CN207680597U - A kind of Zeolite synthesis device - Google Patents
A kind of Zeolite synthesis device Download PDFInfo
- Publication number
- CN207680597U CN207680597U CN201721540120.6U CN201721540120U CN207680597U CN 207680597 U CN207680597 U CN 207680597U CN 201721540120 U CN201721540120 U CN 201721540120U CN 207680597 U CN207680597 U CN 207680597U
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- autoclave body
- kettle cover
- lifting
- kettle
- unit
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- Silicates, Zeolites, And Molecular Sieves (AREA)
Abstract
The Zeolite synthesis device of the easy to clean and discharging of the utility model includes：Reaction member, heating unit, the lifting unit for moving up and down the kettle cover, the roll-over unit for driving autoclave body overturning, device fixed frame, reaction member, heating unit, kettle cover lifting unit, autoclave body roll-over unit and device fixed frame, each part mentioned above are connected and composed unified whole by connecting elements, support arm and fixing bolt etc..Due to introducing kettle cover lifting unit and autoclave body roll-over unit, it efficiently solves the processes such as charging, discharging, cleaning, checking maintenance to need manually to open kettle cover and autoclave body and cannot rotate, the problems such as unloading difficulties and discharging pipeline block, reduce human input, improves device service efficiency.
Description
Technical field
The utility model is related to a kind of chemical production equipments, more particularly to a kind of easy to clean and discharging to be closed for hydro-thermal
At the reaction unit of molecular sieve.
Background technology
Molecular sieve is due to regular pore passage structure and appropriate acid, being widely used in the processes such as oil refining, chemical industry.Synthesis
Molecular sieve in discharge process, if using pipeline discharging, since molecular sieve is the crystalline solid for having certain viscosity, be easy to make
Block, be not easily cleaned at pipeline, in addition, plus raw material and reaction kettle need frequently to open reaction kettle cover, and reaction kettle when cleaning
Body cannot rotate, time-consuming and laborious with manual operation, seriously affect device service efficiency.
Currently, molecular sieve disclosed in Chinese patent CN202376991U, CN203316116U, CN 204933460U etc. closes
The problem of uncapping is not considered at kettle, to feed, the design of discharging and cleaning, for using process, when into kettle plus raw material, unloading
Material and to carrying out thorough cleaning in kettle and when checking maintenance, there are inconvenient drawbacks.
Therefore, design one kind is uncapped conveniently, and autoclave body may be reversed, convenient for the Zeolite synthesis device of charging, cleaning and discharging
It is one of the field problem to be solved.
Utility model content
The purpose of this utility model is to provide a kind of charging, discharging and Zeolite synthesis devices easy to clean.
In order to achieve the above objectives, the application provides a kind of Zeolite synthesis device, including：
One reaction member is equipped with autoclave body and the kettle cover with the kettle mouth sealed connection of the autoclave body；
One heating unit is covered on the autoclave body outer wall；
One moves up and down the lifting unit of the kettle cover, is connect with the kettle cover；
One drives the roll-over unit of autoclave body overturning, is connect with autoclave body；
One device fixed frame, with the lifting unit and the roll-over unit connect and support the fixed lifting unit and
The roll-over unit.
In an embodiment, described device fixed frame is equipped with a column and a pedestal, and the column is fixed on the pedestal
The upper and described column is hollow pillar stand.
In an embodiment, the lifting unit further comprises a first driving means and one first transmission device, institute
First driving means are stated to connect with the kettle cover by first transmission device.
In an embodiment, the first driving means be lifting drive, the lifting drive be manually or
Person is electronic.
In an embodiment, first transmission device includes a lifting and driving screw rod, a moving portion and a connecting elements,
The lifting and driving screw rod is spirally connected the moving portion and the connecting elements successively upwards along the hollow pillar stand axial direction,
The moving portion is set at the top of the hollow pillar stand, and the moving portion top is fixed with described connecting elements one end, the company
The other end of connection member is connect with the kettle cover, and the lifting and driving screw rod drives the moving portion along the hollow pillar stand
Axial direction moves up and down, to drive the kettle cover to move up and down.
In an embodiment, the roll-over unit is connect including an overturning drive device and one with the overturning drive device
Overturning drive screw, the overturning drive screw connect across the hollow pillar stand with the autoclave body, the overturning driving dress
It is set to the overturning drive screw driving force is provided and the overturning drive screw is driven to rotate, and then the overturning drive screw
The autoclave body is driven to be rotated as axle center using the overturning drive screw.
In an embodiment, the autoclave body is a vertical response kettle, and the kettle cover is secured by bolts in the autoclave body
On kettle mouth.
In an embodiment, the kettle cover connection blow-down pipe and pressure gauge, agitating paddle, the blow-down pipe, the pressure
Power table, the agitating paddle are connected to autoclave body inside, and the agitating paddle accesses kettle body bottom by kettle cover.
In an embodiment, the heating unit is an electric heating cover.
Compared with prior art, the Zeolite synthesis device of the easy to clean and discharging of the utility model is mainly used for molecule
The hydro-thermal method of sieve synthesizes, and simultaneously can be used for the fields such as other chemical reactions and organic synthesis；Secondly as introducing kettle cover lifting
Unit and autoclave body roll-over unit efficiently solve the processes such as charging, discharging, cleaning, checking maintenance needs and manually open kettle cover and kettle
The problems such as body cannot rotate, and unloading difficulties and discharging pipeline block, reduces human input, improves device service efficiency.The
Three, which is connected and composed unified whole by fixed frame, and easy to operate, flexible, floor space is small, and can as needed into
Line position sets movement.
Description of the drawings
Fig. 1 is the Zeolite synthesis apparatus structure schematic diagram of the utility model.
Fig. 2 is the utility model kettle cover vertical view.
Wherein, reference numeral：
1- autoclave bodies
2- electric heating covers
3- kettle covers
4- blow-down pipes
5- agitating paddles
6- pressure gauges
7- lifting drives
8- lifting and driving screw rods
9- moving portions
10- connecting elements
11- overturning drive devices
12- overturns drive screw
13- columns
14- pedestals
15~22- fixing bolts
Specific implementation mode
To illustrate the technical characterstic of the utility model, so that those skilled in the art know that the structure of the utility model
Feature, application method and technique effect are illustrated by specific implementation mode and in conjunction with attached drawing to this case, see Fig. 1, Fig. 2.But
As described below is only to illustrate to be used, and is not intended as the limitation of the utility model.
To achieve the above object, the Zeolite synthesis device of the utility model, including：Reaction member, heating unit, up and down
The lifting unit of the mobile kettle cover, roll-over unit, the device fixed frame for driving autoclave body overturning, each part mentioned above is by connecting structure
Part, support arm and fixing bolt etc. connect and compose unified whole.
It is a vertical response that reaction member, which is equipped with autoclave body and the kettle cover with the kettle mouth sealed connection of the autoclave body, reaction member,
Kettle, kettle cover are secured by bolts on kettle mouth；Kettle cover connects blow-down pipe and pressure gauge, agitating paddle, blow-down pipe and pressure
With unicom inside autoclave body, agitating paddle accesses kettle body bottom by kettle cover for table, agitating paddle, wherein autoclave body volume is 1-20L.
Heating unit covers on the autoclave body outer wall, and heating unit is an electric heating cover, is fixed on outside autoclave body, heats
Internal set is resistive heater, and fills silica wool heat preservation, and heating mantle can be easy to disassemble.
Device fixed frame connects and supports with the lifting unit and the roll-over unit and fixes the lifting unit and the overturning list
Member.Further, which is equipped with a column and a pedestal, which is fixed on the pedestal and the column is hollow
Column.Device fixed frame is secured by bolts on pedestal by column and is constituted.
Lifting unit is connect with the kettle cover, and to move up and down the kettle cover, which further comprises one first drive
Dynamic device and one first transmission device, the first driving means are connect by first transmission device with the kettle cover, first biography
Dynamic device is embedded in the device fixed frame.The first driving means be lifting drive, the lifting drive be manually or
Person is electronic.The first driving means include a lifting and driving screw rod, a moving portion and a connecting elements, the lifting and driving screw rod edge
Hollow pillar stand axial direction setting, which connect with the lifting drive, the lifting and driving screw rod edge
It the hollow pillar stand axial direction and sequentially passes through the moving portion and the connecting elements, the other end of the connecting elements and the kettle upwards
Lid connection, under the drive of lifting drive, which drives the moving portion along the axial direction of the hollow pillar stand
Direction moves up and down, in detail it, lifting and driving screw rod drives the moving portion and the connecting elements using threaded engagement, to drive
The kettle cover is moved up and down and (is freely lifted).
Lifting transmission device is manually or electrically to drive, and transmission device provides power, is driven and is moved by lifting and driving screw rod
Dynamic portion and connecting elements freely up and down move, and then drive kettle cover, realize being freely lifted for kettle cover.
Autoclave body roll-over unit, including an overturning drive device and an overturning drive screw, the overturning drive device turn over for this
Turn drive screw driving force is provided and the overturning screw rod is driven to rotate, which passes through the hollow pillar stand and the autoclave body
Connection, the overturning drive screw drive the autoclave body to be rotated using the overturning drive screw as axle center in turn, are driven by overturning
Screw rod drives autoclave body rotation, to realize easy-unloading.
The utility model is a kind of easy to clean and discharging Zeolite synthesis device is accomplished by the following way, by column 13
It is secured by bolts on pedestal 14.Electric heating cover 2 is fixed on autoclave body 1, and passes through fixed support arm and overturning transmission spiral shell
Bar 12 is connected on fixed pillar, and 2 inner disc of electric heating cover has resistance wire, and is filled with silica wool, reaches heat preservation purpose.Kettle cover
3 are fixed on by connecting elements 10 in moving portion 9, and moving portion 9 is connect with column 13, and column 13 is hollow pillar stand, 9 He of moving portion
Lifting and driving screw rod 8 is embedded, and lifting and driving screw rod 8 inside column with connecting elements by being connected, a lifting transmission device 7
Lifting and driving screw rod 8 is connected, provides power for lifting and driving screw rod, lifting and driving screw rod 8 drives connection structure by threaded engagement
Part 10 and moving portion 9, and then kettle cover 3 is driven to move up and down.Autoclave body 1 is connected and fixed holder and overturning drive screw 12, through vertical
It is connect with overturning drive device 11 after column 13, overturning drive device 11 drives overturning drive screw 12 to rotate, and then drives autoclave body 1
It is that axle center is rotated to overturn drive screw 12.
In use, opening kettle cover fixing bolt 15-22, start lifting drive 7, kettle cover 3 is opened and is risen, into kettle
Sequentially add reaction raw materials.It is again started up lifting drive 7, kettle cover 3 is fallen, tightens kettle cover fixing bolt 15-22, is closed
Blow valve 4 is opened agitating paddle 5, is adjusted as needed to certain rotating speed.After mixed material closes uniformly, 2 electricity of electric heating cover is opened
Source carries out temperature programming to autoclave body, and monitors temperature in the kettle, after temperature reaches requirement, proceeds by thermostatic crystallization, and according to
Reaction characteristics adjust the rotating speed of agitating paddle 5.After crystallization, electric heating cover 2 is unloaded, makes autoclave body Temperature fall in air,
It waits for that temperature is cooled to room temperature, opens blow-down pipe 4, after internal and external pressure balance, open kettle cover fixing bolt 15-22, start kettle cover
Kettle cover 3 is opened and is risen by lifting transmission device 7.Start overturning drive device 11, autoclave body is made slowly to rotate, until material stream is from kettle
Mouth flows into the container got ready surely, according to material flow, constantly adjusts autoclave body rotation angle.After the completion of discharging, autoclave body is returned
Just, clear water or caustic dip are poured into autoclave body, determine the need for adding gentle agitation as needed.After the completion of cleaning, again
Start overturning drive device 11, waste water in kettle is released, autoclave body is playbacked to original state, for use.
Compared with prior art, the Zeolite synthesis device of the easy to clean and discharging of the utility model is mainly used for molecule
The hydro-thermal method of sieve synthesizes, and simultaneously can be used for the fields such as other chemical reactions and organic synthesis；Secondly as introducing kettle cover lifting
Unit and autoclave body roll-over unit efficiently solve the processes such as charging, discharging, cleaning, checking maintenance needs and manually open kettle cover and kettle
The problems such as body cannot rotate, and unloading difficulties and discharging pipeline block, reduces human input, improves device service efficiency.The
Three, which is connected and composed unified whole by fixed frame, and easy to operate, flexible, floor space is small, and can as needed into
Line position sets movement.
The utility model can also have other various embodiments, in the situation without departing substantially from the spirit of the present invention and its essence
Under, those skilled in the art can make various corresponding change and deformations according to the utility model, but these are corresponding
Change and distortion should all belong to the protection domain of the utility model the attached claims.
Claims (9)
1. a kind of Zeolite synthesis device, which is characterized in that including：
One reaction member is equipped with autoclave body and the kettle cover with the kettle mouth sealed connection of the autoclave body；
One heating unit is covered on the autoclave body outer wall；
One moves up and down the lifting unit of the kettle cover, is connect with the kettle cover；
One drives the roll-over unit of autoclave body overturning, is connect with autoclave body；
One device fixed frame connects and supports the fixed lifting unit and described with the lifting unit and the roll-over unit
Roll-over unit.
2. Zeolite synthesis device as described in claim 1, which is characterized in that described device fixed frame is equipped with a column and one
Pedestal, the column is fixed on the pedestal and the column is hollow pillar stand.
3. Zeolite synthesis device as claimed in claim 2, which is characterized in that the lifting unit further comprises one first
Driving device and one first transmission device, the first driving means are connect by first transmission device with the kettle cover.
4. Zeolite synthesis device as claimed in claim 3, which is characterized in that the first driving means are lifting driving dress
It sets, the lifting drive is manual or electronic.
5. Zeolite synthesis device as claimed in claim 4, which is characterized in that first transmission device includes that a lifting passes
Dynamic screw rod, a moving portion and a connecting elements, the lifting and driving screw rod along the hollow pillar stand axial direction upwards successively
The moving portion that is spirally connected and the connecting elements, the moving portion are set at the top of the hollow pillar stand, the moving portion top
It is fixed with described connecting elements one end, the other end of the connecting elements is connect with the kettle cover, the lifting and driving screw rod band
It moves the moving portion to move up and down along the axial direction of the hollow pillar stand, to drive the kettle cover to move up and down.
6. Zeolite synthesis device as claimed in claim 3, which is characterized in that the roll-over unit includes an overturning driving dress
Set the overturning drive screw being connect with the overturning drive device with one, the overturning drive screw pass through the hollow pillar stand with
The autoclave body connection, the overturning drive device provide driving force for the overturning drive screw and the overturning are driven to be driven spiral shell
Bar rotates, and then the overturning drive screw drives the autoclave body to be rotated as axle center using the overturning drive screw.
7. Zeolite synthesis device as described in claim 1, which is characterized in that the autoclave body is a vertical response kettle, described
Kettle cover is secured by bolts on the kettle mouth of the autoclave body.
8. Zeolite synthesis device as described in claim 1, which is characterized in that the kettle cover connection blow-down pipe and pressure
Table, agitating paddle, the blow-down pipe, the pressure gauge, the agitating paddle are connected to autoclave body inside, and the agitating paddle is logical
Cross kettle cover access kettle body bottom.
9. Zeolite synthesis device as described in claim 1, which is characterized in that the heating unit is an electric heating cover.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721540120.6U CN207680597U (en) | 2017-11-17 | 2017-11-17 | A kind of Zeolite synthesis device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721540120.6U CN207680597U (en) | 2017-11-17 | 2017-11-17 | A kind of Zeolite synthesis device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207680597U true CN207680597U (en) | 2018-08-03 |
Family
ID=62990125
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721540120.6U Active CN207680597U (en) | 2017-11-17 | 2017-11-17 | A kind of Zeolite synthesis device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207680597U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109482126A (en) * | 2018-12-19 | 2019-03-19 | 江苏久诺建材科技股份有限公司 | A kind of reaction kettle for lacquer production |
| CN112174287A (en) * | 2020-09-27 | 2021-01-05 | 同济大学 | Non-contact continuous feeding and automatic reaction kitchen waste normal-pressure oxidation device |
| CN114588869A (en) * | 2021-06-27 | 2022-06-07 | 长春汇维科技股份有限公司 | Chemical combination device with automatic chemical combination/rinsing function and chemical combination/rinsing method |
-
2017
- 2017-11-17 CN CN201721540120.6U patent/CN207680597U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109482126A (en) * | 2018-12-19 | 2019-03-19 | 江苏久诺建材科技股份有限公司 | A kind of reaction kettle for lacquer production |
| CN112174287A (en) * | 2020-09-27 | 2021-01-05 | 同济大学 | Non-contact continuous feeding and automatic reaction kitchen waste normal-pressure oxidation device |
| CN114588869A (en) * | 2021-06-27 | 2022-06-07 | 长春汇维科技股份有限公司 | Chemical combination device with automatic chemical combination/rinsing function and chemical combination/rinsing method |
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