CN207805591U - A kind of reaction unit continuously produced - Google Patents
A kind of reaction unit continuously produced Download PDFInfo
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- CN207805591U CN207805591U CN201721882055.5U CN201721882055U CN207805591U CN 207805591 U CN207805591 U CN 207805591U CN 201721882055 U CN201721882055 U CN 201721882055U CN 207805591 U CN207805591 U CN 207805591U
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- liquid separation
- separation tank
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- point
- light component
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Abstract
A kind of reaction unit continuously produced, belongs to chemical equipment technical field.It is characterized in that:The reaction kettle(8)Discharge port connect liquid separation tank(1)Feed pipe(4);Liquid separation tank(1)Middle part be fixed with pre- point of slot(2), divide slot in advance(2)By liquid separation tank(1)It is divided into the light component chamber on top and the recombination sub-chamber on top;Divide slot in advance(2)Cross-sectional area be liquid separation tank(1)The 7/10 ~ 9/10 of cross-sectional area is to form liquid separation channel;The pre- point of slot(2)Depth be liquid separation tank(1)The 1/4 ~ 1/5 of tank body height;Liquid separation tank(1)Top be provided with light component delivery outlet(5), liquid separation tank(1)Bottom be provided with heavy constituent delivery outlet(6).The rate and composition for the mixing liquid that can be generated by reaction, control light component and heavy constituent continuously produces, and are monitored in real time without staff.
Description
Technical field
A kind of reaction unit continuously produced, belongs to chemical equipment technical field.
Background technology
The product after the completion of fields such as chemical industry are usually reacted is the mixture of two kinds of mutual exclusive liquid;In order to ensure
The basis storage and application of product often need that two kinds of mutual exclusive mixtures are carried out liquid separation in time.Current liquid separation equipment
It is varied, but be required for staff in most of simple gravity nature liquid separation equipment to observe two kinds of liquid in real time
Interface where liquid level, to prevent or reduce the mixing for occurring two kinds of liquid during liquid separation again.
Utility model content
The technical problems to be solved in the utility model is:It overcomes the deficiencies of the prior art and provide a kind of without monitoring boundary
The reaction unit continuously produced in face.
Technical solution adopted by the utility model to solve its technical problems is:The reaction unit continuously produced, including
Reaction kettle and liquid separation tank, it is characterised in that:The discharge port of the reaction kettle connects the feed pipe of the liquid separation tank;Point
Pre- point of slot is fixed in the middle part of flow container, the heavy constituent chamber for dividing slot that liquid separation tank is divided into the light component chamber and lower part on top in advance
Room;It is pre- that the cross-sectional area of slot is divided to be that the 7/10 ~ 9/10 of liquid separation tank cross-sectional area is connected to light component chamber and recombination to be formed
The liquid separation channel of sub-chamber;The depth of the pre- point of slot is the 1/4 ~ 1/5 of liquid separation tank height;The feed pipe of liquid separation tank
Outlet is located in pre- point of slot;The top of liquid separation tank is provided with light component delivery outlet, and the bottom of liquid separation tank is provided with heavy constituent delivery outlet.
The material that the utility model reacts completion in reaction kettle can be directly transported into the progress liquid separation of liquid separation tank, and be divided
Pre- point of slot is set in the tank body of flow container, what reaction kettle generated needs the mixing liquid of liquid separation to initially enter in pre- point of slot, is dividing in advance
Can be because the effect of gravity be tentatively layered in slot, the mixing liquid being tentatively layered can enter liquid separation channel together, subsequently into weight
Component chamber can be at liquid separation channel when the liquid level for recombinating the heavy constituent that sub-chamber saves bit by bit gradually reaches liquid separation channel middle
The more interfaces small relative to liquid separation tank cross section are formed, this interface area for allowing for liquid separation tank greatly reduces, temporarily
The total amount of unsegregated mixing liquid greatly reduces, and the mixing liquid being tentatively layered is easier to detach.Heavy constituent chamber
Room can be risen to if there is remaining light component on the bottom surface of pre- point of slot, due to whole pressure higher, it is easier to which separation is floated
Into liquid separation channel.It, will not counterweight component chamber and light component chamber because the mixed material newly entered is to be directly entered pre- point of slot
The liquid of room generates agitation, makes the sufficient standing separation of the indoor liquid of two chambers.Making can be spontaneous in the recombination sub-chamber of liquid separation tank
The pure heavies liquid of formation.The rate and composition for the mixing liquid that can be generated by reaction, control light component and heavy constituent
Continuous extraction, monitors in real time without staff.
The inclined bottom surface of the pre- point of slot, angle of inclination are 5 ° ~ 15 °.Divide the inclined bottom surface of slot that can promote light group in advance
Divide separation of floating, prevents the residual of light component.
At least side of the pre- point of slot is equipped with the baffle of plane, liquid separation as described between baffle and liquid separation top tank structure
Channel.The baffle of plane can form the overflow edge of waterfall form, ensure that the mixing liquid being tentatively layered preferably keeps being layered
State steadily enters liquid separation channel, enhances the liquid separation efficiency in liquid separation channel.
The light component delivery outlet and heavy constituent delivery outlet is opened in the opposite side in liquid separation channel.It reduces in liquid separation channel
Agitation of the liquid of flowing to exit weight component ensures standing separation effect.
The light component delivery outlet and heavy constituent delivery outlet is equipped with flow control valve.It can be by flow-rate adjustment, more
The interface of fast control weight component is in the height where liquid separation channel.
The liquid separation tank is vertical tank.
The top of the reaction kettle is equipped with reflux column.
Compared with prior art, advantageous effect possessed by a kind of reaction unit continuously produced of the utility model is:
Reacting the material of completion in reaction kettle when the utility model is used can directly transport into the progress liquid separation of liquid separation tank, and liquid separation
Set pre- point of slot in the tank body of tank, the meeting that reaction kettle generates forms small relative to liquid separation tank cross section more at liquid separation channel
Interface, this interface area for allowing for liquid separation tank greatly reduce, and the total amount of temporary unsegregated mixing liquid greatly reduces,
And the mixing liquid being tentatively layered is easier to detach.The mixed material newly entered is to be directly entered pre- point of slot, will not be right
The liquid for recombinating sub-chamber and light component chamber generates agitation, makes the sufficient standing separation of the indoor liquid of two chambers.It can pass through
The rate and composition of the mixing liquid generated are reacted, light component is controlled and heavy constituent continuously produces, it is real-time without staff
Monitoring.
Description of the drawings
Fig. 1 is a kind of schematic diagram of reaction unit continuously produced of the utility model.
Fig. 2 is a kind of main view Longitudinal cross section schematic of the liquid separation tank of reaction unit continuously produced of the utility model.
Fig. 3 is a kind of top cross section schematic diagram of the liquid separation tank of reaction unit continuously produced of the utility model.
Wherein, 1, liquid separation tank 2, divide slot 3, baffle 4, feed pipe 5, light component delivery outlet 6, heavy constituent delivery outlet in advance
7, reflux column 8, reaction kettle.
Specific implementation mode
Fig. 1 ~ 3 are the most preferred embodiments of the utility model, and 1 ~ 3 pair of the utility model is done furtherly below in conjunction with the accompanying drawings
It is bright.
With reference to attached drawing 1 ~ 3:A kind of reaction unit continuously produced of the utility model includes reaction kettle 8 and vertical liquid separation
The top of tank 1, reaction kettle 8 is equipped with reflux column 7, the feed pipe 4 of the discharge port connection liquid separation tank 1 of reaction kettle 8;In liquid separation tank 1
Portion is fixed with pre- point of slot 2, and slot 2 is divided to divide liquid separation tank 1 to the light component chamber for top and the recombination sub-chamber of lower part in advance;Pre- point
The side of slot 2 be equipped with plane baffle 3, divide in advance slot 2 cross-sectional area be 1 cross-sectional area of liquid separation tank 7/10 ~ 9/10 with
It forms connection light component chamber and recombinates the liquid separation channel of sub-chamber;Pre- divide that the depth of slot 2 is 1 tank body height of liquid separation tank 1/4 ~
1/5;The pre- inclined bottom surface for dividing slot 2, angle of inclination are 5 ° ~ 15 °;The outlet of the feed pipe 4 of liquid separation tank 1 is located in pre- point of slot 2;Point
The top of flow container 1 is provided with light component delivery outlet 5, and the bottom of liquid separation tank 1 is provided with heavy constituent delivery outlet 6, light component delivery outlet 5 and again
Component delivery outlet 6 is opened in the opposite side in liquid separation channel, and light component delivery outlet 5 and heavy constituent delivery outlet 6 are equipped with flow-rate adjustment
Valve.
Basic structure is fixed on 1 inner wall of liquid separation tank with shown in above-mentioned attached drawing 1,2, the circumference of pre- point of different slots 2 seals
On, liquid separation channel is 1/4 ~ 1/5 cylinder that fixed height is 1 tank body height of liquid separation tank on the bottom surface of pre- point of slot 2.
The course of work:What the reaction of reaction kettle 8 generated needs the pre- point of slot that the mixing liquid of liquid separation is directly entered in liquid separation tank 1
, can be because the effect of gravity be tentatively layered dividing in advance in slot 2 in 2, the mixing liquid being tentatively layered can enter liquid separation channel together,
Subsequently into recombination sub-chamber, when the liquid level for recombinating the heavy constituent that sub-chamber saves bit by bit gradually reaches liquid separation channel middle, meeting exists
The more interfaces small relative to liquid separation tank cross section are formed at liquid separation channel, the mixing liquid being tentatively layered further is divided
Layer.Remaining light component rises on the bottom surface of pre- point of slot 2 in recombination sub-chamber, due to whole pressure higher, it is easier to point
Enter liquid separation channel from floating.By the rate and composition of the mixing liquid of entrance, the extraction stream of light component and heavy constituent is controlled
Amount is continuously produced, and is monitored in real time without staff.
The above descriptions are merely preferred embodiments of the present invention, is not to make other forms to the utility model
Limitation, any person skilled in the art is changed or is modified as possibly also with the technology contents of the disclosure above equivalent
The equivalent embodiment of variation.But it is every without departing from the content of the technical scheme of the utility model, the technology according to the utility model is real
Any simple modification, equivalent variations and remodeling, still fall within the guarantor of technical solutions of the utility model made by confrontation above example
Protect range.
Claims (7)
1. a kind of reaction unit continuously produced, including reaction kettle(8)With liquid separation tank(1), it is characterised in that:The reaction kettle
(8)Discharge port connect the liquid separation tank(1)Feed pipe(4);The liquid separation tank(1)Middle part be fixed with pre- point of slot
(2), divide slot in advance(2)By liquid separation tank(1)It is divided into the light component chamber on top and the recombination sub-chamber of lower part;Divide slot in advance(2)Cross
Area of section is liquid separation tank(1)The 7/10 ~ 9/10 of cross-sectional area is to form connection light component chamber and recombinate point of sub-chamber
Liquid channel;The pre- point of slot(2)Depth be liquid separation tank(1)The 1/4 ~ 1/5 of tank body height;Liquid separation tank(1)Feed pipe(4)
Outlet be located at pre- point of slot(2)It is interior;Liquid separation tank(1)Top be provided with light component delivery outlet(5), liquid separation tank(1)Bottom be provided with
Heavy constituent delivery outlet(6).
2. a kind of reaction unit continuously produced according to claim 1, it is characterised in that:The pre- point of slot(2)'s
Inclined bottom surface, angle of inclination are 5 ° ~ 15 °.
3. a kind of reaction unit continuously produced according to claim 1, it is characterised in that:The pre- point of slot(2)'s
At least side is equipped with the baffle of plane(3), baffle(3)With liquid separation tank(1)Liquid separation channel described in being between inner wall.
4. a kind of reaction unit continuously produced according to claim 1, it is characterised in that:The light component delivery outlet
(5)With heavy constituent delivery outlet(6)It is opened in the opposite side in liquid separation channel.
5. a kind of reaction unit continuously produced according to claim 1, it is characterised in that:The light component delivery outlet
(5)With heavy constituent delivery outlet(6)It is equipped with flow control valve.
6. a kind of reaction unit continuously produced according to claim 1, it is characterised in that:The liquid separation tank(1)For
Vertical tank.
7. a kind of reaction unit continuously produced according to claim 1, it is characterised in that:The reaction kettle(8)'s
Top is equipped with reflux column(7).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201721882055.5U CN207805591U (en) | 2017-12-28 | 2017-12-28 | A kind of reaction unit continuously produced |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201721882055.5U CN207805591U (en) | 2017-12-28 | 2017-12-28 | A kind of reaction unit continuously produced |
Publications (1)
Publication Number | Publication Date |
---|---|
CN207805591U true CN207805591U (en) | 2018-09-04 |
Family
ID=63328171
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201721882055.5U Active CN207805591U (en) | 2017-12-28 | 2017-12-28 | A kind of reaction unit continuously produced |
Country Status (1)
Country | Link |
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CN (1) | CN207805591U (en) |
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2017
- 2017-12-28 CN CN201721882055.5U patent/CN207805591U/en active Active
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