CN207694763U - Two-phase haptoreaction device - Google Patents
Two-phase haptoreaction device Download PDFInfo
- Publication number
- CN207694763U CN207694763U CN201721717448.0U CN201721717448U CN207694763U CN 207694763 U CN207694763 U CN 207694763U CN 201721717448 U CN201721717448 U CN 201721717448U CN 207694763 U CN207694763 U CN 207694763U
- Authority
- CN
- China
- Prior art keywords
- atomizer
- liquid layer
- autoclave body
- reserve liquid
- valve
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Nozzles (AREA)
Abstract
The utility model discloses two-phase haptoreaction devices, belong to field of chemical equipment.Including being equipped with upper reserve liquid layer at the top of autoclave body；Autoclave body bottom is equipped with lower reserve liquid layer；The lower reserve liquid layer bottom is equipped with discharge port, and discharge port is connected with the first atomizer and feed pipe, and the second atomizer is equipped between storage tank and upper reserve liquid layer.Present apparatus rational deployment, repeatedly makes two phase reaction object haptoreaction, circular response, reduces the reaction time, the property that improves that the reaction was complete.Simultaneously by the cooperation of controller and intelligent control valve, entire recycle feed is made to reach automation.
Description
Technical field
The utility model is related to field of chemical equipment, and in particular to a kind of two-phase haptoreaction device.
Background technology
In chemical reaction, two phase reaction is common reaction process.Gas liquid reaction, reactive liquid solution in two phase reaction are
Common reactant, usually since contact surface is smaller, influences reaction rate and reaction completeness in the two reaction process.
Utility model content
To solve the above-mentioned problems.The utility model proposes one kind can automation control reaction rate, improve contact surface
Product, promotes the two-phase haptoreaction device of chemical reaction completeness.
To achieve the goals above, the utility model is achieved through the following technical solutions：
A kind of two-phase haptoreaction device, including autoclave body and the chuck on the outside of autoclave body, the autoclave body top are equipped with upper
Reserve liquid layer；The autoclave body bottom is equipped with lower reserve liquid layer；The lower reserve liquid layer bottom is equipped with discharge port, and the lower reserve liquid layer side is set
There is feed inlet；The discharge port is connected with the first threeway, and the two of which interface of first threeway is connected separately with the first mist
Change device and feed pipe, the feed pipe are connected with storage tank, the storage tank is connect with upper reserve liquid layer by pipeline；The storage tank with it is upper
Between reserve liquid layer be equipped with the second atomizer, between second atomizer and upper reserve liquid layer be equipped with the second threeway, the described 2nd 3
One of logical port is connected with air inlet pipe；The upper reserve liquid layer bottom is equipped with multiple liquid outlets, each on the liquid outlet
Equipped with control valve；Elevator pump and the first valve are equipped between first threeway and feed pipe；The air inlet pipe and the second threeway
Between be equipped with the second valve；The jacket surface is equipped with controller, the controller and first valve, the second valve and carries
Liter pump is electrically connected or wireless signal connection.
Further, the outlet of first atomizer is connected with the atomizer of multiple opening upwards, the atomization spray
Head extends to inside autoclave body.
Further, the liquid outlet direction is corresponding with downward and with the atomizer.
Further, the control valve is wirelessly connected with controller.
Further, the atomizer is higher than the lower reserve liquid layer.
Further, cooling water or high-temperature steam are equipped in the chuck.
Further, the top and middle part of the autoclave body are equipped with pressure gauge and pressure valve, and the autoclave body is equipped with exhaust
Valve, the air bleeding valve setting is inside autoclave body and in upper reserve liquid layer.
The utility model two-phase haptoreaction device, advantage are：
(1) reaction liquid of lower reserve liquid layer is atomized with by the first atomizer and atomizer, increases and connect by discharge port
Contacting surface is accumulated, while the mixture after primary first-order equation is back in lower reserve liquid layer, and carries out cycle atomization haptoreaction, improves reaction
Efficiency.
(2) discharge port is connected by feed pipe with storage tank, the mixture after primary first-order equation is back in storage tank, in storage tank
Haptoreaction is carried out again, the mixture after haptoreaction is atomized by the second atomizer again, and be atomized with the first atomizer
The material of lower reserve liquid layer again react by secondary response, promotion.
(3) the utility model rational deployment repeatedly makes two phase reaction object haptoreaction, circular response reduce the reaction time,
Improve the reaction was complete property.
(4) reserve liquid layer is equipped with control valve on, and control valve is intelligent control valve, and open number can be controlled by controller, into
And control reaction rate；Other first valve, the second valve and elevator pump are controller intelligent control, make entire recycle feed
Reach automation.
Description of the drawings
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment
Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only
It is some embodiments of the utility model, for those of ordinary skill in the art, before not making the creative labor property
It puts, other drawings may also be obtained based on these drawings.
Fig. 1 is the structural schematic diagram of the utility model；
1- autoclave bodies, 2- chucks, the upper reserve liquid layers of 3-, reserve liquid layer under 4-, 5- discharge ports, 6- feed inlets, the first threeways of 7-, 8-
Two threeways, the first atomizers of 9-, 10- feed pipes, 11- storage tanks.The second atomizers of 12-, 13- air inlet pipe, 14- liquid outlets, 15- controls
Valve processed, 16- elevator pumps, the first valves of 17-, the second valves of 18-, 19- controllers, 20- atomizers, 21- pressure gauges, 22- pressures
Power valve, 23- air bleeding valves.
Specific implementation mode
The utility model is further described with reference to specific embodiment and attached drawing.
A kind of two-phase haptoreaction device such as Fig. 1, including autoclave body 1 and the chuck 2 positioned at the outside of autoclave body 1 are equipped in chuck 2
Cooling water or high-temperature steam, the top and middle part of autoclave body 1 are equipped with pressure gauge 21, pressure valve 22, and the setting of the air bleeding valve 23 exists
In 1 inside of autoclave body and upper reserve liquid layer 3；1 top of autoclave body is equipped with upper reserve liquid layer 3；1 bottom of autoclave body is equipped with lower reserve liquid layer 4；Lower reserve liquid layer
4 bottoms are equipped with discharge port 5, and lower 4 side of reserve liquid layer is equipped with feed inlet 6；Discharge port 5 is connected with the first threeway 7, the first threeway 7
Two of which interface is connected separately with the first atomizer 9 and feed pipe 10, the outlet of the first atomizer 9 be connected with it is multiple be open to
On atomizer 20, atomizer 20 extends to inside autoclave body 1, and atomizer 20 is higher than the lower reserve liquid layer 4, feed pipe 10
It is connected with storage tank 11, storage tank 11 is connect with upper reserve liquid layer 3 by pipeline；The second atomization is equipped between storage tank 11 and upper reserve liquid layer 3
Device 12, between the second atomizer 12 and upper reserve liquid layer 3 be equipped with the second threeway 8, one of second threeway 8 port be connected with into
Tracheae 13；3 bottom of upper reserve liquid layer is equipped with multiple liquid outlets 14,14 direction of liquid outlet with it is opposite downward and with atomizer 20
It answers, each liquid outlet 14 is equipped with control valve 15；Elevator pump 16 and the first valve are equipped between first threeway 7 and feed pipe 10
17；The second valve 18 is equipped between air inlet pipe 13 and the second threeway 8；2 surface of chuck is equipped with controller 19, controller 19 and first
Valve 17, the second valve 18 is electrically connected with elevator pump 16 or wireless signal connects, and control valve 15 is wirelessly connected with controller 19.
It is such as solution-air haptoreaction, then it is liquid to descend reserve liquid layer 4, and liquid enters lower reserve liquid layer 4 simultaneously by feed inlet 6
Pass through the first atomizer 9；And controller 19 controls the second valve 18 and opens, the first valve 17 is closed, and gas then passes through air inlet pipe
13 second valves 18 enter upper reserve liquid layer 3；The control valve 15 that controller 19 controls the liquid outlet 14 in upper reserve liquid layer 3 partially opens
Or it is fully open, so that gas is entered, the atomized liquid sprayed from atomizer 20 after the gas and the atomization of the first atomizer 9 after
Body haptoreaction, process of the liquid in whereabouts reacts, and returns to lower reserve liquid layer 4, the gas brought into drop and lower liquid storage
Liquid in layer 4 further reacts；Primary first-order equation is recycled due to insufficient, then by discharge port 5 and the first atomizer 9,
Reach that the reaction was complete.
Such as it is that liquid-liquid contact is reacted, then it is A liquid to descend reserve liquid layer 4, and liquid enters lower reserve liquid layer 4 simultaneously by feed inlet 6
Pass through the first atomizer 9；And controller 19 controls the second valve 18 and closes, the first valve 17 is opened, and is B liquid in storage tank 11
Body, B liquid enter upper reserve liquid layer 3 by the second atomizer 12, and controller 19 controls the control of the liquid outlet 14 in upper reserve liquid layer 3
Valve 15 partially opens or fully open, and the B liquid after making the second atomizer 12 be atomized enters from liquid outlet 14, the B liquid after
The A liquid atomized liquid haptoreactions sprayed from atomizer 20 after body atomized liquid and the atomization of the first atomizer 9, liquid is in whereabouts
Process reacts, and returns to lower reserve liquid layer 4, and the gas brought into drop is further reacted with the liquid in lower reserve liquid layer 4；One
Secondary response is recycled due to insufficient, then by discharge port 5 and the first atomizer 9, reaches that the reaction was complete.Primary first-order equation simultaneously
Mixture by elevator pump 16 enter storage tank 11 in, since the B content liquids in storage tank 11 are more, and elevator pump 16 promoted
A content liquids are more in mixing liquid, after entering storage tank 11 and B liquid haptoreactions because of circulation A liquid, then pass through the second mist simultaneously
Change device 12 atomization enter, and with the liquid circulation haptoreaction of lower reserve liquid layer 4.Reach multiple-contact reaction in the process, promotees
Into the complete of reaction, the time is saved.
The technical solution provided above the utility model embodiment is described in detail, used herein specifically
A example is expounded the principle and embodiment of the utility model embodiment, and the explanation of above example is only applicable to help
Assistant solves the principle of the utility model embodiment；Meanwhile for those of ordinary skill in the art, implementing according to the utility model
Example, the there will be changes in specific implementation mode and application range, in conclusion the content of the present specification should not be construed as
Limitations of the present invention.
Claims (7)
1. a kind of two-phase haptoreaction device, it is characterised in that：Chuck including autoclave body and on the outside of autoclave body, the autoclave body top
Portion is equipped with upper reserve liquid layer；The autoclave body bottom is equipped with lower reserve liquid layer；The lower reserve liquid layer bottom is equipped with discharge port, the lower liquid storage
Layer side is equipped with feed inlet；The discharge port is connected with the first threeway, and the two of which interface of first threeway is separately connected
There are the first atomizer and feed pipe, the feed pipe to be connected with storage tank, the storage tank is connect with upper reserve liquid layer by pipeline；It is described
It is equipped with the second atomizer between storage tank and upper reserve liquid layer, the second threeway, institute are equipped between second atomizer and upper reserve liquid layer
It states one of the second threeway port and is connected with air inlet pipe；The upper reserve liquid layer bottom is equipped with multiple liquid outlets, each described
Liquid outlet is equipped with control valve；Elevator pump and the first valve are equipped between first threeway and feed pipe；The air inlet pipe with
The second valve is equipped between second threeway；The jacket surface is equipped with controller, the controller and first valve, second
Valve is electrically connected with elevator pump or wireless signal connects.
2. two-phase haptoreaction device according to claim 1, it is characterised in that：The outlet of first atomizer is connected with
The atomizer of multiple opening upwards, the atomizer extend to inside autoclave body.
3. two-phase haptoreaction device according to claim 2, it is characterised in that：The liquid outlet direction with downward and with
The atomizer is corresponding.
4. two-phase haptoreaction device according to claim 1, it is characterised in that：The control valve wirelessly connects with controller
It connects.
5. two-phase haptoreaction device according to claim 2, it is characterised in that：The atomizer is higher than the lower liquid storage
Layer.
6. two-phase haptoreaction device according to claim 1, it is characterised in that：Cooling water or high temperature are equipped in the chuck
Steam.
7. two-phase haptoreaction device according to claim 1, it is characterised in that：The top and middle part of the autoclave body are equipped with
Pressure gauge and pressure valve, the autoclave body are equipped with air bleeding valve, and the air bleeding valve setting is inside autoclave body and in upper reserve liquid layer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721717448.0U CN207694763U (en) | 2017-12-08 | 2017-12-08 | Two-phase haptoreaction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721717448.0U CN207694763U (en) | 2017-12-08 | 2017-12-08 | Two-phase haptoreaction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207694763U true CN207694763U (en) | 2018-08-07 |
Family
ID=63025796
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721717448.0U Active CN207694763U (en) | 2017-12-08 | 2017-12-08 | Two-phase haptoreaction device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207694763U (en) |
-
2017
- 2017-12-08 CN CN201721717448.0U patent/CN207694763U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN206008688U (en) | A kind of circular response kettle | |
| CN207778974U (en) | A kind of spray drying tower | |
| CN206405435U (en) | A kind of micro-fluidic preparation facilities of nano-Au solution | |
| CN207694763U (en) | Two-phase haptoreaction device | |
| CN115322219B (en) | Continuous production system and method for isopropyl titanate | |
| CN103920444A (en) | Spraying reaction device, integrated spraying reactor system and operation method of integrated spraying reactor system | |
| CN204395959U (en) | A kind of anticorrosion reaction unit of temperature-control pressure-control | |
| CN101613272A (en) | Equipment with atomizing raw materials continuous production ester class | |
| CN207562904U (en) | A kind of sodium methoxide reaction tower | |
| CN207313154U (en) | A kind of calcium carbonate carbonators equipped with gas distributor | |
| CN105371262B (en) | Fountain steam generator | |
| CN207271266U (en) | gas-liquid contact reaction device | |
| CN202666870U (en) | Reaction device | |
| CN207271222U (en) | Intermittent automatic feed gas-liquid reaction apparatus | |
| CN209066045U (en) | A kind of molten copper device | |
| CN209501320U (en) | A kind of nitric acid tail gas recyclable device | |
| CN207271221U (en) | Continuous feed gas-liquid reaction apparatus | |
| CN202933514U (en) | Leaching device | |
| CN206082505U (en) | Be used for 2 liquid caustic soda spraying feeding device of chloroacrylonitrile production | |
| CN209564995U (en) | A kind of injection reaction unit preparing dichlorohydrin from glycerol | |
| CN207667619U (en) | A kind of phenols and isobutene reaction device | |
| CN207655120U (en) | A kind of liquefied ammonia and propionic acid reaction unit improving reaction efficiency | |
| CN106310903A (en) | Waste gas reaction tower capable of secondary treatment | |
| CN209123932U (en) | A kind of spray type reactor | |
| CN108295799B (en) | High-efficiency polyether reactor |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |