CN207705053U - A kind of electrolytic solution for super capacitor production system - Google Patents
A kind of electrolytic solution for super capacitor production system Download PDFInfo
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- CN207705053U CN207705053U CN201820033613.9U CN201820033613U CN207705053U CN 207705053 U CN207705053 U CN 207705053U CN 201820033613 U CN201820033613 U CN 201820033613U CN 207705053 U CN207705053 U CN 207705053U
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- solvent
- purifications
- super capacitor
- electrolytic solution
- atomizing spray
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Abstract
The utility model belongs to electrolyte production technical field, more particularly to a kind of electrolytic solution for super capacitor production system, including dynamic vacuum dryer, solvent purifications system, heating system, vacuum system and solvent recovering system, the solvent purifications system, the heating system, the vacuum system and the solvent recovering system are connected by pipeline with the dynamic vacuum dryer respectively, the dynamic vacuum dryer is provided with atomizing spray washer, and the atomizing spray washer is connected with the output end of the solvent purifications system.Compared with the prior art, the utility model in electrolyte production system by being added atomizing spray washer, realize Rapid Cleaning and the drying of electrolyte, reduce the consumption of solvent for cleaning, the quality for improving product realizes electrolysis liquid product rapid batch quality stability in combination with solvent purifications system and solvent recovering system, production efficiency is improved, and realizes recycling for solvent resource.
Description
Technical field
The utility model belongs to electrolyte production technical field more particularly to a kind of electrolytic solution for super capacitor production system
System.
Background technology
Ultracapacitor is also known as double layer capacitor, charge adsorption-desorption process quick by electrode surface, reversible,
It is a kind of energy stores between traditional capacitor and secondary cell, reforming unit.Ultracapacitor has energy density
High, the advantages that charging time is short, service life is long, operating temperature range is wide, thus there is extensive use in electronics field.
Simultaneously because it adapts to national energy conservation and emission reduction environmental requirement, thus it is also intelligent logistics one an indispensable part of net.
Wherein, as the core component electrolytic solution for super capacitor of ultracapacitor, to the more demanding of the quality of production,
Usually require that its material purity >=99.95%, moisture≤10ppm and metal, anion concentration≤1ppm.However, mesh
What preceding disclosed Patents documents related generally to is one or more of specific electrolyte components, is seldom related to universal pair
Bath cleans, drying, the production system for purifying assembly line form.
In view of this, it is necessory to provide a kind of electrolytic solution for super capacitor flow line production system, super capacitor is realized
The mass production of device electrolyte；To reduce the interference of human factor in production process, energy consumption is reduced, improves production effect
Rate improves the quality of product.
Utility model content
The purpose of this utility model is that：In view of the deficiencies of the prior art, a kind of electrolytic solution for super capacitor life is provided
Production system reduces energy consumption to reduce the interference of human factor in production process, improves production efficiency, improves the product of product
Matter.
To achieve the goals above, the utility model uses following technical scheme：
A kind of electrolytic solution for super capacitor production system, including dynamic vacuum dryer, solvent purifications system, heating system
System, vacuum system and solvent recovering system, the solvent purifications system, the heating system, the vacuum system and described molten
Agent recovery system is connected by pipeline with the dynamic vacuum dryer respectively, and the dynamic vacuum dryer is provided with atomization spray
Washer is drenched, the atomizing spray washer is connected with the output end of the solvent purifications system.
Wherein, the utility model at least has following by the way that atomizing spray washer is arranged in dynamic vacuum dryer
Advantage：The first, atomizing spray washer can carry out 360 degree rotation, solve dynamic vacuum dryer internal washing dead angle hardly possible
The problem of to clean to, effectively promotes product quality；The second, ultracapacitor electrolysis matter can be cleaned and purify, electrolyte
Impurity cleans up, and can remove the moisture that electrolyte contains；Third, atomizing spray cleaning can greatly reduce the use of solvent
Amount realizes entire dryer inner and diffuses solvent, to make solvent in solvent and ultracapacitor electrolysis matter mixed process
It comes into full contact with and is uniformly mixed with ultracapacitor electrolysis matter, and the energy for cleaning solvent being dried loss can be reduced as possible
Amount；4th, atomizing spray cleaning combines dynamic vacuum to dry, on the one hand, substantially reduces drying time, and can reduce to the greatest extent
Part is excessively dry to be occurred rotten, and when machine is internally dry, shower spray of solvent volatilization is whole, than more thoroughly quickly；Another party
Face profound can deviate from moisture existing for super capacitor electrolyte crystals by solvent seasoning, realize common dynamic
Seasoning degree of drying difficult to realize, is ready to prepare high-purity electrolytic solution for super capacitor.
Further include production mixing as the preferred embodiment of electrolytic solution for super capacitor production system described in the utility model
Device, the production mixer pass through the output end phase of pipeline and the dynamic vacuum dryer and the solvent purifications system respectively
Even；The mass production that production mixer is used to be electrolysed liquid product is set, production efficiency is further increased.
As the preferred embodiment of electrolytic solution for super capacitor production system described in the utility model, the dynamic vacuum is dry
Dry machine is also associated with inert gas piping, and the inert gas piping also respectively with the solvent purifications system, the solvent
Recovery system is connected with the atomizing spray washer.So that atomizing spray washer is connect with inert gas piping, may be implemented
Solvent and electrolyte come into contact in a large area, while can also realize the displacement of dynamic vacuum dryer internal atmosphere；Wherein, inertia
Gas is nitrogen, helium or argon gas.
As the preferred embodiment of electrolytic solution for super capacitor production system described in the utility model, the atomizing spray is clear
It is centrifugal atomizing nozzle, Solid cone nozzle, hollow cone nozzles, Fan Spray Nozzle, pneumatic spray nozzle, cleaning-type spray to wash device
One kind in mouth or combinations thereof；Few to meet solvent for cleaning amount, spraying diffuses the good requirement of effect.
As the preferred embodiment of electrolytic solution for super capacitor production system described in the utility model, the solvent purifications system
System includes solvent materials tank, solvent purifications tank, solvent storage tank and solvent measuring tank, and the solvent materials tank, the solvent carry
Pure tank, the solvent storage tank and the solvent measuring tank are sequentially connected by pipeline, the atomizing spray washer with it is described
The output end of solvent measuring tank is connected.It can be direct in this way after the completion of electrolyte is dried by accessing solvent purifications production line
Purification solvent is added, pipeline automation conveying is realized, reduces interference from human factor, improve production efficiency.
As the preferred embodiment of electrolytic solution for super capacitor production system described in the utility model, the solvent recovery system
System is also connected by the vacuum system with the solvent purifications system.It may be implemented to after cleaning by solvent recovering system
Solvent is recycled, while so that the solvent after recycling is returned to solvent purifications system and being carried out dehydration purification, to realize following for solvent
Ring uses, and avoids the wasting of resources.
As the preferred embodiment of electrolytic solution for super capacitor production system described in the utility model, the dynamic vacuum is dry
The high surface area contact device of inertia or inertia hammer body are provided in dry machine；It is electrolysed matter to increase ultracapacitor in drying process
Mixability.
The beneficial effects of the utility model are：A kind of electrolytic solution for super capacitor production system of the utility model, including
Dynamic vacuum dryer, solvent purifications system, heating system, vacuum system and solvent recovering system, the solvent purifications system,
The heating system, the vacuum system and the solvent recovering system pass through pipeline and the dynamic vacuum dryer phase respectively
Even, the dynamic vacuum dryer is provided with atomizing spray washer, the atomizing spray washer and the solvent purifications system
The output end of system is connected.Compared with the prior art, the utility model is clear by the way that atomizing spray is added in electrolyte production system
Device is washed, Rapid Cleaning and the drying of electrolyte is realized, reduces the consumption of solvent for cleaning, improve the quality of product, together
When combine solvent purifications system and solvent recovering system, realize electrolysis liquid product rapid batch quality stability, improve life
Efficiency is produced, and realizes recycling for solvent resource.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model.
In figure：1- solvent purifications systems；11- solvent materials tanks；12- solvent purifications tanks；13- solvent storage tanks；14- solvents
Measuring tank；2- dynamic vacuum dryers；3- heating systems；4- solvent recovering systems；5- vacuum systems；6- atomizing sprays clean
Device；7- inert gas pipings；8- produces mixer.
Specific implementation mode
To keep the technical solution of the utility model and advantage clearer, below in conjunction with specific implementation mode and specification
Attached drawing is described in further detail the utility model and advantage, but the embodiment of the utility model is not limited to
This.
As shown in Figure 1, a kind of electrolytic solution for super capacitor production system, including dynamic vacuum dryer 2, solvent purifications system
System 1, heating system 3, vacuum system 5 and solvent recovering system 4, solvent purifications system 1, heating system 3, vacuum system 5 and molten
Agent recovery system 4 is connected by pipeline with dynamic vacuum dryer 2 respectively, and it is clear that dynamic vacuum dryer 2 is provided with atomizing spray
Device 6 is washed, atomizing spray washer 6 is connected with the output end of solvent purifications system 1.
Wherein, solvent purifications system 1 includes solvent materials tank 2, solvent purifications tank 12, solvent storage tank 13 and solvent metering
Tank 14, solvent materials tank 2, solvent purifications tank 12, solvent storage tank 13 and solvent measuring tank 14 are sequentially connected by pipeline, atomization
Spraying cleaner 6 is connected with the output end of solvent measuring tank 14.By accessing solvent purifications production line, dried in this way in electrolyte
After the completion, purification solvent can be directly added, pipeline automation conveying is realized, reduces interference from human factor, improve life
Produce efficiency.
Wherein, atomizing spray washer 6 is centrifugal atomizing nozzle, Solid cone nozzle, hollow cone nozzles, fan-spray spray
One kind or combinations thereof in mouth, pneumatic spray nozzle, cleaning-type nozzle；Few to meet solvent for cleaning amount, spraying diffuses effect
Good requirement.
Wherein, the utility model is in dynamic vacuum dryer 2 by being arranged atomizing spray washer 6, at least have with
Lower advantage：The first, atomizing spray washer 6 can carry out 360 degree rotation, and it is dead to solve 2 internal washing of dynamic vacuum dryer
Angle be difficult to clean to the problem of, effectively promote product quality；The second, ultracapacitor electrolysis matter can be cleaned and purify, electricity
Solution matter impurity cleans up, and can remove the moisture that electrolyte contains；Third, atomizing spray cleaning can greatly reduce solvent
Usage amount realizes entire dryer inner and diffuses solvent, to make in solvent and ultracapacitor electrolysis matter mixed process
Solvent comes into full contact with and is uniformly mixed with ultracapacitor electrolysis matter, and can reduce as possible and loss is dried to cleaning solvent
Energy；4th, atomizing spray cleaning combines dynamic vacuum to dry, on the one hand, substantially reduces drying time, and can be as possible
Reduce that part is excessively dry to be occurred rotten, and when machine is internally dry, shower spray of solvent volatilization is whole, than more thoroughly quickly；Separately
On the one hand, profound moisture existing for super capacitor electrolyte crystals can be deviate from by solvent seasoning, realized common
Dynamic seasoning degree of drying difficult to realize, is ready to prepare high-purity electrolytic solution for super capacitor.
Preferably, further include production mixer 8, production mixer 8 is respectively by pipeline and dynamic vacuum dryer 2 and molten
The output end of agent purification system 1 is connected；The mass production that production mixer 8 is used to be electrolysed liquid product is set, is contributed into one
Step improves production efficiency.
Preferably, dynamic vacuum dryer 2 is also associated with inert gas piping 7, and inert gas piping 7 also respectively with it is molten
Agent purification system 1, solvent recovering system 4 are connected with atomizing spray washer 6.Make atomizing spray washer 6 and inert gas tube
Road 7 connects, and coming into contact in a large area for solvent and electrolyte may be implemented, while can also realize 2 inside gas of dynamic vacuum dryer
The displacement of atmosphere；Wherein, inert gas is nitrogen, helium or argon gas.
Preferably, solvent recovering system 4 is also connected by vacuum system 5 with solvent purifications system 1.Pass through solvent recovery system
System 4 may be implemented to recycle the solvent after cleaning, while so that the solvent after recycling is returned to solvent purifications system 1 and being dehydrated
Purification, to realize the recycling of solvent, avoids the wasting of resources.
Preferably, the high surface area contact device of inertia or inertia hammer body are provided in dynamic vacuum dryer 2；It is dry to increase
The mixability of ultracapacitor electrolysis matter during dry.
To embody the advantageous effect for the electrolyte that the utility model produces, make into one below in conjunction with embodiment and comparative example
Walk explanation.
Comparative example 1
By 400 kilograms of electrolytic solution for super capacitor formulas, ultracapacitor is electrolysed matter tetraethyl ammonium tetrafluoroborate
(TEA·BF4) be added in dynamic vacuum drier, it opens 50~100 DEG C of heating temperature and is dried in vacuo, it is small every one and half
Shi Jinhang water content detections.After detection is qualified, the electrolytic solution for super capacitor that moisture is less than 10ppm is added by solvent purifications system
Solvent, then detect purity and moisture content index.
Comparative example 2
By 400 kilograms of electrolytic solution for super capacitor formulas, ultracapacitor is electrolysed matter triethyl methyl ammonium tetrafluoroborate
(TEMA·BF4) be added in dynamic vacuum drier, it opens 50~100 DEG C of heating temperature and is dried in vacuo, every one and half
Hour carries out water content detection.After detection is qualified, ultracapacitor of the moisture less than 10ppm is added by solvent purifications system and is electrolysed
The solvent of liquid, then detect purity and moisture content index.
Comparative example 3
By 400 kilograms of electrolytic solution for super capacitor formulas, ultracapacitor is electrolysed matter spiro quaternary ammonium tetrafluoroborate
(SBP·BF4) be added in dynamic vacuum drier, it opens 50~100 DEG C of heating temperature and is dried in vacuo；It is small every one and half
Shi Jinhang water content detections.After detection is qualified, the electrolytic solution for super capacitor that moisture is less than 10ppm is added by solvent purifications system
Solvent, then detect purity and moisture content index.
Embodiment 1
Electrolyte is prepared according to the identical method of comparative example 1, difference is to use atomizing spray washer instead to carry out clearly
It washes, closed vacuum system every one and a half hours, make inert gas that 0.5 kilogram of cleaning solvent be added by atomizing spray washer
Dimethyl carbonate.After adding cleaning solvent, stopping, which vacuumizes, keeps half an hour mixing, then opens one hour and be dried in vacuo；It opens simultaneously
Open chilled solvent recovery system, the dry solvent being evaporated of recycling；So cycle.After detection is qualified, pass through solvent purifications system
The solvent of electrolytic solution for super capacitor of the moisture less than 10ppm is added in system, then detects purity and moisture content index.
Embodiment 2
Electrolyte is prepared according to the identical method of comparative example 2, difference is to use atomizing spray washer instead to carry out clearly
It washes, closed vacuum system every one and a half hours, make inert gas that 0.5 kilogram of cleaning solvent be added by atomizing spray washer
Acetonitrile.After adding cleaning solvent, stopping, which vacuumizes, keeps half an hour mixing, then opens one hour and be dried in vacuo；Open freezing simultaneously
Solvent recovering system, the dry solvent being evaporated of recycling；So cycle.After detection is qualified, it is added by solvent purifications system
The solvent of electrolytic solution for super capacitor of the moisture less than 10ppm, then detect purity and moisture content index.
Embodiment 3
Electrolyte is prepared according to the identical method of comparative example 3, difference is to use atomizing spray washer instead to carry out clearly
It washes, closed vacuum system every one and a half hours, make inert gas that 0.5 kilogram of cleaning solvent be added by atomizing spray washer
Acetonitrile.After adding cleaning solvent, stopping, which vacuumizes, keeps half an hour mixing, then opens one hour and be dried in vacuo；Open freezing simultaneously
Solvent recovering system, the dry solvent being evaporated of recycling；So cycle.After detection is qualified, it is added by solvent purifications system
The solvent of electrolytic solution for super capacitor of the moisture less than 10ppm, then detect purity and moisture content index.
Wherein, in comparative example 1~3 and Examples 1 to 3 ultracapacitor electrolysis matter and electrolytic solution for super capacitor moisture
Numerical statistic such as following table：
By the test result of upper table it is found that the electrolyte prepared using Tthe utility model system is at least had the advantage that：
1) quantity of solvent used from experiment compares, and using atomizing spray cleaning method, can reduce the production time, improves production efficiency,
Reduce production waste.If 2) consider cleaning solvent recycling, unnecessary cleaning solution storage tank is used less；Meanwhile the electricity of production
It solves liquid quality more to stablize, reduce with standard recipe difference.Even if 3) use Conventional drying methods that can dry bath surface water
Point, it is also difficult to thoroughly removal electrolyte crystals moisture, so the electrolytic solution for super capacitor moisture produced is higher；And this
Utility model combines dynamic vacuum to dry by atomizing spray cleaning, profound can deviate from super capacitor electricity by solvent seasoning
Moisture existing for matter crystals is solved, common dynamic seasoning degree of drying difficult to realize is realized.4) solvent purifications are combined
And solvent recovering system, electrolysis liquid product rapid batch quality stability is realized, improves production efficiency, and realize solvent
Resource recycles.
According to the disclosure and teachings of the above specification, the utility model those skilled in the art can also be to above-mentioned reality
The mode of applying is changed and is changed.Therefore, the utility model is not limited to above-mentioned specific implementation mode, every this field skill
It is new that art personnel any conspicuously improved, replacement or modification made on the basis of the utility model belongs to this practicality
The protection domain of type.In addition, although some specific terms, these terms has been used to be intended merely to facilitate in this specification
It is bright, any restrictions are not constituted to the utility model.
Claims (7)
1. a kind of electrolytic solution for super capacitor production system, it is characterised in that：Including dynamic vacuum dryer, solvent purifications system
System, heating system, vacuum system and solvent recovering system, the solvent purifications system, the heating system, the vacuum system
It is connected respectively with the dynamic vacuum dryer by pipeline with the solvent recovering system, the dynamic vacuum dryer setting
There are atomizing spray washer, the atomizing spray washer to be connected with the output end of the solvent purifications system.
2. electrolytic solution for super capacitor production system according to claim 1, it is characterised in that：It further include production mixing
Device, the production mixer pass through the output end phase of pipeline and the dynamic vacuum dryer and the solvent purifications system respectively
Even.
3. electrolytic solution for super capacitor production system according to claim 1, it is characterised in that：The dynamic vacuum drying
Machine is also associated with inert gas piping, and the inert gas piping is also returned with the solvent purifications system, the solvent respectively
Receipts system is connected with the atomizing spray washer.
4. electrolytic solution for super capacitor production system according to claim 1, it is characterised in that：The atomizing spray cleaning
Device is centrifugal atomizing nozzle, Solid cone nozzle, hollow cone nozzles, Fan Spray Nozzle, pneumatic spray nozzle, cleaning-type nozzle
In one kind or combinations thereof.
5. electrolytic solution for super capacitor production system according to claim 1, it is characterised in that：The solvent purifications system
Including solvent materials tank, solvent purifications tank, solvent storage tank and solvent measuring tank, the solvent materials tank, the solvent purifications
Tank, the solvent storage tank and the solvent measuring tank are sequentially connected by pipeline, the atomizing spray washer with it is described molten
The output end of agent measuring tank is connected.
6. electrolytic solution for super capacitor production system according to claim 1, it is characterised in that：The solvent recovering system
Also it is connected with the solvent purifications system by the vacuum system.
7. electrolytic solution for super capacitor production system according to claim 1, it is characterised in that：The dynamic vacuum drying
The high surface area contact device of inertia or inertia hammer body are provided in machine.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201820033613.9U CN207705053U (en) | 2018-01-09 | 2018-01-09 | A kind of electrolytic solution for super capacitor production system |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201820033613.9U CN207705053U (en) | 2018-01-09 | 2018-01-09 | A kind of electrolytic solution for super capacitor production system |
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| CN207705053U true CN207705053U (en) | 2018-08-07 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108091496A (en) * | 2018-01-09 | 2018-05-29 | 东莞市天丰电源材料有限公司 | A kind of electrolytic solution for super capacitor production system |
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2018
- 2018-01-09 CN CN201820033613.9U patent/CN207705053U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108091496A (en) * | 2018-01-09 | 2018-05-29 | 东莞市天丰电源材料有限公司 | A kind of electrolytic solution for super capacitor production system |
| CN108091496B (en) * | 2018-01-09 | 2024-02-23 | 东莞市天丰电源材料有限公司 | Supercapacitor electrolyte production system |
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