CN207655147U - A kind of helical-ribbon type chemical reaction device - Google Patents
A kind of helical-ribbon type chemical reaction device Download PDFInfo
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- CN207655147U CN207655147U CN201721587662.9U CN201721587662U CN207655147U CN 207655147 U CN207655147 U CN 207655147U CN 201721587662 U CN201721587662 U CN 201721587662U CN 207655147 U CN207655147 U CN 207655147U
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- shell
- ribbon type
- helical
- chemical reaction
- fixedly connected
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Abstract
A kind of helical-ribbon type chemical reaction device, reaction unit including support device and in the support device, the reaction unit is equipped with shell, the shell is internally provided with helix(ribbon type) agitator, the helix(ribbon type) agitator is equipped with fixed block, the lower section of the fixed block is equipped with swing arm, and the swing arm is fixedly connected by fixed block with helix(ribbon type) agitator;The inner wall of the shell is equipped with freezing liquid interlayer, the lower section of the freezing liquid interlayer is equipped with circulating pump, the circulating pump is fixedly connected by freezing liquid interlayer with shell, the side of the shell is equipped with electric-controlled plate, the surface of the electric-controlled plate is equipped with conducting wire, and the electric-controlled plate is electrically connected by conducting wire and the heating plate set on the outer casing bottom.It in the utility model, can be handled convenient for the SAPMAC method of reaction unit by being provided with the circulating pump of freezing liquid interlayer, by being provided with the electric-controlled plate of heating plate, be convenient for thermal response processing, have the advantages of simple structure and easy realization.
Description
Technical field
The utility model is related to technical field of chemical reaction devices, more particularly to a kind of helical-ribbon type chemical reaction device.
Background technology
Reactor is a kind of equipment for realizing reaction process, is widely used in the fields such as chemical industry, oil refining, metallurgy.Reactor
For realizing the heterogeneous reaction process such as single liquid phase reaction process and the solid, gas-liquid-solid of liquid liquid, gas-liquid, liquid, this patent is absorbed in one
Kind is concerning in N, the product of N'- carbonyl dimidazoles, N, N'- carbonyl dimidazoles, alias 1,1'- carbonyl dimidazoles, 1,1'- carbonyls, two miaow
Azoles and carbonyl dimidazoles, molecular formula C7H6N4O, molecular weight 162.15, white crystal are mainly used for organic synthesis and pesticide, doctor
Medicine intermediate.
In the prior art, in the processing procedure of reactor, for realizing single liquid phase reaction process and liquid liquid, gas-liquid,
The heterogeneous reaction process such as the solid, gas-liquid-solid of liquid.Being set up in device has stirring (mechanical agitation, airflow stirring etc.) device.Ratio of height to diameter compared with
When big, multiple impellers leaf can be used.When material need to be heated or cooled during the reaction, chuck can be set at reactor wall,
Or heat-transfer surface is set in device, it can also be exchanged heat by outer circulation.
Above-mentioned processing mode, to N, in the reaction treatment of the product of N'- carbonyl dimidazoles, there are one in versatility
Fixed defect, when existing reaction unit is effectively reacted, because the product boiling point of N, N'- carbonyl dimidazoles is higher, and not
It is dissolved in water, is needed in the case of carrying out hot-working reaction cooperation SAPMAC method crystallization, is needed to be equipped with different devices, increase fund
Input and place occupy.
Utility model content
Based on this, the purpose of this utility model is to provide a kind of helical-ribbon type chemical reaction device.
To solve the above problems, the utility model provides the following technical solutions:A kind of helical-ribbon type chemical reaction device, including
Support device and the reaction unit in the support device, the reaction unit are equipped with shell, the inside of the shell
Equipped with helix(ribbon type) agitator, the helix(ribbon type) agitator is equipped with fixed block, and the lower section of the fixed block is equipped with swing arm, the rotation
Bar is fixedly connected by fixed block with helix(ribbon type) agitator;The inner wall of the shell is equipped with freezing liquid interlayer, the freezing liquid
The lower section of interlayer is equipped with circulating pump, and the circulating pump is fixedly connected by freezing liquid interlayer with shell, and the side of the shell is set
There are electric-controlled plate, the surface of the electric-controlled plate to be equipped with conducting wire, the electric-controlled plate passes through conducting wire and the heating for being set to the outer casing bottom
Plate is electrically connected.
As a kind of preferred embodiment of the utility model, the surface of the swing arm is equipped with reinforcing bar, the reinforcing bar
It is fixedly connected with swing arm.
As a kind of preferred embodiment of the utility model, the end of the reinforcing bar is equipped with vane, and the vane is logical
Reinforcing bar is crossed to be fixedly connected with swing arm.
As a kind of preferred embodiment of the utility model, the support device is equipped with fixed ear, the fixed ear
Upper setting holder, the holder are fixedly connected by fixed ear with support device.
As a kind of preferred embodiment of the utility model, the top of the fixed ear is equipped with feeder, the pan feeding
The side of device is equipped with motor, and the feeder is fixedly connected by the fixed ear on shell with holder.
As a kind of preferred embodiment of the utility model, the both sides of the feeder are equipped with connecting shaft, the pan feeding
Device is connected by connecting shaft and shell.
As a kind of preferred embodiment of the utility model, the top of the shell is equipped with air gauge, the shell
Side is equipped with outlet, and the air gauge, outlet are all fixedly connected with shell.
Compared with prior art, the beneficial effects of the utility model are as follows:
1. by the one group of freezing liquid interlayer that is internally provided in shell, a circulating pump is arranged in freezing liquid interlayer and lower section,
Freezing liquid progress can be promoted to be recycled in the inside of shell, play good SAPMAC method knot by the circulating effect of circulating pump
Brilliant effect.
2. by the way that two groups of heating plates are arranged in the inside of shell, after being attached by conducting wire and electric-controlled plate, can heat
Plate is energized, and cooperation helix(ribbon type) agitator can carry out rotary heating to raw material, convenient for reinforcing reaction effect.
Description of the drawings
Fig. 1 is a kind of structural schematic diagram of helical-ribbon type chemical reaction device in one embodiment of the utility model;
Fig. 2 is the schematic diagram of the helix(ribbon type) agitator in Fig. 1.
In figure:1- support devices, 2- fixed ears, 3- holders, 4- feeders, 5- motors, 6- connecting shafts, 7- reaction units,
8- shells, 9- air gauges, the outlets 10-, 11- freezing liquids interlayer, 12- circulating pumps, 13- helix(ribbon type) agitators, 14- fixed blocks,
15- swing arms, 16- reinforcing bars, 17- vanes, 18- electric-controlled plates, 19- conducting wires, 20- heating plates.
Following specific implementation mode will further illustrate the utility model in conjunction with above-mentioned attached drawing.
Specific implementation mode
The utility model is more fully retouched below with reference to relevant drawings for the ease of understanding the utility model,
It states.Several embodiments of the utility model are given in attached drawing.But the utility model can in many different forms come in fact
It is existing, however it is not limited to embodiment described herein.Make public affairs to the utility model on the contrary, purpose of providing these embodiments is
It is more thorough and comprehensive to open content.
It should be noted that when element is referred to as " being fixedly arranged on " another element, it can be directly on another element
Or there may also be elements placed in the middle.When an element is considered as " connection " another element, it can be directly connected to
To another element or it may be simultaneously present centering elements.Term as used herein " vertical ", " horizontal ", " left side ",
" right side " and similar statement are for illustrative purposes only.
Unless otherwise defined, all of technologies and scientific terms used here by the article is led with the technology for belonging to the utility model
The normally understood meaning of technical staff in domain is identical.Terminology used in the description of the utility model herein only be
The purpose of description specific embodiment, it is not intended that in limitation the utility model.Term " and or " used herein includes
Any and all combinations of one or more relevant Listed Items.
It please refers to Fig.1 to Fig. 2, a kind of helical-ribbon type chemical reaction device provided in one embodiment of the utility model, including
Support device 1 and reaction unit 7 set on the support device 1, the reaction unit 7 are equipped with shell 8, the shell 8
It is internally provided with helix(ribbon type) agitator 13, the helix(ribbon type) agitator 13 is equipped with fixed block 14, and the lower section of the fixed block 14 is set
There are swing arm 15, the swing arm 15 to be fixedly connected with helix(ribbon type) agitator 13 by fixed block 14, the setting of swing arm 15 is convenient for reinforcing
The setting of bar 16;The inner wall of the shell 8 is equipped with freezing liquid interlayer 11, and the lower section of the freezing liquid interlayer 11 is equipped with circulating pump
12, the circulating pump 12 is fixedly connected by freezing liquid interlayer 11 with shell 8, and the side of the shell 8 is equipped with electric-controlled plate 18, institute
The surface for stating electric-controlled plate 18 is equipped with conducting wire 19, and the electric-controlled plate 18 passes through conducting wire 19 and the heating plate for being set to 8 bottom of the shell
20 are electrically connected.
Referring to Fig. 2, the surface of the swing arm 15 is equipped with reinforcing bar 16, the reinforcing bar 16 is fixedly connected with swing arm 15,
The setting of reinforcing bar 16 is convenient for increasing the durability of vane 17.
Referring to Fig. 2, the end of the reinforcing bar 16 is equipped with vane 17, the vane 17 passes through reinforcing bar 16 and swing arm 15
It is fixedly connected, the setting of vane 17 is convenient for increase rotatory.
Referring to Fig. 1, the support device 1 is equipped with fixed ear 2, holder 3, the holder are set in the fixed ear 2
3 are fixedly connected by fixed ear 2 with support device 1.The top of the fixed ear 2 is equipped with feeder 4, the side of the feeder 4
Face is equipped with motor 5, and the feeder 4 is fixedly connected by the fixed ear 2 on shell 8 with holder 3, and the setting of feeder 4 is convenient for
Carry out the entrance of raw material.
Referring to Fig. 1, the both sides of the feeder 4 are equipped with connecting shaft 6, the feeder 4 passes through connecting shaft 6 and shell 8
It connects, connecting shaft 6 is used convenient for cooperation shell 8.
Referring to Fig. 1, the top of the shell 8 is equipped with air gauge 9, the side of the shell 8 is equipped with outlet 10, the gas
Pressure table 9, outlet 10 are all fixedly connected with shell 8, and the setting of air gauge 9 is convenient for effectively detecting reaction unit 7.
Operation principle:It, can be by the way that branch be arranged first by being provided with the fixed ear 2 of holder 3 in the both sides of support device
Frame 3, can effectively be supported, and be provided with the feeder 4 of motor 5 above, effective built-in convenient for raw material progress, secondly
Helix(ribbon type) agitator 13 is set in the inside of shell 8, the vane 17 with reinforcing bar 16 can be coordinated by swing arm 15, can coordinate and add
It is effectively stirred while hot plate 20 is internally heated reaction unit 7, increases reaction effect, then in shell 8
Inside setting freezing liquid interlayer 11, freezing liquid interlayer 11 can be carried out effective by the circulating pump 12 of lower section in the inside of shell 8
Cycle, the SAPMAC method of complex reaction device 7 carries out crystallization reaction, and the setting of double reaction increases versatility, reduces money
The input of gold.
Certain embodiment of the utility model above described embodiment only expresses, the description thereof is more specific and detailed,
But it should not be understood as limiting the scope of the patent of the utility model.It should be pointed out that for the common of this field
For technical staff, without departing from the concept of the premise utility, various modifications and improvements can be made, these all belong to
In the scope of protection of the utility model.Therefore, the protection domain of the utility model patent should be determined by the appended claims.
Claims (7)
1. a kind of helical-ribbon type chemical reaction device, including support device (1) and the reaction unit in the support device (1)
(7), it is characterised in that:The reaction unit (7) includes shell (8), and the shell (8) is internally provided with helix(ribbon type) agitator
(13), the helix(ribbon type) agitator (13) is equipped with fixed block (14), and the lower section of the fixed block (14) is equipped with swing arm (15), institute
Swing arm (15) is stated to be fixedly connected with helix(ribbon type) agitator (13) by fixed block (14);The reaction unit (7) is equipped with shell
(8), the inner wall of the shell (8) is equipped with freezing liquid interlayer (11), and the lower section of the freezing liquid interlayer (11) is equipped with circulating pump
(12), the circulating pump (12) is fixedly connected by freezing liquid interlayer (11) with shell (8), and the side of the shell (8) is equipped with
Electric-controlled plate (18), the surface of the electric-controlled plate (18) are equipped with conducting wire (19), the electric-controlled plate (18) by conducting wire (19) be set to
The heating plate (20) of shell (8) bottom is electrically connected.
2. helical-ribbon type chemical reaction device according to claim 1, which is characterized in that the surface of the swing arm (15) is equipped with
Reinforcing bar (16), the reinforcing bar (16) are fixedly connected with swing arm (15).
3. helical-ribbon type chemical reaction device according to claim 2, which is characterized in that the end of the reinforcing bar (16) is set
There are vane (17), the vane (17) to be fixedly connected with swing arm (15) by reinforcing bar (16).
4. helical-ribbon type chemical reaction device according to claim 1, which is characterized in that the support device (1) is equipped with
Fixed ear (2), setting holder (3) on the fixed ear (2), the holder (3) are solid by fixed ear (2) and support device (1)
Fixed connection.
5. helical-ribbon type chemical reaction device according to claim 4, which is characterized in that set below the fixed ear (2)
There are holder (3), the top of the fixed ear (2) to be equipped with feeder (4), the side of the feeder (4) is equipped with motor (5), institute
Feeder (4) is stated to be fixedly connected with holder (3) by the fixed ear (2) on shell (8).
6. helical-ribbon type chemical reaction device according to claim 5, which is characterized in that the both sides of the feeder (4) are set
There are connecting shaft (6), the feeder (4) to be connected by connecting shaft (6) and shell (8).
7. helical-ribbon type chemical reaction device according to claim 1, which is characterized in that the top of the shell (8) is equipped with
The side of air gauge (9), the shell (8) is equipped with outlet (10), and the air gauge (9), outlet (10) are all fixed with shell (8)
Connection.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201721587662.9U CN207655147U (en) | 2017-11-24 | 2017-11-24 | A kind of helical-ribbon type chemical reaction device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201721587662.9U CN207655147U (en) | 2017-11-24 | 2017-11-24 | A kind of helical-ribbon type chemical reaction device |
Publications (1)
Publication Number | Publication Date |
---|---|
CN207655147U true CN207655147U (en) | 2018-07-27 |
Family
ID=62946301
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201721587662.9U Expired - Fee Related CN207655147U (en) | 2017-11-24 | 2017-11-24 | A kind of helical-ribbon type chemical reaction device |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN207655147U (en) |
-
2017
- 2017-11-24 CN CN201721587662.9U patent/CN207655147U/en not_active Expired - Fee Related
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Date | Code | Title | Description |
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GR01 | Patent grant | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180727 Termination date: 20201124 |