CN207738731U - A kind of crude oil rectification systems - Google Patents
A kind of crude oil rectification systems Download PDFInfo
- Publication number
- CN207738731U CN207738731U CN201721686596.0U CN201721686596U CN207738731U CN 207738731 U CN207738731 U CN 207738731U CN 201721686596 U CN201721686596 U CN 201721686596U CN 207738731 U CN207738731 U CN 207738731U
- Authority
- CN
- China
- Prior art keywords
- reative cell
- tank body
- tank
- crude oil
- inlet pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000010779 crude oil Substances 0.000 title claims abstract description 51
- 238000004332 deodorization Methods 0.000 claims abstract description 31
- 239000003921 oil Substances 0.000 claims abstract description 14
- 238000000746 purification Methods 0.000 claims abstract description 8
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 37
- 229910052757 nitrogen Inorganic materials 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 14
- 239000007789 gas Substances 0.000 claims description 12
- 229910001873 dinitrogen Inorganic materials 0.000 claims description 7
- 238000004064 recycling Methods 0.000 claims description 7
- 239000008157 edible vegetable oil Substances 0.000 abstract description 16
- 238000001816 cooling Methods 0.000 abstract description 7
- 238000010525 oxidative degradation reaction Methods 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 4
- 239000012535 impurity Substances 0.000 description 12
- 235000019198 oils Nutrition 0.000 description 10
- 238000000034 method Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 3
- 238000007670 refining Methods 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 239000010775 animal oil Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000004781 supercooling Methods 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
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- Fats And Perfumes (AREA)
Abstract
The utility model discloses a kind of crude oil rectification systems, including crude oil tank, heating tank, centrifuge and deodorization tank, deodorization tank includes tank body, reative cell, overflow pipe, oil inlet pipe and air inlet pipe, short transverse of the reative cell in tank body is equipped with multiple, overflow pipe runs through reative cell and it is located at the height that head in purification tank is less than purification channel opening, the tail portion of overflow pipe extends to reative cell below, air inlet pipe is connected to across tank body with the bottom of reative cell, reative cell bottom in tank body positioned at bottom is communicated with flowline, flowline runs through the bottom of tank body, oil inlet pipe is communicated across tank body with the reative cell of the top in tank body.Crude oil overflow to reative cell below in reative cell carries out out that removing is smelly again, and crude oil flows out after the deodorization of multiple reative cells from the flowline of the reative cell of bottom, obtains the edible oil with expected property.Crude oil is less susceptible to that oxidative degradation occurs, and can improve the cooling effect of hot deodorization edible oil.
Description
Technical field
The utility model is related to crude oil refining techniques field, more particularly to a kind of crude oil rectification systems.
Background technology
Crude oil refers to being produced from animal or vegetable oil material, not by the primary oil of refining processing.Crude oil is due to processing work
Skill is simple, and this oil is impure more, oxidizable rotten, unsuitable long term storage.
Crude oil is flowed out from crude oil tank first in refining process, is gone using centrifuge after heating tank heats
Except impurity removes stink finally by deodorization tank.Wherein, deodorization mainly removes those in crude oil and is allowed to generate foreign odor and peculiar smell
Impurity.The impurity of removing generally includes free fatty;The compound for causing foreign odor and peculiar smell, such as aldehyde, ketone, alcohol and hydro carbons;With
The compound generated due to peroxide and pigment thermally decompose.These impurity, which should be removed fully just, can make edible oil have expection
Property.For example, the aliphatic acid in edible oil should substantially be reduced to about 0.1%-0.2%, it can just obtain that there is expected property
Edible oil.
Crude oil deodorization is typically in the presence of a kind of inert gas such as steam or nitrogen, under a high vacuum, in hot conditions
Lower progress.When inert stripping gas undesirable impurity of stripping from crude oil, hot conditions promote undesirable impurity
Thermal decomposition.High vacuum prevents oxidative degradation of the crude oil during deodorization.
Once deodorization is completed, the hot deodorization edible oil being formed by just is cooled.It is known at high temperature, deodorization eats oil pole
Oxidative degradation easily occurs.Therefore, by cooling, deodorization edible oil is made to be preferably minimized limit to the sensibility of oxidation.
Cooling usually carries out in a heat recovery units, and hot deodorization edible oil provides under vacuum at this time.Heat
Recovery unit can be the important component that may not be deodorizing apparatus, its operation be in order to by using wait for deodorization into
Crude oil is expected as indirect cooling way, from just recycling heat in the deodorization edible oil of blowdown.Heat is recycled by using crude oil,
The deodorization edible oil of heat can reach the desired temperature for being respectively adapted to storage and deodorization with crude oil simultaneously.However, using a kind of
Pipe-the shell heat exchanger commonly used is come to reach above-mentioned purpose be particularly undesirable, because being usually the pressure drop overcome in heat exchanger
And the outer mechanical pump needed may cause gas leakage, to make the hot deodorization edible oil oxidation under vacuum.
Therefore, it is desirable that finding the method that deodorization eats oil-proofness that can improve, that is, it is less susceptible to that oxidative degradation occurs,
And the method that the cooling effect of hot deodorization edible oil can be improved.
Utility model content
The purpose of this utility model is to provide a kind of crude oil rectification systems, is less susceptible to that oxidative degradation occurs, and can improve
The cooling effect of hot deodorization edible oil.
The above-mentioned technical purpose of the utility model technical scheme is that:
A kind of crude oil rectification systems, including crude oil tank, heating tank, centrifuge and deodorization tank, the deodorization tank include tank body,
Reative cell, overflow pipe, oil inlet pipe and air inlet pipe, short transverse of the reative cell in tank body are equipped with multiple, the overflow pipe
Through the reative cell and its be located at the height of head in purification tank less than purification channel opening, the tail portion of the overflow pipe extends to
Reative cell below, the air inlet pipe are connected to across the tank body with the bottom of the reative cell, are located at most in the tank body
The reative cell bottom of lower section is communicated with flowline, and the flowline runs through the bottom of the tank body, and the oil inlet pipe passes through tank body
It is communicated with the reative cell of the top in tank body.
By using above-mentioned technical proposal, the reative cell of oil inlet pipe the top out of tank body flows into, while passing through air inlet pipe
The nitrogen being passed through.When the undesirable impurity of nitrogen stripping from crude oil, and heat exchange is carried out with the crude oil of heat, reduces crude oil
Temperature, can prevent crude oil from going out smelly period oxygenolysis to a certain extent.Crude oil overflow in reative cell is to below
Reative cell carries out out that removing is smelly again, and crude oil is after the deodorization of multiple reative cells from the flowline stream of the reative cell of bottom
Go out, obtains the edible oil with expected property.
Further, the air inlet pipe is located at the part of reative cell and is communicated with isocon, the isocon and the air inlet
For the horizontal and circumferential permutation of pipe in the air inlet pipe, the isocon is equipped with several stomatas.
By using above-mentioned technical proposal, gas can uniformly be diffused into the crude oil of reative cell, makes by the setting of isocon
The stripping of crude oil is more abundant.
Further, the one end of the air inlet pipe far from tank body is connected to nitrogen gas tank, and the air inlet pipe is equipped with air valve.
By using above-mentioned technical proposal, air valve can control the flow velocity of the nitrogen exported in nitrogen gas tank.
Further, drier is equipped in the air inlet pipe between nitrogen gas tank and air valve.
By using above-mentioned technical proposal, drier can remove the moisture in nitrogen, avoid the impurity in moisture and moisture
It brings into crude oil.
Further, the tank base is communicated with blowdown pipe, and the blowdown pipe lower end is connected to blow down container.
By using above-mentioned technical proposal, the material flowed out in reative cell in tank body can be discharged in discharge duct.
Further, the top of the tank is communicated with the first vacuum pump, the gas outlet connection condensation of first vacuum pump
Device, the liquid outlet of the condenser are connected to condensate liquid recycling can, and the gas outlet of the condenser is connected to the second vacuum pump, and described the
The gas outlet of two vacuum pumps is communicated with outside air.
By using above-mentioned technical proposal, the nitrogen being discharged out of tank body obtains condensate liquid by condenser, condenses liquid stream
Enter the impurity that condensate liquid recycling can avoid in condensate liquid to be discharged directly to the external world and cause environmental pollution, by condensed nitrogen
Outside air is then immediately discharged to by the second vacuum pump.
In conclusion the utility model has the advantages that:The reative cell of oil inlet pipe the top out of tank body flows into,
The nitrogen being passed through simultaneously by air inlet pipe.When the undesirable impurity of nitrogen stripping from crude oil, and carried out with the crude oil of heat
Heat exchange reduces the temperature of crude oil, can prevent crude oil from going out smelly period oxygenolysis to a certain extent.Crude oil in reative cell
Overflow to reative cell below carries out out that removing is smelly again, and crude oil is after the deodorization of multiple reative cells from the reaction of bottom
The flowline of room flows out, and obtains the edible oil with expected property.Crude oil is less susceptible to that oxidative degradation occurs, and can improve heat and remove
The cooling effect of smelly edible oil.
Description of the drawings
Fig. 1 is the system schematic of the utility model embodiment;
Fig. 2 is the structural schematic diagram of the utility model embodiment deodorization tank;
Fig. 3 is the structural schematic diagram of the utility model embodiment air inlet pipe and isocon.
In figure, 1, crude oil tank;2, heating tank;3, centrifuge;4, deodorization tank;401, tank body;402, reative cell;403, overflow
Pipe;404, oil inlet pipe;405, air inlet pipe;406, flowline;407, isocon;408, stomata;409, nitrogen gas tank;410, air valve;
411, drier;412, blowdown pipe;413, blow down container;414, the first vacuum pump;415, condenser;416, condensate liquid recycling can;
417, the second vacuum pump.
Specific implementation mode
The utility model is described in further detail below in conjunction with attached drawing.
This specific embodiment is only the explanation to the utility model, is not limitations of the present invention, ability
Field technique personnel can as needed make the present embodiment the modification of not creative contribution after reading this specification, but
As long as within the protection scope of the present utility model all protected by Patent Law.
A kind of crude oil rectification systems, as shown in Figure 1, including crude oil tank 1, heating tank 2, centrifuge 3 and deodorization tank 4.
As shown in Fig. 2, deodorization tank 4 includes tank body 401, reative cell 402, overflow pipe 403, oil inlet pipe 404 and air inlet pipe
405, short transverse of the reative cell 402 in tank body 401 be equipped with it is multiple, in the present embodiment, there are four reative cells 402.Overflow
Pipe 403 runs through reative cell 402 and it is located at the height that head in purification tank is less than purification channel opening, and the tail portion of overflow pipe 403 is prolonged
Reative cell 402 below is extended to, air inlet pipe 405 is connected to the bottom of reative cell 402 across tank body 401, is located in tank body 401
402 bottom of reative cell of bottom is communicated with flowline 406, and flowline 406 runs through the bottom of tank body 401, and oil inlet pipe 404 passes through
Tank body 401 is communicated with the reative cell 402 of the top in tank body 401.
401 bottom of tank body is communicated with blowdown pipe 412, and the object flowed out in reative cell 402 in tank body 401 can be discharged in discharge duct
Material.412 lower end of blowdown pipe is connected to blow down container 413.
As shown in figure 3, more abundant in order to make nitrogen contact with the crude oil in reative cell 402, air inlet pipe 405 is located at reaction
The part of room 402 is communicated with isocon 407, and isocon 407, in air inlet pipe 405, divides with the horizontal and circumferential permutation of air inlet pipe 405
Flow tube 407 is equipped with several stomatas 408.
Air inlet pipe 405 is communicated with nitrogen gas tank 409, and in order to adjust the air velocity of nitrogen, air valve is provided in air inlet pipe 405
410.Air inlet pipe 405 between air valve 410 and nitrogen gas tank 409 is equipped with drier 411, can remove the moisture in nitrogen, avoids
Impurity in moisture and moisture is brought into crude oil.
401 top of tank body is communicated with the first vacuum pump 414, and the gas outlet of the first vacuum pump 414 is connected to condenser 415, cold
The liquid outlet connection condensate liquid recycling can 416 of condenser 415, the gas outlet of condenser 415 are connected to the second vacuum pump 417, and second is true
The gas outlet of sky pump 417 is communicated with outside air.The nitrogen being discharged in from tank body 401 obtains condensate liquid by condenser 415, cold
Lime set, which flows into the impurity that condensate liquid recycling can 416 can avoid in condensate liquid and is discharged directly to the external world, causes environmental pollution, through supercooling
Nitrogen after solidifying is then immediately discharged to outside air by the second vacuum pump 417.
Claims (6)
1. a kind of crude oil rectification systems, including crude oil tank (1), heating tank (2), centrifuge (3) and deodorization tank (4), it is characterized in that:
The deodorization tank (4) includes tank body (401), reative cell (402), overflow pipe (403), oil inlet pipe (404) and air inlet pipe (405),
Short transverse of the reative cell (402) in tank body (401) be equipped with it is multiple, the overflow pipe (403) run through the reative cell
(402) and it is located at the height that head in purification tank is less than purification channel opening, and the tail portion of the overflow pipe (403) extends under it
The reative cell (402) of side, the air inlet pipe (405) are connected to across the tank body (401) with the bottom of the reative cell (402),
Reative cell (402) bottom in the tank body (401) positioned at bottom is communicated with flowline (406), and the flowline (406) is passed through
The bottom of the tank body (401) is worn, the oil inlet pipe (404) passes through the reative cell of tank body (401) and tank body (401) interior the top
(402) it communicates.
2. a kind of crude oil rectification systems according to claim 1, it is characterized in that:The air inlet pipe (405) is located at reative cell
(402) part is communicated with isocon (407), the isocon (407) and the horizontal and circumferential permutation of the air inlet pipe (405) in
On the air inlet pipe (405), the isocon (407) is equipped with several stomatas (408).
3. a kind of crude oil rectification systems according to claim 1, it is characterized in that:The air inlet pipe (405) is far from tank body
(401) one end connection nitrogen gas tank (409), the air inlet pipe (405) are equipped with air valve (410).
4. a kind of crude oil rectification systems according to claim 3, it is characterized in that:It is located at nitrogen on the air inlet pipe (405)
Drier (411) is equipped between tank (409) and air valve (410).
5. a kind of crude oil rectification systems according to claim 1, it is characterized in that:Tank body (401) bottom, which is communicated with, lets out
Expects pipe (412), blowdown pipe (412) the lower end connection blow down container (413).
6. a kind of crude oil rectification systems according to claim 1, it is characterized in that:The is communicated at the top of the tank body (401)
One vacuum pump (414), the gas outlet connection condenser (415) of first vacuum pump (414), condenser (415) go out
Liquid mouth connection condensate liquid recycling can (416), gas outlet the second vacuum pump of connection (417) of the condenser (415), described second
The gas outlet of vacuum pump (417) is communicated with outside air.
Priority Applications (1)
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CN201721686596.0U CN207738731U (en) | 2017-12-06 | 2017-12-06 | A kind of crude oil rectification systems |
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CN201721686596.0U CN207738731U (en) | 2017-12-06 | 2017-12-06 | A kind of crude oil rectification systems |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109234009A (en) * | 2018-11-23 | 2019-01-18 | 宁夏泰和成食品科技有限公司 | The crude oil method of purification of edible oil |
CN113617052A (en) * | 2021-07-19 | 2021-11-09 | 茂名海和石油化工有限公司 | Stripping oil refining process using nitrogen as gas source |
-
2017
- 2017-12-06 CN CN201721686596.0U patent/CN207738731U/en not_active Expired - Fee Related
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109234009A (en) * | 2018-11-23 | 2019-01-18 | 宁夏泰和成食品科技有限公司 | The crude oil method of purification of edible oil |
CN113617052A (en) * | 2021-07-19 | 2021-11-09 | 茂名海和石油化工有限公司 | Stripping oil refining process using nitrogen as gas source |
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Granted publication date: 20180817 |