CN207576411U - For the hydrolysis kettle of bis- chloro- 5- fluorobenzoyl chlorides preparation process of 2,4- - Google Patents
For the hydrolysis kettle of bis- chloro- 5- fluorobenzoyl chlorides preparation process of 2,4- Download PDFInfo
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- CN207576411U CN207576411U CN201721696246.2U CN201721696246U CN207576411U CN 207576411 U CN207576411 U CN 207576411U CN 201721696246 U CN201721696246 U CN 201721696246U CN 207576411 U CN207576411 U CN 207576411U
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Abstract
The utility model discloses the hydrolysis kettle for 2,4 dichloro, 5 fluorobenzoyl chloride preparation process, including head cover, feed inlet, handle, motor, shaft, autoclave body, supporting rack, valve, liquid outlet, pedestal, paddle, bearing, isolation board and snap-gauge.The beneficial effects of the utility model are：Snap-gauge is socketed on shaft surface, and snap-gauge is movably connected with shaft, the normal operation of shaft is not influenced, isolation board can effectively prevent the sputtering of stirring liquid, so that stirring region reduces, so that the reflux of stirring liquid is rapider, enhance stirring efficiency, and paddle is in flabellum shape structure, so that stirring leaf area bigger, stirring is more abundant, equally enhance stirring efficiency, isolation board is threaded by handle and autoclave body, convenient for the installation and dismounting of isolation board, enhance the practicability of device, autoclave body and supporting rack, head cover is in be fixedly connected, so that apparatus structure connection is even closer firm, enhance the stability of device.
Description
Technical field
The utility model is related to a kind of hydrolysis kettle, particularly for the water of 2,4-, bis- chloro- 5- fluorobenzoyl chlorides preparation process
Kettle is solved, belongs to hydrolysis kettle application field.
Background technology
2,4- bis- chloro- 5- fluorobenzoyl chlorides are a kind of synthetics, which is colourless or yellowish liquid, is a kind of corruption
Corrosion liquid, needs to use in preparation process is produced hydrolysis kettle, but existing hydrolysis kettle appoints so that there are one when in use
Determine defect, the existing hydrolysis kettle being used in 2,4-, bis- chloro- 5- fluorobenzoyl chlorides preparation process stirring efficiency in use
Often not enough efficiently, inner space causes greatly liquid splash serious, it is impossible to and reflux is effectively formed, and is commonly used in 2,4- bis-
Isolation board is often not provided with inside hydrolysis kettle in chloro- 5- fluorobenzoyl chlorides preparation process, liquid has certain general in sputtering
Rate is splashed to outside, and unexpected injury is caused to human body, therefore, is proposed regarding to the issue above for 2,4-, bis- chloro- 5- fluorobenzoyls
The hydrolysis kettle of chlorine preparation process.
Utility model content
The purpose of this utility model is that solve the above-mentioned problems and provides for bis- chloro- 5- fluorobenzoyl chlorides of 2,4-
The hydrolysis kettle of preparation process.
The utility model is achieved through the following technical solutions above-mentioned purpose, is used for, and-dichloro -- prepared by fluorobenzoyl chloride
The hydrolysis kettle of journey, including autoclave body, the autoclave body bottom both sides are provided with supporting rack, and support frame as described above bottom is provided with pedestal, institute
It states both sides at the top of autoclave body and is provided with feed inlet, and head cover is provided at the top of the autoclave body, the head cover is internally provided with motor, institute
It states motor bottom and is connected with shaft, described shaft one end is provided with bearing, and the shaft surface is provided with several paddles, institute
It states and is socketed with snap-gauge at the top of shaft, the snap-gauge is connected with an isolation board, and described isolation board one end is connected with handle, the autoclave body
Bottom end is provided with a liquid outlet, and the liquid outlet is internally provided with a valve.
Preferably, for the ease of the normal rotation of rotation axis, the snap-gauge is socketed on the shaft surface, and the snap-gauge
It is movably connected with the shaft.
Preferably, in order to make apparatus structure even closer firm, the autoclave body is with support frame as described above, the head cover in fixation
Connection.
Preferably, for the ease of the adjusting of isolation board, the isolation board is connected by the handle and the autoclave body in screw thread
It connects.
Preferably, in order to enhance stirring efficiency, make stirring more abundant, the paddle is in flabellum shape structure.
The beneficial effects of the utility model are：Snap-gauge is socketed on shaft surface, and snap-gauge is movably connected with shaft, not shadow
The normal operation of shaft is rung, isolation board can effectively prevent the sputtering of stirring liquid so that stirring region reduces, so that stirring liquid
Reflux it is rapider, enhance stirring efficiency, and paddle be in flabellum shape structure so that stirring leaf area bigger, stirring more
Fully, equally enhance stirring efficiency, isolation board is threaded by handle and autoclave body, convenient for isolation board installation with tearing open
It unloads, and certain adjusting can be carried out to the position of isolation board according to actual conditions, enhance the practicability of device, autoclave body and branch
Support, head cover are in be fixedly connected so that apparatus structure connection is even closer firm, enhances the stability of device.
Description of the drawings
Fig. 1 is the utility model overall structure diagram.
Fig. 2 is regional enlarged drawing at the utility model A.
In figure：1st, head cover；2nd, feed inlet；3rd, handle；4th, motor；5th, shaft；6th, autoclave body；7th, supporting rack；8th, valve；9th, go out
Liquid mouth；10th, pedestal；11st, paddle；12nd, bearing；13rd, isolation board；14th, snap-gauge.
Specific embodiment
The following is a combination of the drawings in the embodiments of the present utility model, and the technical scheme in the embodiment of the utility model is carried out
It clearly and completely describes, it is clear that the described embodiments are only a part of the embodiments of the utility model rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are without making creative work
All other embodiments obtained shall fall within the protection scope of the present invention.
It please refers to Fig.1 shown in -2, for the hydrolysis kettle of 2,4-, bis- chloro- 5- fluorobenzoyl chlorides preparation process, including autoclave body 6,
6 two bottom sides of autoclave body are provided with supporting rack 7, and 7 bottom of supporting rack is provided with pedestal 10, and 6 top both sides of autoclave body are provided with feed inlet
2, and 6 top of autoclave body is provided with head cover 1, head cover 1 is internally provided with motor 4, and 4 bottom of motor is connected with shaft 5,5 one end of shaft
Bearing 12 is provided with, and 5 surface of shaft is provided with several paddles 11,5 top of shaft is socketed with snap-gauge 14, and snap-gauge 14 is connected with
One isolation board 13,13 one end of isolation board are connected with handle 3, and 6 bottom end of autoclave body is provided with a liquid outlet 9, and liquid outlet 9 is internally provided with
One valve 8.
As a kind of technical optimization scheme of the utility model, snap-gauge 14 is socketed on 5 surface of shaft, and snap-gauge 14 and shaft
5 are movably connected.
As a kind of technical optimization scheme of the utility model, autoclave body 6 is in be fixedly connected with supporting rack 7, head cover 1.
As a kind of technical optimization scheme of the utility model, isolation board 13 is threaded by handle 3 and autoclave body 6.
As a kind of technical optimization scheme of the utility model, paddle 11 is in flabellum shape structure.
When the utility model is used, first, hydrolysis kettle is positioned over suitable position, liquid to be mixed is respectively placed in
Inside feed inlet 2, entered inside autoclave body 6 by feed inlet 2, at this point, closing liquid outlet 9 by control valve 8, when to be mixed
After liquid inputs, isolation board 13 is adjusted by handle 3 so that snap-gauge 4 is closed and is socketed on 5 surface of shaft, then starts
Motor 4, motor 4 drive shaft 5 to rotate, and shaft 5 rotates, and paddle 11 is driven to rotate, mixing liquid is sufficiently stirred,
After the completion of stirring, motor 4 is closed, after shaft 5 is totally stationary, control valve 8 causes liquid outlet 9 to open, and makes after being sufficiently stirred
Liquid flowed out by liquid outlet 9, complete hydrolytic process.
It is obvious to a person skilled in the art that the utility model is not limited to the details of above-mentioned exemplary embodiment, and
And in the case of the spirit or essential attributes without departing substantially from the utility model, it can realize that this practicality is new in other specific forms
Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this practicality is new
The range of type is indicated by the appended claims rather than the foregoing description, it is intended that by containing in the equivalent requirements of the claims is fallen
All changes in justice and range are embraced therein.Any reference numeral in claim should not be considered as limitation
Involved claim.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in each embodiment can also be properly combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (5)
1. for the hydrolysis kettle of 2,4-, bis- chloro- 5- fluorobenzoyl chlorides preparation process, including autoclave body (6), it is characterised in that：The kettle
Body (6) two bottom sides are provided with supporting rack (7), and support frame as described above (7) bottom is provided with pedestal (10), autoclave body (6) top
Both sides are provided with feed inlet (2), and are provided with head cover (1) at the top of the autoclave body (6), and the head cover (1) is internally provided with motor
(4), motor (4) bottom is connected with shaft (5), and described shaft (5) one end is provided with bearing (12), and the shaft (5)
Surface is provided with several paddles (11), is socketed with snap-gauge (14) at the top of the shaft (5), the snap-gauge (14) be connected with one every
From plate (13), described isolation board (13) one end is connected with handle (3), and autoclave body (6) bottom end is provided with a liquid outlet (9), institute
It states liquid outlet (9) and is internally provided with a valve (8).
2. the hydrolysis kettle according to claim 1 for being used for 2,4-, bis- chloro- 5- fluorobenzoyl chlorides preparation process, feature exist
In：The snap-gauge (14) is socketed on the shaft (5) surface, and the snap-gauge (14) is movably connected with the shaft (5).
3. the hydrolysis kettle according to claim 1 for being used for 2,4-, bis- chloro- 5- fluorobenzoyl chlorides preparation process, feature exist
In：The autoclave body (6) and support frame as described above (7), the head cover (1) are in being fixedly connected.
4. the hydrolysis kettle according to claim 1 for being used for 2,4-, bis- chloro- 5- fluorobenzoyl chlorides preparation process, feature exist
In：The isolation board (13) is threaded by the handle (3) and the autoclave body (6).
5. the hydrolysis kettle according to claim 1 for being used for 2,4-, bis- chloro- 5- fluorobenzoyl chlorides preparation process, feature exist
In：The paddle (11) is in flabellum shape structure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721696246.2U CN207576411U (en) | 2017-12-08 | 2017-12-08 | For the hydrolysis kettle of bis- chloro- 5- fluorobenzoyl chlorides preparation process of 2,4- |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721696246.2U CN207576411U (en) | 2017-12-08 | 2017-12-08 | For the hydrolysis kettle of bis- chloro- 5- fluorobenzoyl chlorides preparation process of 2,4- |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207576411U true CN207576411U (en) | 2018-07-06 |
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ID=62736677
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721696246.2U Active CN207576411U (en) | 2017-12-08 | 2017-12-08 | For the hydrolysis kettle of bis- chloro- 5- fluorobenzoyl chlorides preparation process of 2,4- |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207576411U (en) |
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2017
- 2017-12-08 CN CN201721696246.2U patent/CN207576411U/en active Active
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: 213034 basic chemical industry zone, Xingang District, Chunjiang Town, Xinbei District, Changzhou City, Jiangsu Province Patentee after: Jiangsu Feiyu Medical Technology Co.,Ltd. Address before: 213100 basic chemical industry zone, Xingang District, Chunjiang Town, Xinbei District, Changzhou City, Jiangsu Province Patentee before: CHANGZHOU FEIYU CHEMICAL Co.,Ltd. |
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| CP03 | Change of name, title or address |