CN207708557U - A kind of rectifier unit producing organic high purity reagent - Google Patents
A kind of rectifier unit producing organic high purity reagent Download PDFInfo
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- CN207708557U CN207708557U CN201721795232.6U CN201721795232U CN207708557U CN 207708557 U CN207708557 U CN 207708557U CN 201721795232 U CN201721795232 U CN 201721795232U CN 207708557 U CN207708557 U CN 207708557U
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Abstract
The utility model discloses a kind of rectifier units producing organic high purity reagent, including casing assembly, heating component, transmission assembly, transmission assembly, separation assembly, reflux assembly, condensation, gas-liquid separation component and collection assembly, the casing assembly includes discharge nozzle, motor, electrothermal tube, rectifying still, outer courage, recycle feed pipe, distillation cascade, supporting rack and agitating shaft；Rectifier unit uses dumped packing rectifying column, use specification for two to ten millimeters of θ ring fillers, the theoretical cam curve of every meter of dumped packing rectifying column is ten five to two ten, rectifying column effective height can be down to 1. 5 to 2 meter, greatly reduce the construction cost in rectifying workshop, corresponding dumped packing rectifying column is only needed to change when more new varieties, on-line cleaning need not be carried out again, a large amount of manpower, financial resources and material resources can be saved, the construction of 20 dumped packing rectifying column parallel connections simultaneously, can reach the single concatenated yield of major diameter tower section.
Description
Technical field
The utility model belongs to technical field of rectification, and in particular to a kind of rectifier unit producing organic high purity reagent.
Background technology
Rectifying is using a kind of separation process that each component volatility in mixture is different and is detached each component, often
Equipment has plate distillation column and stuffing rectification column.The principle and equipment flowsheet of precise distillation are identical as conventional distillation, only
The relative volatility between component in material to be separated system is smaller, thus uses high-efficiency and precision filler to realize point of component to be separated
From purification.
When original Organic chemical solvents class reagent rectification and purification, generally use tower diameter is less than or equal to 300 millimeters of rule
Whole packed tower, because regular packed tower has many advantages, such as that pressure drop is low, operating flexibility is high, mass transfer effect is good, but regular packed tower is every
Rice theoretical cam curve be generally less than five, for reach purity 99 points nine or more percent high purity reagent working condition, it is past
Toward effective tower height at ten to ten five meters or more, and since chemical reagent has small lot multi items characteristic, lead to regular packed tower
It is difficult to carry out on-line cleaning when more new varieties, general 15 meters or more of regular packed tower cleaning frequency at five to seven days, is given and uses
Person makes troubles.
Utility model content
The purpose of this utility model is to provide a kind of rectifier units producing organic high purity reagent, to solve above-mentioned background
When proposing original Organic chemical solvents class reagent rectification and purification in technology, generally use tower diameter is less than or equal to 300 millimeters
Regular packed tower, because regular packed tower has many advantages, such as that pressure drop is low, operating flexibility is high, mass transfer effect is good, but regular packed tower
Every meter of theoretical cam curve is generally less than five, for reach purity 99 points nine or more percent high purity reagent working condition,
Often effective tower height leads to structured packing at ten to ten five meters or more, and since chemical reagent has small lot multi items characteristic
Be difficult to carry out on-line cleaning when tower more new varieties, general 15 meters or more of regular packed tower cleaning frequency at five to seven days, to making
The problem of user makes troubles.
To achieve the above object, the utility model provides the following technical solutions：A kind of rectifying producing organic high purity reagent
Device, including casing assembly, heating component, transmission assembly, transmission assembly, separation assembly, reflux assembly, condensation, gas-liquid
Separation assembly and collection assembly, the casing assembly include discharge nozzle, motor, electrothermal tube, rectifying still, outer courage, recycle feed pipe,
Distillation cascade, supporting rack and agitating shaft, the rectifying still is located at the upper surface of support frame as described above, and fixes and connect with support frame as described above
It connects, the lateral wall of the rectifying still is fixedly connected with the outer courage, and the inside of the outer courage is equipped with the electrothermal tube, the electrothermal tube
It is fixedly connected with the rectifying still, the bottom end of the rectifying still is equipped with the motor, and the output end of the motor is fixedly connected with institute
Agitating shaft is stated, the right side of the motor is equipped with the discharge nozzle, and the discharge nozzle is fixedly connected with the rectifying still, the rectifying
The top of kettle is fixedly connected with the distillation cascade, and the right side of the distillation cascade is equipped with the recycle feed pipe, the recycle feed pipe
It is fixedly connected with the rectifying still, the motor and the electrothermal tube are electrically connected with external power supply, the heating component packet
Include cycle discharge nozzle, heat source import and heater, the right side of the rectifying still is equipped with the heater, the heater with it is described
Supporting rack is fixedly connected, and the cycle discharge nozzle is located at the top of the heater, and is fixedly connected with the heater, described
Cycle discharge nozzle is fixedly connected with the recycle feed pipe by pipeline, and the left surface of the heater is fixedly connected with the heat source
Import, the heater and external power supply are electrically connected, the transmission assembly include circulating pump feed pipe, circulating pump discharge nozzle and
The lower section of circulating pump, the heater is equipped with the circulating pump, and the circulating pump is fixedly connected with support frame as described above, the cycle
The circulating pump discharge nozzle is fixedly connected at the top of pump, the circulating pump discharge nozzle, which is fixed with the heat source import by pipeline, to be connected
It connects, the left surface of the circulating pump is fixedly connected with the circulating pump feed pipe, and the circulating pump feed pipe is logical with the discharge nozzle
Piping is fixedly connected, and the separation assembly includes rectifying discharge nozzle, dumped packing rectifying column, mounting box and the radical material of rectifying
The top of pipe, the rectifying still is equipped with the mounting box, and the mounting box is fixedly connected with support frame as described above, the mounting box
Madial wall is fixedly connected with the dumped packing rectifying column, and it is radical that the bottom end of the dumped packing rectifying column is fixedly connected with the rectifying
Expects pipe, the radical expects pipe of rectifying are fixedly connected with the distillation cascade, and the top of the dumped packing rectifying column is fixedly connected with institute
State rectifying discharge nozzle, the reflux assembly includes return duct, flow back into expects pipe, return channel and reflux discharge nozzle, the mounting box
Left side above be equipped with the return channel, the return channel is fixedly connected with support frame as described above, and the top of the return channel is fixed
Expects pipe is flowed back into described in connection, the expects pipe that flows back into is fixedly connected with the rectifying discharge nozzle by pipeline, the return duct
It is fixedly connected positioned at the right surface of the return channel, and with the return channel, the bottom end of the return channel is fixedly connected with described return
Expects pipe is flowed out, the condensation includes condensation inlet tube, condenser and condensate outlet pipe, and the lower section of the return channel is equipped with institute
It states condensate outlet pipe to be fixedly connected with support frame as described above equipped with the condensate outlet pipe, institute is fixedly connected at the top of the condenser
Condensation inlet tube is stated, the condensation inlet tube is fixedly connected with the reflux discharge nozzle by pipeline, the following table of the condenser
Face is fixedly connected with the condensate outlet pipe, and the condenser is electrically connected with external power supply, and the gas-liquid separation component includes gas
The lower section of liquid inlet tube, gas-liquid separator and gas-liquid outlet, the condenser is equipped with the gas-liquid separator, the gas-liquid point
It is fixedly connected with support frame as described above from device, the top of the gas-liquid separator is fixedly connected with the gas-liquid inlet tube, the gas-liquid
Inlet tube is fixedly connected with the condensate outlet pipe by pipeline, and the gas liquid outlet pipe is located at the bottom of the gas-liquid separator
End, and be fixedly connected with the gas-liquid separator, the gas-liquid separator is electrically connected with external power supply, the collection assembly packet
Collecting pipe and volumetric flask are included, the lower section of the gas-liquid separator is equipped with the volumetric flask, and the volumetric flask is solid with support frame as described above
The top of fixed connection, the volumetric flask is fixedly connected with the collecting pipe, and the collecting pipe passes through pipeline with the gas liquid outlet pipe
It is fixedly connected.
Preferably, the electrothermal tube is snakelike shape, and the electrothermal tube is bolted with the rectifying still.
Preferably, cylindrical hole is opened up inside the mounting box, the dumped packing rectifying column passes through circle with the mounting box
Post holes is fixedly connected.
Preferably, the motor is rotatablely connected with the agitating shaft.
Preferably, the mounting box is fixedly connected with support frame as described above by the first axle sleeve.
Preferably, the quantity of the dumped packing rectifying column is 20, and the mounting box is cuboid.
Preferably, the return channel is fixedly connected with support frame as described above by the second axle sleeve.
Preferably, the outer courage is welded and fixed with the rectifying still.
Preferably, the lateral wall of the agitating shaft is fixedly connected with paddle, and the quantity of the paddle is six.
Compared with prior art, the utility model has the beneficial effects that：Rectifier unit uses dumped packing rectifying column, uses
Specification is two to ten millimeters of θ ring fillers, and the theoretical cam curve of every meter of dumped packing rectifying column is ten five to two ten, can will be smart
It evaporates tower effective height and is down to 1. 5 to 2 meter, greatly reduce the construction cost in rectifying workshop, only needed more when more new varieties
Corresponding dumped packing rectifying column is changed, on-line cleaning need not be carried out again, a large amount of manpower, financial resources and material resources can be saved,
The construction of 20 dumped packing rectifying column parallel connections simultaneously, can reach the single concatenated yield of major diameter tower section, realizes experiment
Application of the efficient random packing that room pilot-scale uses in industrialized production.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is the rectifying still interior view in the utility model；
Fig. 3 is the mounting box vertical view in the utility model；
In figure：The outer courage of 10- casing assemblies, 11- discharge nozzles, 12- motors, 13- electrothermal tubes, 14- rectifying stills, 15-, 16- are followed
Ring feed pipe, 17- distillation cascades, 18- supporting racks, 19- agitating shafts, 20- heating components, 21- cycle discharge nozzle, 22- heat source imports,
23- heaters, 30- transmission assemblies, 31- circulating pumps feed pipe, 32- circulating pumps discharge nozzle, 33- circulating pumps, 40- separation assemblies,
41- rectifying discharge nozzle, 42- dumped packings rectifying column, 43- mounting boxs, 44- rectifying feed pipe, 50- reflux assemblies, 51- reflux
Pipe, 52- flow back into expects pipe, 53- return channels, 54- reflux discharge nozzle, 60- condensations, 61- condensation inlet tube, 62- condensers,
63- condensate outlets pipe, 70- gas-liquid separations component, 71- gas-liquids inlet tube, 72- gas-liquid separators, 73- gas liquid outlets pipe, 80- are received
Collect component, 81- collecting pipes, 82- volumetric flasks.
Specific implementation mode
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
The every other embodiment obtained, shall fall within the protection scope of the present invention.
- 3 are please referred to Fig.1, the utility model provides a kind of technical solution：A kind of rectifying dress producing organic high purity reagent
It sets, including casing assembly 10, heating component 20, transmission assembly 30, transmission assembly 30, separation assembly 40, reflux assembly 50, condensation
Component 60, gas-liquid separation component 70 and collection assembly 80, casing assembly 10 include discharge nozzle 11, motor 12, electrothermal tube 13, rectifying
Kettle 14, outer courage 15, recycle feed pipe 16, distillation cascade 17, supporting rack 18 and agitating shaft 19, rectifying still 14 are located at the upper of supporting rack 18
Surface, and be fixedly connected with supporting rack 18, the lateral wall of rectifying still 14 is fixedly connected with outer courage 15, and the inside of outer courage 15 is equipped with electric heating
Pipe 13, electrothermal tube 13 are fixedly connected with rectifying still 14, and the bottom end of rectifying still 14 is equipped with motor 12, and the output end of motor 12, which is fixed, to be connected
Agitating shaft 19 is connect, the right side of motor 12 is equipped with discharge nozzle 11, and discharge nozzle 11 is fixedly connected with rectifying still 14, the top of rectifying still 14
It is fixedly connected with distillation cascade 17, the right side of distillation cascade 17 is equipped with recycle feed pipe 16, and recycle feed pipe 16 is fixed with rectifying still 14 to be connected
It connects, motor 12 and electrothermal tube 13 are electrically connected with external power supply, and heating component 20 includes cycle discharge nozzle 21, heat source import 22
It is equipped with heater 23 with the right side of heater 23, rectifying still 14, heater 23 is fixedly connected with supporting rack 18, recycles discharge nozzle 21
It is fixedly connected positioned at the top of heater 23, and with heater 23, cycle discharge nozzle 21 is solid by pipeline with recycle feed pipe 16
The left surface of fixed connection, heater 23 is fixedly connected with heat source import 22, and heater 23 is electrically connected with external power supply, transmission assembly
30 include circulating pump feed pipe 31, circulating pump discharge nozzle 32 and circulating pump 33, and the lower section of heater 23 is equipped with circulating pump 33, cycle
Pump 33 is fixedly connected with supporting rack 18, and the top of circulating pump 33 is fixedly connected with circulating pump discharge nozzle 32, circulating pump discharge nozzle 32 and
Heat source import 22 is fixedly connected by pipeline, and the left surface of circulating pump 33 is fixedly connected with circulating pump feed pipe 31, circulating pump charging
Pipe 31 is fixedly connected with discharge nozzle 11 by pipeline, and separation assembly 40 includes rectifying discharge nozzle 41, dumped packing rectifying column 42, peace
The top of mounted box 43 and the radical expects pipe 44 of rectifying, rectifying still 14 is equipped with mounting box 43, and mounting box 43 is fixedly connected with supporting rack 18,
The madial wall of mounting box 43 is fixedly connected with dumped packing rectifying column 42, and the bottom end of dumped packing rectifying column 42 is fixedly connected with rectifying and swashs
Feed pipe 44, the radical expects pipe 44 of rectifying are fixedly connected with distillation cascade 17, and the top of dumped packing rectifying column 42 is fixedly connected with rectifying
Discharge nozzle 41, reflux assembly 50 include return duct 51, flow back into expects pipe 52, return channel 53 and reflux discharge nozzle 54, mounting box 43
Left side above be equipped with return channel 53, return channel 53 is fixedly connected with supporting rack 18, and the top of return channel 53 is fixedly connected with reflux
Feed pipe 52 flows back into expects pipe 52 and is fixedly connected by pipeline with rectifying discharge nozzle 41, and return duct 51 is located at the right side of return channel 53
Surface, and be fixedly connected with return channel 53, the bottom end of return channel 53 is fixedly connected with reflux discharge nozzle 54, and condensation 60 includes cold
Solidifying inlet tube 61, condenser 62 and condensate outlet pipe 63, the lower section of return channel 53 are equipped with condensate outlet pipe 63 and are equipped with condensate outlet
Pipe 63 is fixedly connected with supporting rack 18, and the top of condenser 62 is fixedly connected with condensation inlet tube 61, condensation inlet tube 61 and reflux
Discharge nozzle 54 is fixedly connected by pipeline, and the lower surface of condenser 62 is fixedly connected with condensate outlet pipe 63, condenser 62 and outside
Power supply is electrically connected, and gas-liquid separation component 70 includes gas-liquid inlet tube 71, gas-liquid separator 72 and gas-liquid outlet 73, condenser
62 lower section is equipped with gas-liquid separator 72, and gas-liquid separator 72 is fixedly connected with supporting rack 18, and the top of gas-liquid separator 72 is solid
Surely connection gas-liquid inlet tube 71, gas-liquid inlet tube 71 is fixedly connected with condensate outlet pipe 63 by pipeline, gas liquid outlet pipe 73
It being fixedly connected in the bottom end of gas-liquid separator 72, and with gas-liquid separator 72, gas-liquid separator 72 is electrically connected with external power supply,
Collection assembly 80 includes collecting pipe 81 and volumetric flask 82, and the lower section of gas-liquid separator 72 is equipped with volumetric flask 82, volumetric flask 82 and branch
Support 18 is fixedly connected, and the top of volumetric flask 82 is fixedly connected with collecting pipe 81, and collecting pipe 81 passes through pipeline with gas liquid outlet pipe 73
It is fixedly connected.
In the present embodiment, the model Y2 of motor 12, rectifying still 14 is 304 or 316 liters of stainless steels
Matter or enamel material, 200 DEG C of 33 highest heatproof of circulating pump belong to explosion-proof type pump, and heater 23 is tubular heat exchanger,
Heat source can be conduction oil or water vapour；The heater material is 304 or 316L stainless steels, dumped packing rectifying column 44
20 are shared, every is all cylinder, is 1-2M per root long degree, the filler of internal diameter 50MM, dumped packing rectifying column 44 are θ
Ring filler, specification 2-10MM, material are 316L stainless steels, and the theoretical cam curve of every meter of dumped packing rectifying column 44 is 15-20
A, 51 internal diameter of return duct of return channel 53 is 1st/10 to ten/5ths of gas phase bore, and condenser 62 is tube type cold
Condenser or plate-type condenser, volumetric flask 82 are cylinder；Volumetric flask 82 is 304 or 316L stainless steels.
In the present embodiment, casing assembly 10 includes discharge nozzle 11, motor 12, electrothermal tube 13, rectifying still 14, outer courage 15, follows
Material is imported into rectifying still by ring feed pipe 16, distillation cascade 17, supporting rack 18 and agitating shaft 19 when carrying out rectifying to material
In 14, steam is provided to rectifying still 14 by heater 23, so that material in kettle is heated, then motor 12 is given to be powered, pass through motor
12 drive agitating shafts 19, make materials inside thermally equivalent, and during stirring, by the filled layer inside outer courage 15,
It effectively reduces temperature to scatter and disappear, and by the heating of electrothermal tube 13, improves the efficiency of heating surface and rectifying material of material
Rate, heating component 20 include cycle discharge nozzle 21, heat source import 22 and heater 23, are carried out when to 14 materials inside of rectifying still
When heating, by the work of heater 23, steam is imported into from cycle discharge nozzle 21 in rectifying still, to rectifying still 14 into
Row heating, transmission assembly 30 includes circulating pump feed pipe 31, circulating pump discharge nozzle 32 and circulating pump 33, when steam is from recycle feed
When pipe 16 is imported into circulating pump 33, continue to transfer thermal energy in heater 23 by circulating pump 33, to improve resource
Use, separation assembly 40 include rectifying discharge nozzle 41, dumped packing rectifying column 42, mounting box 43 and the radical expects pipe 44 of rectifying,
When material heating after a certain period of time, imported into dumped packing rectifying column 42 from distillation cascade 17, by dumped packing rectifying column 42,
Make feed separation, the material after separation is exported from rectifying discharge nozzle 41, and reflux assembly 50 includes return duct 51, flows back into expects pipe
52, return channel 53 and reflux discharge nozzle 54, the material after separation are imported into return duct 51, and by flowing back, discharge nozzle 54 is imported into
In condenser 62, then material is cooled down by condenser 62, during material after cooling is imported into 72 in gas-liquid separator,
Thermal material is imported in return channel 53 by gas-liquid separator 72, cold material is then imported into volumetric flask 82.
Further, electrothermal tube 13 is snakelike shape, and electrothermal tube 13 is bolted with rectifying still 14.
In the present embodiment, when heating 14 materials inside of rectifying still, by the work of snakelike shape electrothermal tube 13, make heating surface
Product increases, to accelerate the temperature inside rectifying still 14.
Further, cylindrical hole is opened up inside mounting box 43, dumped packing rectifying column 42 passes through cylindrical hole with mounting box 43
It is fixedly connected.
In the present embodiment, when installing dumped packing rectifying column 42, by the cylindrical hole inside mounting box 43, convenient in bulk
Filling extract rectification column 42 is installed to inside mounting box 43.
Further, motor 12 is rotatablely connected with agitating shaft 19.
In the present embodiment, when electrothermal tube 13 and heater 23 heat rectifying still 14, stirred by the drive of motor 12
The rotation of axis 19 is mixed, 14 materials inside uniform stirring of rectifying still is made.
Further, mounting box 43 is fixedly connected with supporting rack 18 by the first axle sleeve.
In the present embodiment, when box 43 is fixedly mounted, supporting rack 18 and mounting box 43 are fixed by the first axle sleeve,
To improve stability of the mounting box 43 on supporting rack 18.
Further, the quantity of dumped packing rectifying column 42 is 20, and mounting box 43 is cuboid.
In the present embodiment, for the ease of replacing the quantity of dumped packing rectifying column 42, mounting box 43 is set as cuboid.
Further, return channel 53 is fixedly connected with supporting rack 18 by the second axle sleeve.
In the present embodiment, when installing return channel 53, supporting rack 18 and return channel 53 are fixed by the second axle sleeve,
To improve the stability of return channel 53.
Further, outer courage 15 is welded and fixed with rectifying still 14.
In the present embodiment, in order to improve stability of the outer courage 15 on rectifying still 14, outer courage 15 is welded to rectifying still
On 14 lateral wall.
Further, the lateral wall of agitating shaft 19 is fixedly connected with paddle, and the quantity of paddle is six.
In the present embodiment, in order to enable 14 materials inside thermally equivalent of rectifying still, when agitating shaft 19 rotates, agitating shaft 19
Six paddles in outside work at the same time.
The operation principle and process for using of the utility model：After the utility model installs, material is imported into rectifying
In kettle 14, steam is provided to rectifying still 14 by heater 23, so that material in kettle is heated, then motor 12 is given to be powered, pass through electricity
Machine 12 drives agitating shaft 19, makes materials inside thermally equivalent, and during stirring, passes through the filling inside outer courage 15
Layer, effectively reduce temperature scatter and disappear, when steam is imported into from recycle feed pipe 16 in circulating pump 33, by circulating pump 33 after
It is continuous to transfer thermal energy in heater 23, when material heating after a certain period of time, imported into dumped packing rectifying column from distillation cascade 17
In 42, by dumped packing rectifying column 42, make feed separation, the material after separation is exported from rectifying discharge nozzle 41, after separation
Material is imported into return duct 51, and by flowing back, discharge nozzle 54 is imported into condenser 62, then by condenser 62 by material
It is cooled down, during material after cooling is imported into 72 in gas-liquid separator, thermal material is imported by gas-liquid separator 72 and is flowed back
In device 53, cold material is then imported into volumetric flask 82.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is appreciated that can these embodiments be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaiied
Change, replace and modification, the scope of the utility model are defined by the appended claims and the equivalents thereof.
Claims (9)
1. a kind of rectifier unit producing organic high purity reagent, it is characterised in that：Including casing assembly (10), heating component
(20), transmission assembly (30), separation assembly (40), reflux assembly (50), condensation (60), gas-liquid separation component (70) and receipts
Collect component (80), the casing assembly (10) includes discharge nozzle (11), motor (12), electrothermal tube (13), rectifying still (14), outer courage
(15), recycle feed pipe (16), distillation cascade (17), supporting rack (18) and agitating shaft (19), the rectifying still (14) are located at described
The upper surface of supporting rack (18), and be fixedly connected with support frame as described above (18), the lateral wall of the rectifying still (14) is fixedly connected
The inside of the outer courage (15), the outer courage (15) is equipped with the electrothermal tube (13), the electrothermal tube (13) and the rectifying still
(14) it is fixedly connected, the bottom end of the rectifying still (14) is equipped with the motor (12), and the output end of the motor (12), which is fixed, to be connected
The agitating shaft (19) is connect, the right side of the motor (12) is equipped with the discharge nozzle (11), the discharge nozzle (11) and the essence
It evaporates kettle (14) to be fixedly connected, the top of the rectifying still (14) is fixedly connected with the distillation cascade (17), the distillation cascade (17)
Right side is equipped with the recycle feed pipe (16), and the recycle feed pipe (16) is fixedly connected with the rectifying still (14), the electricity
Machine (12) and the electrothermal tube (13) are electrically connected with external power supply, and the heating component (20) includes cycle discharge nozzle
(21), the right side of heat source import (22) and heater (23), the rectifying still (14) is equipped with the heater (23), the heating
Device (23) is fixedly connected with support frame as described above (18), and the cycle discharge nozzle (21) is located at the top of the heater (23), and
It is fixedly connected with the heater (23), the cycle discharge nozzle (21), which is fixed with the recycle feed pipe (16) by pipeline, to be connected
It connects, the left surface of the heater (23) is fixedly connected with the heat source import (22), the heater (23) and external power supply electricity
Property connection, the transmission assembly (30) includes circulating pump feed pipe (31), circulating pump discharge nozzle (32) and circulating pump (33), described
The lower section of heater (23) is equipped with the circulating pump (33), and the circulating pump (33) is fixedly connected with support frame as described above (18), institute
It states and is fixedly connected with the circulating pump discharge nozzle (32) at the top of circulating pump (33), the circulating pump discharge nozzle (32) and the heat source
Import (22) is fixedly connected by pipeline, and the left surface of the circulating pump (33) is fixedly connected with the circulating pump feed pipe (31),
The circulating pump feed pipe (31) is fixedly connected with the discharge nozzle (11) by pipeline, and the separation assembly (40) includes rectifying
Discharge nozzle (41), dumped packing rectifying column (42), mounting box (43) and the radical expects pipe of rectifying (44), the rectifying still (14) it is upper
Side is equipped with the mounting box (43), and the mounting box (43) is fixedly connected with support frame as described above (18), the mounting box (43)
Madial wall is fixedly connected with the dumped packing rectifying column (42), and the bottom end of the dumped packing rectifying column (42) is fixedly connected described
The radical expects pipe of rectifying (44), the radical expects pipe of rectifying (44) are fixedly connected with the distillation cascade (17), the dumped packing essence
The top of fractional distillation column (42) is fixedly connected with the rectifying discharge nozzle (41), and the reflux assembly (50) includes return duct (51), reflux
The left side top of feed pipe (52), return channel (53) and reflux discharge nozzle (54), the mounting box (43) is equipped with the return channel
(53), the return channel (53) is fixedly connected with support frame as described above (18), is fixedly connected at the top of the return channel (53) described
Expects pipe (52) is flowed back into, the expects pipe (52) that flows back into is fixedly connected with the rectifying discharge nozzle (41) by pipeline, described time
Flow tube (51) is located at the right surface of the return channel (53), and is fixedly connected with the return channel (53), the return channel (53)
Bottom end be fixedly connected with the reflux discharge nozzle (54), the condensation (60) includes condensation inlet tube (61), condenser
(62) it is equipped with the condensate outlet pipe (63) with condensate outlet pipe (63), the lower section of the return channel (53) and is equipped with described be condensed out
Mouth pipe (63) is fixedly connected with support frame as described above (18), and the condensation inlet tube is fixedly connected at the top of the condenser (62)
(61), the condensation inlet tube (61) is fixedly connected with the reflux discharge nozzle (54) by pipeline, the condenser (62)
Lower surface is fixedly connected with the condensate outlet pipe (63), and the condenser (62) is electrically connected with external power supply, the gas-liquid point
Include gas-liquid inlet tube (71), gas-liquid separator (72) and gas-liquid outlet (73) from component (70), the condenser (62)
Lower section is equipped with the gas-liquid separator (72), and the gas-liquid separator (72) is fixedly connected with support frame as described above (18), the gas
The top of liquid/gas separator (72) is fixedly connected with the gas-liquid inlet tube (71), the gas-liquid inlet tube (71) and the condensate outlet
Pipe (63) is fixedly connected by pipeline, and the gas liquid outlet pipe (73) is located at the bottom end of the gas-liquid separator (72), and with institute
It states gas-liquid separator (72) to be fixedly connected, the gas-liquid separator (72) is electrically connected with external power supply, the collection assembly
(80) include collecting pipe (81) and volumetric flask (82), the lower section of the gas-liquid separator (72) is equipped with the volumetric flask (82), institute
It states volumetric flask (82) to be fixedly connected with support frame as described above (18), the top of the volumetric flask (82) is fixedly connected with the collecting pipe
(81), the collecting pipe (81) is fixedly connected with the gas liquid outlet pipe (73) by pipeline.
2. a kind of rectifier unit producing organic high purity reagent according to claim 1, it is characterised in that：The electrothermal tube
(13) it is snakelike shape, the electrothermal tube (13) is bolted with the rectifying still (14).
3. a kind of rectifier unit producing organic high purity reagent according to claim 1, it is characterised in that：The mounting box
(43) internal to open up cylindrical hole, the dumped packing rectifying column (42) is fixedly connected with the mounting box (43) by cylindrical hole.
4. a kind of rectifier unit producing organic high purity reagent according to claim 1, it is characterised in that：The motor
(12) it is rotatablely connected with the agitating shaft (19).
5. a kind of rectifier unit producing organic high purity reagent according to claim 1, it is characterised in that：The mounting box
(43) it is fixedly connected by the first axle sleeve with support frame as described above (18).
6. a kind of rectifier unit producing organic high purity reagent according to claim 1, it is characterised in that：It is described in bulk to fill out
Expect that the quantity of rectifying column (42) is 20, the mounting box (43) is cuboid.
7. a kind of rectifier unit producing organic high purity reagent according to claim 1, it is characterised in that：The return channel
(53) it is fixedly connected by the second axle sleeve with support frame as described above (18).
8. a kind of rectifier unit producing organic high purity reagent according to claim 1, it is characterised in that：The outer courage
(15) it is welded and fixed with the rectifying still (14).
9. a kind of rectifier unit producing organic high purity reagent according to claim 1, it is characterised in that：The agitating shaft
(19) lateral wall is fixedly connected with paddle, and the quantity of the paddle is six.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721795232.6U CN207708557U (en) | 2017-12-20 | 2017-12-20 | A kind of rectifier unit producing organic high purity reagent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721795232.6U CN207708557U (en) | 2017-12-20 | 2017-12-20 | A kind of rectifier unit producing organic high purity reagent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207708557U true CN207708557U (en) | 2018-08-10 |
Family
ID=63056943
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112322320A (en) * | 2020-10-21 | 2021-02-05 | 恒河材料科技股份有限公司 | Separation equipment for carbon-nine resin oil and use method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112322320A (en) * | 2020-10-21 | 2021-02-05 | 恒河材料科技股份有限公司 | Separation equipment for carbon-nine resin oil and use method thereof |
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