CN207709025U - A kind of device of continous way speed up gas and liquid reaction - Google Patents
A kind of device of continous way speed up gas and liquid reaction Download PDFInfo
- Publication number
- CN207709025U CN207709025U CN201721500775.0U CN201721500775U CN207709025U CN 207709025 U CN207709025 U CN 207709025U CN 201721500775 U CN201721500775 U CN 201721500775U CN 207709025 U CN207709025 U CN 207709025U
- Authority
- CN
- China
- Prior art keywords
- cooling tank
- gas
- pipe
- helix tube
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 22
- 238000001816 cooling Methods 0.000 claims abstract description 31
- 239000000463 material Substances 0.000 claims abstract description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 230000001105 regulatory effect Effects 0.000 claims description 9
- 230000004888 barrier function Effects 0.000 claims description 4
- 239000011344 liquid material Substances 0.000 abstract description 10
- 239000000498 cooling water Substances 0.000 abstract description 5
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 8
- 229910052801 chlorine Inorganic materials 0.000 description 8
- 239000000460 chlorine Substances 0.000 description 8
- 150000002576 ketones Chemical class 0.000 description 6
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000001133 acceleration Effects 0.000 description 1
- 150000001263 acyl chlorides Chemical class 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a kind of devices of continous way speed up gas and liquid reaction, including cooling tank, helix tube in cooling tank and the feed pipe and discharge nozzle being connect with helix tube, the sidewall bottom of cooling tank offers circulating water intake, the top side wall of cooling tube is equipped with circulating water outlet, the bottom of helix tube is equipped with material inlet, one end of feed pipe is stretched at the top of cooling tank and is connected to material inlet, the other end of feed pipe is connected to the gentle body expects pipe of liquid expects pipe respectively by three-way pipe, the top of helix tube is equipped with material outlet, discharge nozzle is stretched at the top of cooling tank and is connected to material outlet.The time of contact for thereby increasing gas material and liquid material enables reaction fully completely, and saves space, and cooling water is reaction cooling immediately in cooling tank, while improving reaction efficiency, in turn ensures the security performance of reaction.
Description
Technical field
The utility model belongs to the device field for accelerating reaction, is more particularly to a kind of acceleration gas material and liquid material
The device of reaction.
Background technology
Mixture after the reaction of benzene and acyl chlorides is thick ketone, and thick ketone also needs further to be reacted with chlorine.Existing use
In accelerating the device of thick ketone and chlorine reaction rate to be to be passed directly into a straight tube distributor in reaction kettle, chlorine is from distributor
It spills into reaction kettle, the chlorine spilt into reaction kettle is reacted with material.
The chlorine direct current time in this structure is too short, and chlorine and reacting for thick ketone are incomplete.In order to increase thick ketone and chlorine
The time of contact of gas and contact area, are often added agitating device in a kettle.But it again can not be complete after agitating device is added
All risk insurance demonstrate,proves the leakproofness of reaction kettle, causes security risk.
Utility model content
The purpose of this utility model is to provide one kind and may make chlorine and the complete continous way speed up gas and liquid of thick reactive ketone anti-
The device answered.
One side according to the present utility model provides a kind of device of continous way speed up gas and liquid reaction, including cooling
Tank, the helix tube in the cooling tank and the feed pipe and discharge nozzle being connect with the helix tube,
The sidewall bottom of the cooling tank offers circulating water intake, and the top side wall of the cooling tank goes out equipped with recirculated water
Mouthful,
The bottom of the helix tube is equipped with material inlet, and one end of the feed pipe is stretched into simultaneously at the top of the cooling tank
It being connected to the material inlet, the other end of the feed pipe is connected to the gentle body expects pipe of liquid expects pipe respectively by three-way pipe,
The top of the helix tube be equipped with material outlet, the discharge nozzle stretched at the top of the cooling tank and with the material outlet
Connection.
The time of contact for thereby increasing gas material and liquid material enables reaction fully completely, and saves sky
Between, cooling water is reaction cooling immediately in cooling tank, while improving reaction efficiency, in turn ensures the security performance of reaction.
In some embodiments, the helix tube includes Raschig ring pipe, filled with multiple drawings west in the Raschig ring pipe
Ring, the both ends of the Raschig ring pipe are equipped with the barrier web plate for limiting the Raschig ring.Raschig ring pipe can further increase gas
The contact area and time of contact of body material and liquid material so that more abundant, the raising reaction efficiency of gas-liquid contact.
In some embodiments, the spacing between each layer tube body of the helix tube is 50-100mm.Spacing is excessive to touch
It is bad to hit effect, the too small collision efficiency of spacing is high, but temperature is but difficult to control, and is easy to cause safety accident, spacing is controlled
It in 50-100mm, can not only ensure the efficiency of reaction, but also can ensure the safety of reaction.
In some embodiments, the liquid expects pipe is equipped with the first regulating valve, and the gas expects pipe is equipped with second
Regulating valve.By the proportioning of the first regulating valve and the controllable gas material and liquid material entered of the second regulating valve, ensure gas
The abundant reaction of body material and liquid material.
In some embodiments, flowmeter is equipped at the material inlet.Inlet flow rate can be set according to flowmeter
Size.
Description of the drawings
Fig. 1 is a kind of structural schematic diagram of the device of continous way speed up gas and liquid reaction of one embodiment of the utility model.
Specific implementation mode
Fig. 1 schematically illustrates a kind of device of the continous way speed up gas and liquid reaction of embodiment of the utility model.
As shown in Fig. 1, the continous way speed up gas and liquid reaction device include cooling tank 1, the helix tube 2 in cooling tank 1 and with
The feed pipe 3 and discharge nozzle 4 that helix tube 2 connects.The sidewall bottom of cooling tank 1 offers circulating water intake 11, the side of cooling tank
Circulating water outlet 12 is equipped at the top of wall.Cooling water enters from circulating water intake 11 in cooling tank 1, is flowed out from circulating water outlet 12,
Helix tube 2 is immersed in cooling water, plays the role of cooling.The bottom of helix tube 2 is equipped with material inlet, one end of feed pipe 3 from
The top of cooling tank 1 is stretched into and is connected to material inlet, the other end of feed pipe 3 by three-way pipe 5 respectively with liquid expects pipe 61
It is connected to gas expects pipe 62, the top of helix tube 2 is equipped with material outlet, and discharge nozzle 4 is stretched into from the top of cooling tank 1 and and material
Outlet.The time of contact for thereby increasing gas material and liquid material enables reaction fully completely, and saves sky
Between, cooling water is reaction cooling immediately in cooling tank 1, while improving reaction efficiency, in turn ensures the security performance of reaction.
In this embodiment, helix tube 2 includes Raschig ring pipe 21, and Raschig ring pipe 21 is located at the middle part of helix tube.Raschig ring
Multiple Raschig rings 22 are filled in pipe 21.The both ends of Raschig ring pipe 21 are equipped with the barrier web plate 23 for limiting Raschig ring.Draw west
Endless tube 21 can further increase contact area and the time of contact of gas material and liquid material so that gas-liquid contact more fills
Point, improve reaction efficiency.Barrier net 23 can both play the role of fixed Raschig ring 22, be also convenient for passing through for material.Spiral shell
Spacing between each layer tube body of coil 2 is 50-100mm.The excessive collision effect of spacing is bad, and the too small collision efficiency of spacing is high,
But temperature is but difficult to control, and is easy to cause safety accident, spacing is controlled to the effect that can both ensure reaction in 50-100mm
Rate, and can ensure the safety of reaction.Liquid expects pipe 61 is equipped with the first regulating valve 611, and gas expects pipe 62 is equipped with second and adjusts
Save valve 621.It can control the proportioning of the gas material and liquid material that enter by the first regulating valve 611 and the second regulating valve 621,
Ensure the abundant reaction of gas material and liquid material.Flowmeter is equipped at material inlet.Inlet flow can be set according to flowmeter
The size of amount.
Above-described is only some embodiments of the utility model.For those of ordinary skill in the art, exist
Under the premise of not departing from the concept of the present invention, various modifications and improvements can be made, it is new that these belong to this practicality
The protection domain of type.
Claims (5)
1. a kind of device of continous way speed up gas and liquid reaction, which is characterized in that the spiral shell including cooling tank, in the cooling tank
Coil and the feed pipe and discharge nozzle being connect with the helix tube,
The sidewall bottom of the cooling tank offers circulating water intake, top side wall be equipped with circulating water outlet,
The bottom of the helix tube be equipped with material inlet, one end of the feed pipe stretched at the top of the cooling tank and with institute
Material inlet connection is stated, the other end of the feed pipe is connected to the gentle body expects pipe of liquid expects pipe respectively by three-way pipe, described
The top of helix tube is equipped with material outlet, and the discharge nozzle stretches at the top of the cooling tank and connects with the material outlet
It is logical.
2. the device of continous way speed up gas and liquid reaction according to claim 1, which is characterized in that the helix tube includes drawing
Western endless tube, the Raschig ring pipe is interior to be filled with multiple Raschig rings, and the both ends of the Raschig ring pipe are equipped with for limiting the drawing west
The barrier web plate of ring.
3. the device of continous way speed up gas and liquid reaction according to claim 1, which is characterized in that each layer of the helix tube
Spacing between tube body is 50-100mm.
4. the device of continous way speed up gas and liquid reaction according to claim 1, which is characterized in that set in the liquid expects pipe
There are the first regulating valve, the gas expects pipe to be equipped with the second regulating valve.
5. the device of continous way speed up gas and liquid reaction according to claim 1, which is characterized in that set at the material inlet
There is flowmeter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721500775.0U CN207709025U (en) | 2017-11-10 | 2017-11-10 | A kind of device of continous way speed up gas and liquid reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721500775.0U CN207709025U (en) | 2017-11-10 | 2017-11-10 | A kind of device of continous way speed up gas and liquid reaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207709025U true CN207709025U (en) | 2018-08-10 |
Family
ID=63061193
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721500775.0U Expired - Fee Related CN207709025U (en) | 2017-11-10 | 2017-11-10 | A kind of device of continous way speed up gas and liquid reaction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207709025U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107670594A (en) * | 2017-11-10 | 2018-02-09 | 大丰鑫源达化工有限公司 | A kind of device of continous way speed up gas and liquid reaction |
-
2017
- 2017-11-10 CN CN201721500775.0U patent/CN207709025U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107670594A (en) * | 2017-11-10 | 2018-02-09 | 大丰鑫源达化工有限公司 | A kind of device of continous way speed up gas and liquid reaction |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180810 |