CN207632748U - A kind of White Mineral Oil special production apparatus of classification removal micro-moisture - Google Patents

A kind of White Mineral Oil special production apparatus of classification removal micro-moisture Download PDF

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Publication number
CN207632748U
CN207632748U CN201721779602.7U CN201721779602U CN207632748U CN 207632748 U CN207632748 U CN 207632748U CN 201721779602 U CN201721779602 U CN 201721779602U CN 207632748 U CN207632748 U CN 207632748U
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CN
China
Prior art keywords
moisture
filler
hypergravity
micro
mineral oil
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Expired - Fee Related
Application number
CN201721779602.7U
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Chinese (zh)
Inventor
莫学坤
徐冰冰
贾威阵
崔玉金
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Zhejiang Zhengxin Petroleum Technology Co Ltd
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Zhejiang Zhengxin Petroleum Technology Co Ltd
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Priority to CN201721779602.7U priority Critical patent/CN207632748U/en
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Abstract

The utility model discloses a kind of White Mineral Oil special production apparatus of classification removal micro-moisture.The device includes by the sequentially connected Mixer pot of pipeline, first step drier, hypergravity de-watering apparatus, first step drier is deflector type fixed bed drying device, inside set the first filler, second filler is set in hypergravity de-watering apparatus, the design of deflector type filler can increase the contact area of material in drier, just water rem oval be improved, then through hypergravity equipment, micro-moisture is removed, with the entire removal process of batches about 5min.In the fixed bed drying device of the first step, the water content of processed oil product is less than 40ppm, meet basic oil product water removal to require, this is walked out of oil and removes more micro moisture through hypergravity equipment, the water content of oil product is 10 25ppm, can be applied to catalyst industry, whole device is small, conveniently moving, it is efficient.

Description

A kind of White Mineral Oil special production apparatus of classification removal micro-moisture
Technical field
The utility model is related to a kind of White Mineral Oil special production apparatus more particularly to a kind of classification to remove the white of micro-moisture Dormant oil special production apparatus belongs to Petrochemical Production Technologies field.
Background technology
In White Mineral Oil production process, there is no special requirements to moisture for the White Mineral Oil or White Mineral Oil of general applications.But Be in the field of particular/special requirement, as transformer oil production in, it is desirable that oil in water content be no more than 70ppm, it is fine in winter It is produced under bright weather condition, production requirement can be reached, but in the case that southern air humidity is relatively high, without water removal Equipment, oil product cannot be satisfied requirement.The dedicated White Mineral Oil of catalyst, moisture requirement is no more than 25ppm, in common production technology Under, requirement is cannot be satisfied, therefore can generally be removed water by heating.But only heating water removal in current water removal device, can only will be oily Free water and floating water in product remove, and fat liquor system is even formd for the micro moisture being dispersed in oil Moisture, it is more difficult to remove.Water removal device relatively advanced at present, is filtered using clay, adsorbs micro-moisture.The technology and device Defect be:Water removal is unable to reach lower level most down to 35ppm;Batch production removes water time about 20- every time 40min;Equipment occupation space is larger, and water-absorbent material is single, and carclazyte needs replacement processing repeatedly, Reusability less efficient; And pre-treatment needs to heat and can be only achieved water removal purpose, and whole efficiency is low, and energy consumption is high, and micro-moisture can not remove.Excessively add Heat can cause White Mineral Oil to turn yellow, to which product is rotten.
The utility model uses multistep treatment, using deflector type fixed bed drying device, connects hypergravity de-watering apparatus, at different levels Using different fillers, whole device is small, and conveniently moving, heating time is short, and sectional removes moisture, to meet different product Requirement, low power consuming, high efficiency, can will water removal the time foreshorten to 5min.
Utility model content
The purpose of this utility model is that generally requiring heating for existing water removal device could remove water, and remove water the time The defects of length, energy consumption is high, while micro moisture can not remove provides a kind of special life of White Mineral Oil of classification removal micro-moisture Produce device.The device uses baffling using fixed bed drying device and the cooperation classification water removal of hypergravity equipment especially in drier Formula filler designs, and increases the contact area of material, improves just water rem oval, then through hypergravity equipment, removes micro-moisture, together The entire removal process of batches about 5min.In the fixed bed drying device of the first step, the water content of processed oil product is less than 40ppm meets basic oil product water removal and requires, this is walked out of oil and removes more micro moisture through hypergravity equipment, and oil product contains Water is 10-25ppm, can be applied to catalyst industry, subsequently canned through whole process sealing, ensures oil quality.
The White Mineral Oil special production apparatus of the classification removal micro-moisture of the utility model, including be sequentially connected by pipeline Mixer pot, first step drier, hypergravity de-watering apparatus and the pump being used to provide power;The first step drier is Deflector type fixed bed drying device, it is internal to use Multi-level deflector formula pipeline, it is equipped with the first filler in deflector type pipeline, hypergravity removes Second filler is set in water installations, in the connecting pipe of Mixer pot and deflector type fixed bed drying device, deflector type fixed bed drying It is equipped with the oil outlet controlled by valve in the connecting pipe of device and hypergravity de-watering apparatus.
First filler is anhydrous calcium chloride, anhydrous magnesium chloride, silica gel, atlapulgite, A type molecular sieve or X-type point Son sieve.
Second filler is A type molecular sieve, Y type molecular sieve or X-type molecular sieve.
The device of the utility model then may be used to the product of moisture no requirement (NR) in use, White Mineral Oil first passes through Mixer pot reconciliation Directly to become finished product by canned by Mixer pot oil outlet.There is the product of strict demand then to enter the first step moisture to dry Device, deflector type fixed bed drying device, oil product carry out comprehensive engagement in drier, by deflector type and filler, are provided by pump dynamic Power carries out primary dry water removal by fixed bed drying device, and whole process does not cause to damage without heating equipment to oil quality. Water removal can make the water content of oil product be down to 30-45ppm herein, if desired can be directly canned at this by the oil outlet of drier The finished product of grade.In requirement higher of the catalyst industry to White Mineral Oil product, need to use more accurate micro water removal Equipment, therefore oil product need to enter super-gravity device, under the high speed rotation of super-gravity device, oil product is dispersed into minimum list Position, respectively by filler, micro-moisture is spread out at this time, is adsorbed when passing through filler, to cause denier moisture and White Mineral Oil separates, and molecular sieve filling is used in hypergravity de-watering apparatus, molecular sieve is utilized to White Mineral Oil without adsorption energy The property of power.Entire separation process about 3min, and super-gravity device can continue working, ensure that the efficient of separation, precisely. The product detached herein can reach 10-25ppm, meet catalyst industry or to the more stringent row of White Mineral Oil moisture requirement The demand of industry, subsequently canned to need whole process closed canned, reduction is contacted with air, and moisture in air is avoided to enter White Mineral Oil product In.
The utility model has the beneficial effects that:
1. by hypergravity equipment application to dewatering process, water rem oval is improved, shortens material (grease) disengaging time, together When micro-moisture can be separated.
2. fixed bed drying device uses deflector type filler, the comprehensive engagement of material, water rem oval higher, liquid flow ensure that Dynamic speed is faster.
3. entire water removal device high-efficiency operation, removal process about 5min can be completed, and reduce the influence to White Mineral Oil quality.
4. can according to water removal require, carry out classification water removal it is canned, grading is clear.
5. the occupied space of whole device is smaller, space is greatly saved, while the mobility of equipment is strong, it can be to difference White Mineral Oil product and there are other White Mineral Oil products of particular/special requirement to carry out water removal and accurate micro water removal.
Description of the drawings
Fig. 1 is the structural schematic diagram of utility model device.
Specific implementation mode
Referring to Fig.1, the White Mineral Oil special production apparatus of the classification removal micro-moisture of the utility model, including pass through pipeline The trend of sequentially connected Mixer pot, first step drier, hypergravity de-watering apparatus, White Mineral Oil provides power by pump;Described First step drier is deflector type fixed bed drying device, internal to use Multi-level deflector formula pipeline, and the is equipped in deflector type pipeline One filler, the first filler are anhydrous calcium chloride, anhydrous magnesium chloride, silica gel, atlapulgite, A type molecular sieve or X-type molecular sieve.It is super Second filler is set in gravity de-watering apparatus, and the second filler uses A type molecular sieve, Y type molecular sieve or X-type molecular sieve.It is reconciling The connecting pipe of tank and deflector type fixed bed drying device, the connecting pipe of deflector type fixed bed drying device and hypergravity de-watering apparatus On be equipped with the oil outlet controlled by valve.The device such as CN206082411U may be used in the Mixer pot of the present invention, through reconciling Afterwards, directly canned to the product of moisture no requirement (NR) is finished product.The product finely removed water is needed, enters fixed bed deflector type through pipeline Drier, through repeatedly reverse-flow type water removal after, reach moisture requirement, to moisture requirement grade in 30-50ppm can be straight Cans picking dresses up finished product.The follow-up removing for needing denier moisture, oil product enter hypergravity de-watering apparatus through pipeline, are revolved through high speed Turning, oil product is dispersed into nano sized particles, is more easy to make packing material absorbing moisture, after water-oil separating, the leakage fluid dram separation below product device Out, whole sealing is canned after pipeline.Obtain the oil product of water content 10-25ppm.

Claims (3)

1. a kind of White Mineral Oil special production apparatus of classification removal micro-moisture, which is characterized in that including being connected successively by pipeline Mixer pot, first step drier, hypergravity de-watering apparatus and the pump being used to provide power connect;The first step drier It is internal to use deflector type pipeline for deflector type fixed bed drying device, the first filler, hypergravity water removal are equipped in deflector type pipeline Second filler is set in device, in the connecting pipe of Mixer pot and deflector type fixed bed drying device, deflector type fixed bed drying device And the oil outlet controlled by valve is equipped in the connecting pipe of hypergravity de-watering apparatus.
2. the White Mineral Oil special production apparatus of classification removal micro-moisture according to claim 1, which is characterized in that described The first filler be anhydrous calcium chloride, anhydrous magnesium chloride, silica gel, atlapulgite, A type molecular sieve or X-type molecular sieve.
3. the White Mineral Oil special production apparatus of classification removal micro-moisture according to claim 1, which is characterized in that described The second filler be A type molecular sieve, Y type molecular sieve or X-type molecular sieve.
CN201721779602.7U 2017-12-19 2017-12-19 A kind of White Mineral Oil special production apparatus of classification removal micro-moisture Expired - Fee Related CN207632748U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721779602.7U CN207632748U (en) 2017-12-19 2017-12-19 A kind of White Mineral Oil special production apparatus of classification removal micro-moisture

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721779602.7U CN207632748U (en) 2017-12-19 2017-12-19 A kind of White Mineral Oil special production apparatus of classification removal micro-moisture

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CN207632748U true CN207632748U (en) 2018-07-20

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109308961A (en) * 2018-11-24 2019-02-05 运城清海科技有限公司 A kind of transformer dry equipment
CN109692503A (en) * 2019-01-24 2019-04-30 湖南昊华化工有限责任公司 A kind of device and method removing minim moisture from organic solvent

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109308961A (en) * 2018-11-24 2019-02-05 运城清海科技有限公司 A kind of transformer dry equipment
CN109308961B (en) * 2018-11-24 2024-03-08 运城清海科技有限公司 Transformer drying equipment
CN109692503A (en) * 2019-01-24 2019-04-30 湖南昊华化工有限责任公司 A kind of device and method removing minim moisture from organic solvent

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GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180720

Termination date: 20191219

CF01 Termination of patent right due to non-payment of annual fee