CN207576376U - A kind of chemical engineering experiment device convenient for control reaction process - Google Patents

A kind of chemical engineering experiment device convenient for control reaction process Download PDF

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Publication number
CN207576376U
CN207576376U CN201721206863.XU CN201721206863U CN207576376U CN 207576376 U CN207576376 U CN 207576376U CN 201721206863 U CN201721206863 U CN 201721206863U CN 207576376 U CN207576376 U CN 207576376U
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reative cell
reaction process
chemical engineering
control reaction
suction
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祖象欢
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Jining Kang Sheng Rainbow Biological Technology Co Ltd
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Jining Kang Sheng Rainbow Biological Technology Co Ltd
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Abstract

The utility model discloses a kind of chemical engineering experiment devices convenient for control reaction process, including autoclave body, the autoclave body is divided into reative cell and conveying room, the centre position of the bottom end of the reative cell is equipped with motor, the bottom end of the motor is equipped with shaft, if arterial highway stirring rod is equidistantly installed in shaft, the side wall of the reative cell is equipped with and puts thermosphere, the outside for putting thermosphere is equipped with flowing water chamber, the top of the reative cell is equipped with aspiration pump, the right end of the aspiration pump is equipped with exhaust tube, if the exhaust tube stretches into reative cell and is connected with arterial highway suction branch, suction plate is equipped in the reative cell, if the suction plate is equipped with arterial highway suction hole, the suction branch is connected with suction hole;The beneficial effects of the utility model are:While accelerating reaction process, the variable of reaction can be more accurately controlled, using filtrate net, solid-liquid separation treatment is carried out to product, convenient for the collection of the product to different conditions.

Description

A kind of chemical engineering experiment device convenient for control reaction process
Technical field
The utility model is related to a kind of chemical engineering experiment equipment, specifically a kind of chemical engineering experiment dress convenient for control reaction process It puts.
Background technology
The relationship of the mankind and chemical industry is very close, spreads to the every aspect of life.In the modern life, almost at any time with Ground all be unable to do without chemical products, from material lifes such as food, clothing, housing and transportation to the cultural lives such as culture and arts, amusement, being required for Chemical product services for it.Some chemical products play epoch-making important function in human development history.Their production and Using in addition represent certain historical stage of human civilization.The product that chemical industry is provided to people be it is colourful, it in addition to Production lot of materials is used for other than being made used in various products behaviours, and the product that also dosage is seldom but effect is fairly obvious makes People’s lives are constantly improved.All chemical machineries of the chemical industry equipment including chemical industry equipment are all real in chemical plant Tool used by existing Chemical Manufacture.The control and guarantee of the normal operation of chemical products production process, product quality and yield, It is unable to do without the adaptation and normal operation of various chemical industry equipments.Existing major part chemical reaction is solid-liquid reaction, during reaction Control is inconvenient, it is difficult to the variation of the parameters in effective control reaction.
Utility model content
It is above-mentioned to solve the purpose of this utility model is to provide a kind of chemical engineering experiment device convenient for control reaction process The problem of being proposed in background technology.
To achieve the above object, the utility model provides following technical solution:
A kind of chemical engineering experiment device convenient for control reaction process, including autoclave body, the autoclave body is divided into reative cell and defeated Expect room, the centre position of the bottom end of the reative cell is equipped with motor, and the bottom end of the motor is equipped with shaft, in shaft If arterial highway stirring rod has been mounted equidistant, the side wall of the reative cell, which is equipped with, puts thermosphere, and the outside for putting thermosphere is equipped with stream Water cavity, the top of the reative cell are equipped with aspiration pump, and the right end of the aspiration pump is equipped with exhaust tube, the pumping If pipe stretches into reative cell and is connected with arterial highway suction branch, it is equipped with suction plate in the reative cell, in the suction plate If equipped with arterial highway suction hole, the suction branch is connected with suction hole, and the bottom end of the side of the reative cell is equipped with Inflator pump is equipped with appendix on the outlet side of the inflator pump, and the appendix stretches into the inner cavity of reative cell and company Air bag is connected to, the air bag is located at the bottom of reative cell, and the centre position of the baseplane of the reative cell is equipped with feed opening, The conveying room is located at the lower section of reative cell, is connected between the conveying room and reative cell by feed opening, described The inner cavity of conveying room is equipped with filtrate net, and the conveying room must be respectively arranged on the left side and the right side solid outlet and liquid outlet opening, The oblique upper of filtrate net that the solid outlet is located at, the liquid outlet opening are the obliquely downward of filtrate net.
As further program of the utility model:The flowing water chamber be fastened reative cell side wall and with putting heat Layer fits, and the upper and lower ends of the flowing water chamber are respectively equipped with water inlet pipe and drainpipe.
As further program of the utility model:The surface of the suction plate is equipped with waterproof membrane.
As further program of the utility model:The left and right sides of the feed opening is equipped with deflector.
As further program of the utility model:The inert gases such as nitrogen are used in the inflator pump.
As the utility model further scheme:The air bag is high molecule plastic material.
Compared with prior art, the beneficial effects of the utility model are:Conveying lid is opened, material is put into reative cell, Motor drives stirring rod rotation, is stirred operation to material, accelerates the process of chemical reaction;Aspiration pump after material reaction to producing Raw gas absorption and discharge reduce the bubble generated during reaction, while accelerating reaction process, can more accurately control The variable of reaction;Flowing water chamber is added in the water source of different temperatures, utilizes the high specific heat capacity principle of water so that put thermosphere and flowing water chamber Internal heat generation exchanges, and then the temperature of control reaction stablized;When reaction raw materials are relatively fewer, inflator pump is opened, air bag is filled Gas extends, and fills the bottom space of reative cell, prevents reactant flow less, causes to stir insufficient or is not easy to gas Adsorption treatment;Product after reaction falls into conveying room at feed opening through deflector, filtrate net is utilized in conveying room, to production Product carry out solid-liquid separation treatment, convenient for the collection of the product to different conditions.
Description of the drawings
Fig. 1 is the structure diagram of the utility model.
Fig. 2 is the structure diagram of flowing water chamber in the utility model.
In figure:1- autoclave bodies, 2- reative cells, 3- conveyings room, 4- motors, 5- shafts, 6- stirring rods, 7- conveyings lid, 8- flowing water Chamber, 9- put thermosphere, 10- aspiration pumps, 11- exhaust tubes, 12- suction branches, 13- suction plates, 14- suction holes, 15- waterproof membranes, 16- Inflator pump, 17- appendixs, 18- air bags, 19- feed openings, 20- deflectors, 21- filtrates net, 22- solid outlets, 23- liquid Discharge port.
Specific embodiment
The following is a combination of the drawings in the embodiments of the present utility model, and the technical scheme in the embodiment of the utility model is carried out It clearly and completely describes, it is clear that the described embodiments are only a part of the embodiments of the utility model rather than whole Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are without making creative work All other embodiments obtained shall fall within the protection scope of the present invention.
It please refers to Fig.1 and Fig. 2, in the utility model embodiment, a kind of chemical engineering experiment device convenient for control reaction process, Including autoclave body 1, the autoclave body 1 divides for reative cell 2 and conveying room 3, and the centre position of the bottom end of the reative cell 2 is equipped with Motor 4, the bottom end of the motor 4 is equipped with shaft 5, if being equidistantly equipped with arterial highway stirring rod 6 in shaft 5, the reaction The side wall of room 2, which is equipped with, puts thermosphere 9, and the outside for putting thermosphere 9 is equipped with flowing water chamber 8, and the top of the reative cell 2 is equipped with Aspiration pump 10, the right end of the aspiration pump 10 are equipped with exhaust tube 11, and the exhaust tube 11 is stretched into reative cell 2 and connected If there is arterial highway suction branch 12, suction plate 13 is equipped in the reative cell 2, if the suction plate 13 is equipped with arterial highway air-breathing Hole 14, the suction branch 12 are connected with suction hole 14, and the bottom end of the side of the reative cell 2 is equipped with inflator pump 16, appendix 17 is installed on the outlet side of the inflator pump 16, the appendix 17 stretch into the inner cavity of reative cell 2 and Air bag 18 is connected with, the air bag 18 is located at the bottom of reative cell 2, and the interposition of the baseplane of the reative cell 2 installs There is feed opening 19, the conveying room 3 is located at the lower section of reative cell 2, passes through blanking between the conveying room 3 and reative cell 2 Mouth 19 is connected, and the inner cavity of the conveying room 3 is equipped with filtrate net 21, and the conveying room 3 must be respectively arranged on the left side and the right side solid Body discharge port 22 and liquid outlet opening 23, the oblique upper of filtrate net 21 that the solid outlet 22 is located at, the liquid Discharge port 23 is the obliquely downward of filtrate net 21.
The flowing water chamber 8 be fastened reative cell 2 side wall and fit with putting thermosphere 9, the flowing water chamber 8 Upper and lower ends are respectively equipped with water inlet pipe and drainpipe.
The surface of the suction plate 13 is equipped with waterproof membrane.
The left and right sides of the feed opening 19 is equipped with deflector 20.
The inert gases such as nitrogen are used in the inflator pump 16.
The air bag 18 is high molecule plastic material.
The operation principle of the utility model is:Conveying lid is opened, material is put into reative cell, motor drives stirring rod rotation Turn, operation is stirred to material, accelerates the process of chemical reaction;Aspiration pump to the gas absorption that is generated after material reaction side by side Go out, reduce the bubble generated during reaction, while accelerating reaction process, can more accurately control the variable of reaction;It will stream Water cavity adds in the water source of different temperatures, utilizes the high specific heat capacity principle of water so that and it puts thermosphere and is exchanged with the fever of flowing water intracavitary, and then The temperature of stable control reaction;When reaction raw materials are relatively fewer, inflator pump is opened, airbag aeration is extended, filling reaction The bottom space of room prevents reactant flow less, causes to stir insufficient or is not easy to gas absorption processing;After reaction Product through deflector, fallen at feed opening in conveying room, filtrate net utilized in conveying room, product is carried out at separation of solid and liquid Reason, convenient for the collection of the product to different conditions.
It is obvious to a person skilled in the art that the utility model is not limited to the details of above-mentioned exemplary embodiment, and And in the case of the spirit or essential attributes without departing substantially from the utility model, it can realize that this practicality is new in other specific forms Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this practicality is new The range of type is indicated by the appended claims rather than the foregoing description, it is intended that by containing in the equivalent requirements of the claims is fallen All changes in justice and range are embraced therein.Any reference numeral in claim should not be considered as limitation Involved claim.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in each embodiment can also be properly combined, forms those skilled in the art The other embodiment being appreciated that.

Claims (6)

1. a kind of chemical engineering experiment device convenient for control reaction process, including autoclave body(1), which is characterized in that the autoclave body(1) It is divided into reative cell(2)With conveying room(3), the reative cell(2)The centre position of bottom end motor is installed(4), it is described Motor(4)Bottom end shaft is installed(5), shaft(5)If arterial highway stirring rod is equidistantly installed on(6), the reative cell(2) Side wall be equipped with put thermosphere(9), described puts thermosphere(9)Outside be equipped with flowing water chamber(8), the reative cell(2)Top Aspiration pump is installed(10), the aspiration pump(10)Right end exhaust tube is installed(11), the exhaust tube(11)It stretches into Reative cell(2)If interior and be connected with arterial highway suction branch(12), the reative cell(2)It is interior to be equipped with suction plate(13), it is described Suction plate(13)If equipped with arterial highway suction hole(14), the suction branch(12)With suction hole(14)It is connected, it is described Reative cell(2)The bottom end of side inflator pump is installed(16), the inflator pump(16)Outlet side on appendix is installed (17), the appendix(17)Stretch into reative cell(2)Inner cavity and be connected with air bag(18), the air bag(18)It is located at Reative cell(2)Bottom, the reative cell(2)Baseplane centre position be equipped with feed opening(19), the conveying room (3)Positioned at reative cell(2)Lower section, the conveying room(3)With reative cell(2)Between pass through feed opening(19)It is connected, institute The conveying room stated(3)Inner cavity be equipped with filtrate net(21), the conveying room(3)Solid outlet must be respectively arranged on the left side and the right side (22)And liquid outlet opening(23), the solid outlet(22)The filtrate net being located at(21)Oblique upper, the liquid Discharge port(23)For filtrate net(21)Obliquely downward.
2. the chemical engineering experiment device according to claim 1 convenient for control reaction process, which is characterized in that the flowing water Chamber(8)It is fastened in reative cell(2)Side wall and with putting thermosphere(9)It fits, the flowing water chamber(8)Upper and lower ends point It She You not water inlet pipe and drainpipe.
3. the chemical engineering experiment device according to claim 1 convenient for control reaction process, which is characterized in that the air-breathing Plate(13)Surface be equipped with waterproof membrane.
4. the chemical engineering experiment device according to claim 1 convenient for control reaction process, which is characterized in that the blanking Mouthful(19)The left and right sides be equipped with deflector(20).
5. the chemical engineering experiment device according to claim 1 convenient for control reaction process, which is characterized in that the inflation Pump(16)It is interior to use the inert gases such as nitrogen.
6. the chemical engineering experiment device according to claim 1 convenient for control reaction process, which is characterized in that the air bag (18)It is high molecule plastic material.
CN201721206863.XU 2017-09-19 2017-09-19 A kind of chemical engineering experiment device convenient for control reaction process Active CN207576376U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721206863.XU CN207576376U (en) 2017-09-19 2017-09-19 A kind of chemical engineering experiment device convenient for control reaction process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721206863.XU CN207576376U (en) 2017-09-19 2017-09-19 A kind of chemical engineering experiment device convenient for control reaction process

Publications (1)

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CN207576376U true CN207576376U (en) 2018-07-06

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110252207A (en) * 2019-05-27 2019-09-20 陈祖友 A kind of chemical reaction filter device convenient for extracting gas

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110252207A (en) * 2019-05-27 2019-09-20 陈祖友 A kind of chemical reaction filter device convenient for extracting gas
CN110252207B (en) * 2019-05-27 2021-07-27 山东沾化天元精细化工有限公司 Chemical reaction filter equipment convenient to extract gas

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