3 represent washer, and 31 represent the first inlet, and 33 represent tube body, and 34 represent lid, and 35
Partition board is represented, 351 represent through-hole, and 36 represent hollow tube, and 4 represented for the first communicating pipe, and 5 represented for the second communicating pipe.
Specific implementation mode
The various exemplary embodiment of the utility model is now described in detail, which is not considered as to this practicality
Novel limitation, and it is understood as some aspects to the utility model, the more detailed description of characteristic and embodiment.
It should be understood that the term described in the utility model is only to describe special embodiment, it is not intended to limit this
Utility model.In addition, for the numberical range in the utility model, it is thus understood that specifically disclose the upper and lower bound of the range
And each median between them.Median and any other statement value in any statement value or stated ranges or
Smaller range is also included in the utility model each of between median in the range.On these are small range of
Limit and lower limit can be included or excluded independently in range.
Unless otherwise stated, all technical and scientific terms used herein has field described in the utility model
The normally understood identical meanings of those having ordinary skill in the art.Although the utility model only describes preferred method and material,
It can also be used in the implementation or test of the utility model and similar or equivalent any method and material described herein.This explanation
All documents mentioned in book are incorporated by reference into, to disclosure and description and the relevant method of the document and/or material.
When conflicting with any document being incorporated to, it is subject to the content of this specification.
It, can be to the specific implementation of the utility model specification without departing substantially from the scope of the utility model or spirit
Mode does a variety of improvement and variation, this will be apparent to those skilled in the art.Present specification and embodiment
It is merely exemplary.
It is the term of opening, i.e., about "comprising" used herein, " comprising ", " having ", " containing " etc.
Mean including but not limited to.
Any or all combinations about "and/or" used herein, including the things.
Below by way of specific implementation mode, and in conjunction with attached drawing, the utility model is described in further detail.
As shown in Figure 1, the utility model provides a kind of batch cleaning device of nuclear magnetic tube comprising：Receive cleaning waste liquid
Liquid receptacle 2, and the washer 3 that is arranged on the liquid receptacle 2；The liquid receptacle 2 is integrated with the washer 3 to be set
It sets；The liquid receptacle 2 includes bleeding point 22；The washer 3 includes the first inlet 31, is arranged in first inlet 31
The first communicating pipe 4, and the connection washer 3 and the liquid receptacle 2 the second communicating pipe 5；Wherein, first connection
Pipe 4 can be connected to the washer and be stored with the solvent bottle of solvent；The gas in the liquid receptacle 2 is extracted by the bleeding point 22
Body, to form negative pressure in the liquid receptacle 2 and the washer 3, so that solvent in the solvent bottle passes through described the
A connecting pipe 4 enters the washer 3, cleans the multiple nuclear magnetic tubes placed in the washer 3.
In the batch cleaning device using nuclear magnetic tube described in the utility model, one end of first communicating pipe 4 can
Dismounting is connected to first inlet 31, and the other end is inserted into the solvent bottle 1 for being stored with solvent, second communicating pipe 5,
3 integrated molding of the liquid receptacle 2 and the washer, and be seamlessly connected with the liquid receptacle 2 second communicating pipe 5, institute
It states and was seamlessly connected with the washer 3 the second communicating pipe 5；Aspiration pump is set in the bleeding point 22, liquid is connect in aspiration pump extraction
Air in device 2 extracts solvent in the solvent bottle 1 to form negative pressure in the liquid receptacle 2 and the washer 3, molten
Agent enters the washer 3 and under the action of negative pressure, and the nuclear magnetic tube in washer 3 described in solvent flush is completed to nuclear magnetic tube
Cleaning.The cleaning of nuclear magnetic tube is completed, and solvent slop is flow to by the second communicating pipe 5 in the liquid receptacle 2, easily and fast, efficiently
Complete the cleaning of multiple nuclear magnetic tubes in ground.
As shown in Fig. 2, the utility model provides a kind of batch cleaning device of nuclear magnetic tube, embodiment party shown in Fig. 1
On the basis of formula, further include：The washer 3 further includes the tube body 33 of upper opening and is covered in opening for the tube body 33
Lid 34 at mouthful；The tube body 33 and the contact surface that 34 contact surface of the lid is frosted processing.
The washer 3 includes the tube body 33 and the lid 34, convenient for placing and taking out nuclear magnetic tube.The nuclear magnetic tube
Batch cleaning device before cleaning nuclear magnetic tube, open the lid 34, nuclear magnetic tube be placed in the tube body 33, then
The lid of the lid 34 is bonded on the tube body 33, the tube body 33 and the contact surface of the lid 34 are ground contact surface,
The tube body 33 and 34 sealed set of the lid, it is ensured that the washer 3 constitutes closely sealed system.It is cleaned when completing nuclear magnetic tube
Afterwards, the lid 34 is being opened, the nuclear magnetic tube after taking out cleaning in the tube body 33.
In said program, it is further opened with the first liquid outlet 24 on the liquid receptacle 2 and is arranged in first liquid outlet 24
The second vacuum cock 25 at place；First liquid outlet 24 is located at the lower part of the liquid receptacle 2；It is collected when in the liquid receptacle 2
Solvent slop reach a certain height, i.e., solvent slop fills up the liquid receptacle 2, then opens the second vacuum cock 25, and solvent slop is from institute
It states and is flowed out in the first liquid outlet 24, first liquid outlet 24 is located at the lower part of the liquid receptacle 2, makes in the liquid receptacle 2
Solvent slop can all flow out.
In said program, the first vacuum cock 23 is provided at the bleeding point 22；The bleeding point 22 is opened in described
The top of liquid receptacle 2.The first vacuum cock 23 is opened, aspiration pump can extract the liquid receptacle 2 in the bleeding point 22
In air.The bleeding point 22 is located at the top of the liquid receptacle 2, and institute will not be blocked by collecting solvent slop in the liquid receptacle 2
Bleeding point 22 is stated, ensures that the bleeding point 22 can normally be evacuated work.
As shown in figure 3, a kind of batch cleaning device of nuclear magnetic tube is provided in the one of embodiment of the utility model,
Further include following technical characteristic on the basis of embodiment shown in fig. 1 or fig. 2：It is horizontally set on inside the tube body 33
Partition board 35, a multiple through-holes 351 are opened on the partition board 35；And it is fixed on multiple hollow tubes at 351 position of the through-hole
36, the hollow tube 36 extracts solvent washing nuclear magnetic tube from the solvent bottle；Wherein, first inlet 31, the through-hole
351 are connected to the hollow tube 36.
First inlet 31, the through-hole 351 and the hollow tube 36 form the circulation passage of solvent, by nuclear magnetic tube
Open Side Down is erected on the hollow tube 36, and under the action of negative pressure, the solvent gone out from the hollow tube 36 is directly from core
The opening of magnetic tube enters inside nuclear magnetic tube, and flush clean nuclear magnetic tube fast and efficiently completes the cleaning to nuclear magnetic tube.Different institutes
The size for stating tube body 33 and the partition board 35, opens up the through-hole 351 of different number on partition board 35, on each through-hole 351
One hollow tube 36 is set, the function of multiple nuclear magnetic tubes is realized while cleaning.
In said program, the partition board 35 is bonded setting with the inner wall of the tube body 33, and second communicating pipe 5 connects
Upper surface flush in one end of the washer 3 and the partition board 35, second communicating pipe 5 are connected to the liquid receptacle 2
The other end stretch into inside the liquid receptacle 2.Preferably, the other end of second communicating pipe 5 extends to the liquid receptacle 2
Lower part.The side wall of the partition board 35 is bonded setting with the inner wall of the tube body 33, and under the action of negative pressure, solvent is from solvent bottle 1
It sucks in washer 3, solvent enters hollow tube 36 from through-hole 351 and washes away the nuclear magnetic tube supported on hollow tube 36, solvent cleaning
Nuclear-magnetism bottom of the tube, then gap of the solvent between hollow tube outer wall and nuclear-magnetism inside pipe wall drop down onto on the partition board 35, clean core
Magnetic tube inner wall is finally located in second communicating pipe 5 of same level from the partition board 35, and passed through for the second communicating pipe
5 flow into liquid receptacle 2, complete the recycling to solvent slop.
In said program, height value of the distance between the partition board 35 and 34 top of the lid value more than nuclear magnetic tube；
The height value of the hollow tube 36 is more than the height value of nuclear magnetic tube.
When nuclear magnetic tube is erected on the hollow tube 36, the partition board 35 and 34 shape of the lid can be vertically arranged in
At accommodation space in, the outer diameter of the hollow tube 36 is less than the internal diameter of nuclear magnetic tube, the inner wall of hollow tube 36 not with nuclear magnetic tube
Inner wall contacts, and nuclear-magnetism inside pipe wall is cleaned convenient for solvent, meanwhile, the height value of the hollow tube 36 is more than the height value of nuclear magnetic tube,
The solvent gone out from the hollow tube 36 directly washes away nuclear-magnetism bottom of the tube, completes the cleaning to nuclear-magnetism bottom of the tube, completes to core
It is clear thoroughly to clean nuclear magnetic tube for the cleaning of magnetic tube bottom and inner wall.Further, a diameter of 2.5mm of the hollow tube 36~
3mm, height value are 170mm~200mm, and the distance value of the two neighboring hollow tube 36 is not less than 8mm.
The material of the liquid receptacle 2 and the washer 3 is corrosion-resistant glass.
It, can be to the specific implementation of the utility model specification without departing substantially from the scope of the utility model or spirit
Mode does a variety of improvement and variation, this will be apparent to those skilled in the art.By the specification of the utility model
Obtained other embodiment is apparent obtain for technical personnel.Present specification and embodiment are only exemplary
's.
Claims (10)
1. a kind of batch cleaning device of nuclear magnetic tube, which is characterized in that the cleaning device includes：Receive the liquid receptacle of cleaning waste liquid
(2), and washer (3) on the liquid receptacle (2) is set；The liquid receptacle (2) is integrated with the washer (3)
Setting；
The liquid receptacle (2) includes bleeding point (22)；
The washer (3) includes the first inlet (31), is arranged in the first communicating pipe (4) of first inlet (31),
And the second communicating pipe (5) of the connection washer (3) and the liquid receptacle (2)；
Wherein, first communicating pipe (4) can be connected to the washer (3) and be stored with the solvent bottle of solvent；Pass through the pumping
Gas port (22) extracts the gas in the liquid receptacle (2), negative to be formed in the liquid receptacle (2) and the washer (3)
Pressure cleans the cleaning so that the solvent in the solvent bottle enters the washer (3) by first communicating pipe (4)
The multiple nuclear magnetic tubes placed in device (3).
2. the batch cleaning device of nuclear magnetic tube according to claim 1, which is characterized in that the washer (3) further includes
The tube body (33) of upper opening and be covered in the tube body (33) opening lid (34).
3. the batch cleaning device of nuclear magnetic tube according to claim 2, which is characterized in that the tube body (33) and the lid
Body (34) contact surface is the contact surface of frosted processing.
4. the batch cleaning device of nuclear magnetic tube according to claim 3, which is characterized in that the washer (3) further includes：
It is horizontally set on the internal partition board (35) of the tube body (33), multiple through-holes (351) are offered on the partition board (35)；
The corresponding multiple hollow tubes (36) being fixed at the through-hole (351) position, for extracting solvent washing core from solvent bottle
Magnetic tube；
Wherein, first inlet (31), the through-hole (351) are connected with the hollow tube (36).
5. the batch cleaning device of nuclear magnetic tube according to claim 4, which is characterized in that partition board (35) upper surface with
Height value of the value more than nuclear magnetic tube the distance between at the top of the lid (34).
6. the batch cleaning device of nuclear magnetic tube according to claim 4, which is characterized in that the partition board (35) and the pipe
The inner wall fitting setting of body (33).
7. the batch cleaning device of nuclear magnetic tube according to claim 4, which is characterized in that second communicating pipe (5) sets
The upper surface flush in one end of the washer (3) and the partition board (35) is set, second communicating pipe (5) is arranged described
It is internal that the other end of liquid receptacle (2) stretches into the liquid receptacle (2).
8. the batch cleaning device of nuclear magnetic tube according to claim 7, which is characterized in that second communicating pipe (5)
The other end extends to the lower part of the liquid receptacle (2).
9. the batch cleaning device of nuclear magnetic tube according to claim 1, which is characterized in that be arranged at the bleeding point (22)
There is the first vacuum cock (23)；The bleeding point (22) is opened in the top of the liquid receptacle (2).
10. the batch cleaning device of nuclear magnetic tube according to claim 1, which is characterized in that the lower part of the liquid receptacle (2)
The the second vacuum cock (25) for being further opened with the first liquid outlet (24) and being arranged at first liquid outlet (24).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721843245.6U CN207857481U (en) | 2017-12-26 | 2017-12-26 | The batch cleaning device of nuclear magnetic tube |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721843245.6U CN207857481U (en) | 2017-12-26 | 2017-12-26 | The batch cleaning device of nuclear magnetic tube |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207857481U true CN207857481U (en) | 2018-09-14 |
Family
ID=63466632
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721843245.6U Expired - Fee Related CN207857481U (en) | 2017-12-26 | 2017-12-26 | The batch cleaning device of nuclear magnetic tube |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207857481U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113695304A (en) * | 2020-05-22 | 2021-11-26 | 兰州大学 | Nuclear magnetic pipe cleaner and cleaning method |
-
2017
- 2017-12-26 CN CN201721843245.6U patent/CN207857481U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113695304A (en) * | 2020-05-22 | 2021-11-26 | 兰州大学 | Nuclear magnetic pipe cleaner and cleaning method |
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180914 |