CN207552350U - The device of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar - Google Patents
The device of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar Download PDFInfo
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- CN207552350U CN207552350U CN201721610037.1U CN201721610037U CN207552350U CN 207552350 U CN207552350 U CN 207552350U CN 201721610037 U CN201721610037 U CN 201721610037U CN 207552350 U CN207552350 U CN 207552350U
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- exchange resin
- activated carbon
- juice
- case
- resin tower
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Abstract
The device of a kind of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar dissolves case, activated carbon including sequentially connected raw sugar and decolourizes in advance case, ceramic film component, plate and frame filter press, the first exchange resin tower and the second exchange resin tower.Body connection relation is as follows：The raw sugar dissolving case juice opening case that decolourizes in advance with activated carbon is connect into juice mouth, the activated carbon case juice opening that decolourizes in advance is connect with ceramic film component into juice mouth, ceramic film component trapped fluid outlet connection is back to activated carbon and decolourizes in advance case, ceramic film component juice opening is connect with plate and frame filter press into juice mouth, the outlet of plate and frame filter press juice is connect with the first exchange resin tower into juice mouth, first exchange resin tower juice opening is connect with the second exchange resin tower into juice mouth, and the second exchange resin tower juice opening is connected to evaporative crystallization workshop section.
Description
Technical field
The utility model is related to the devices of a kind of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar, belong to
In Sugar Engineering technical field.
Background technology
In refined sugar clarifying process, traditional method is to first pass through the pigment that honey washout goes in raw sugar 40%~50%,
Then raw sugar is dissolved, obtains remelt syrup, recycled carbon full charge and filtering or phosphoric acid floats and the method for filtering removes back
The 40%~60% of remaining pigment in dissolved syrup finally further uses ion exchange resin and remelt syrup progress desalination is taken off
Color can obtain the product that purity is about 99.9% after crystallization.But after carbon full charge and filtering or phosphoric acid are floated and are filtered
Remelt syrup turbidity it is still higher, it is easy to pollute the ion exchange resin of postorder workshop section, not only increase ion exchange resin
Load, also reduce service life of ion exchange resin.In order to be lowered into the turbidity of remelt syrup before ion exchange resin, have
Dissolved syrup of whirling after carbon full charge or phosphoric acid float is passed through plate and frame filter press, leaf filter and pocket type by a little sugar refineries successively
Filter three-stage filtration, but effect is still undesirable.In order to be lowered into before ion exchange resin the turbidity of remelt syrup and
Shorten refined sugar clarification process flow, Peng Wenbo et al. (number of patent application：201310729069.3) reported remelt syrup
Successively by plate and frame filter press coarse filtration, microfiltration of ceramic membrane, the decoloration of ion exchange resin desalination is then entered back into；Though this method
Remelt syrup can so be made to obtain relatively low turbidity before entering ion exchange resin, also shorten refined sugar clarification process flow,
But the process due to being washed which omits raw sugar honey and remelt syrup carbon full charge twice are important, along with ceramic micro filter film does not have
The ability of standby decoloration so that the color value of remelt syrup is higher before into ion exchange resin, not only shortens the regeneration of resin
Period and the regeneration frequency for increasing resin also add the load of resin, can also reduce the service life of resin.Therefore it provides
A kind of clarifying effect is more preferable, production efficiency higher, and the lower refined sugar defecation method of cost is necessary.
Utility model content
The purpose of this utility model is to provide a kind of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar
Device, to solve, remelt syrup clarifying effect is poor in traditional refined sugar clarification process and the ion exchange resin service life is low
Technical problem.
To achieve these goals, the utility model employs following technical scheme：
The device of a kind of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar, including sequentially connected original
Sugar dissolving case, activated carbon decolourize case, ceramic film component, plate and frame filter press, the first exchange resin tower and the second ion in advance
Exchange resin tower.
The device, specific connection relation are as follows：
The raw sugar dissolving case juice opening case that decolourizes in advance with activated carbon connect into juice mouth, and activated carbon decolourizes case juice opening and ceramic in advance
Membrane module is connected into juice mouth, and ceramic film component trapped fluid outlet connection is back to activated carbon and decolourizes in advance case, ceramic film component juice
Mouth is connect with plate and frame filter press into juice mouth, and the outlet of plate and frame filter press juice is connect with the first exchange resin tower into juice mouth, the
One exchange resin tower juice opening is connect with the second exchange resin tower into juice mouth, the second exchange resin tower juice
Mouth is connected to evaporative crystallization workshop section.
Further, raw sugar dissolving case 2 and activated carbon decolourize case with agitating device in advance.
Further, first exchange resin tower is lower charging top discharge.
Further, second exchange resin tower is upper feeding bottom discharge.
Further, the average membrane pore size of the ceramic film component is 0.005~0.05 μm.
Further, the operating parameter of the ceramic membrane is：Transmembrane pressure be 0.10~0.30MPa, crossflow velocity 4.0
~5.0m/s, filtration temperature are 80~95 DEG C.
Further, first ion exchange resin is macroporous strong basic anion exchange resin.
Further, second ion exchange resin is storng-acid cation exchange resin or Subacidity cation
Exchanger resin.
Compared with prior art, the advantageous effect that the utility model has：
1st, it using the remelt syrup after ceramic micro filter film process carbon full charge and plate and frame filter press filtering, reduces into ion
The turbidity of remelt syrup before exchanger resin, so as to reduce the load of ion exchange resin and increase ion exchange resin
Service life；And membrane resistance is smaller caused by fouling on ceramic membrane, thus ceramic membrane cross rate clarification syrup membrane flux it is larger, and film
Flux decline speed is slow, and higher membrane flux can be maintained to filter, so as to extend the Membrane cleaning period and reduce cleaning frequency membrane.
2nd, the multistage microfiltration of ceramic membrane system being made of the ceramic micro filter film of Pyatyi parallel connection is employed, every grade by two film groups
Part forms, and has level-one to play replacement wheel and washes, ensure that microfiltration of ceramic membrane system is capable of the operation of long-time stable.
3rd, remelt syrup enter ion exchange resin depth decoloration before, employ honey wash, carbon full charge twice it is more honest and clean
The process of valency decolourizes in advance to raw sugar and remelt syrup, can not only reduce the load of ion exchange resin, can also increase
Add its service life.
4th, obtained refinery liquor turbidity is less than 1.0NTU, color value is less than 10IU, conductivity is less than 10 μ s/cm, clarification effect
Fruit is preferable.
Description of the drawings
Fig. 1 is the device that a kind of activated carbon described in embodiment, ceramic membrane and ion exchange resin couple processing and refining sugar
Equipment connection diagram.
In figure：
Raw sugar dissolves case 2, hot water or sugar water entrance 1, raw sugar dissolving case juice opening 3；
Activated carbon decolourizes case 5 in advance, and activated carbon decolourizes case into juice mouth 4 in advance, and activated carbon decolourizes case juice opening 6 in advance；
Ceramic film component 10, ceramic film component are retained into juice mouth 11, ceramic film component juice opening 9, Ceramic excessive filtration membrane module
Liquid outlet 8；
Plate and frame filter press 14, plate and frame filter press is into juice mouth 15, plate and frame filter press juice opening 16；
First exchange resin tower 18, the first exchange resin tower go out into juice mouth 17, the first exchange resin tower
Juice mouth 19；
Second exchange resin tower 21, the second exchange resin tower go out into juice mouth 20, the second exchange resin tower
Juice mouth 22.
Specific embodiment
The technical solution of the utility model is further elaborated below by embodiment.
Embodiment 1
The device of a kind of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar, including sequentially connected original
Sugar dissolving case 2, activated carbon decolourize in advance case 5, ceramic film component 10, plate and frame filter press 14, the first exchange resin tower 18 and
Second exchange resin tower 21.
Specific connection relation is as follows：
The case that decolourizes in advance with activated carbon of raw sugar dissolving case juice opening 3 is connect into juice mouth 4, activated carbon decolourize in advance case juice opening 6 and
Ceramic film component is connected into juice mouth 11, and 8 connection of ceramic film component trapped fluid outlet is back to activated carbon and decolourizes in advance case 5, ceramic membrane
Component juice opening 9 is connect with plate and frame filter press into juice mouth 15, the outlet 16 of plate and frame filter press juice and the first exchange resin tower
It being connected into juice mouth 17, the first exchange resin tower juice opening 19 is connect with the second exchange resin tower into juice mouth 20, the
Two exchange resin tower juice openings 22 are connected to evaporative crystallization workshop section.
The raw sugar dissolving case 2 and activated carbon decolourize case 13 with agitating device in advance.
First exchange resin tower 18 is lower charging top discharge.
Second exchange resin tower 21 is upper feeding bottom discharge.
Embodiment to be produced using 1 described device of embodiment below
Embodiment 2
Activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar method, include the following steps：
(1) it dissolves：
Raw sugar is dissolved to 60 ° of Bx with water, obtains raw sugar remelt syrup；
(2) activated carbon decolourizes in advance：
Activated carbon is added in into raw sugar remelt syrup, fully obtain activated carbon after absorption decolourizes syrup in advance；
(3) ceramic membrane filter decarburization：
The syrup that decolourized in advance to activated carbon using ceramic film component is filtered, and obtains decarburization syrup；
(4) ion-exchange resin decolorization desalination：
It decolourizes first with the first ion exchange resin to decarburization syrup, obtains the first penetrating fluid；
The second ion exchange resin is recycled to carry out desalination to the first penetrating fluid, obtains the second penetrating fluid；
(5) it evaporates, crystallize：
Second penetrating fluid is through being concentrated by evaporation and obtaining refined sugar after cane sugar boiling and crystal.
Water described in step (1) is 75 DEG C of hot water or the sugar water of sugar refinery filter wash cloth
The addition of step (2) described activated carbon is the 0.2% of step (1) the raw sugar quality, and is reacted at 55 DEG C
10min。
Activated carbon described in step (2) decolourize in advance syrup coloration be less than 250 RBU.
The average membrane pore size of ceramic film component described in step (3) is 0.005 μm.
The operating parameter of the ceramic membrane is：Transmembrane pressure is 0.10MPa, crossflow velocity 4.0m/s, and filtration temperature is
80℃。
The first ion exchange resin described in step (4) is macroporous strong basic anion exchange resin.
The second ion exchange resin described in step (4) is handed over for storng-acid cation exchange resin or Subacidity cation
Change resin.
Embodiment 3
Activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar method, include the following steps：
(1) it dissolves：
Raw sugar is dissolved to 65 ° of Bx with water, obtains raw sugar remelt syrup；
(2) activated carbon decolourizes in advance：
Activated carbon is added in into raw sugar remelt syrup, fully obtain activated carbon after absorption decolourizes syrup in advance；
(3) ceramic membrane filter decarburization：
The syrup that decolourized in advance to activated carbon using ceramic film component is filtered, and obtains decarburization syrup；
(4) ion-exchange resin decolorization desalination：
It decolourizes first with the first ion exchange resin to decarburization syrup, obtains the first penetrating fluid；
The second ion exchange resin is recycled to carry out desalination to the first penetrating fluid, obtains the second penetrating fluid；
(5) it evaporates, crystallize：
Second penetrating fluid is through being concentrated by evaporation and obtaining refined sugar after cane sugar boiling and crystal.
Water described in step (1) is 85 DEG C of hot water or the sugar water of sugar refinery filter wash cloth
The addition of step (2) described activated carbon is the 1% of step (1) the raw sugar quality, and is reacted at 65 DEG C
40min。
Activated carbon described in step (2) decolourize in advance syrup coloration be less than 250RBU.
The average membrane pore size of ceramic film component described in step (3) is 0.05 μm.
The operating parameter of the ceramic membrane is：Transmembrane pressure is 0.30MPa, crossflow velocity 5.0m/s, and filtration temperature is
95℃。
The first ion exchange resin described in step (4) is macroporous strong basic anion exchange resin.
The second ion exchange resin described in step (4) is handed over for storng-acid cation exchange resin or Subacidity cation
Change resin.
Claims (9)
1. the device of a kind of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar, which is characterized in that including successively
Raw sugar dissolving case, the activated carbon of connection decolourize in advance case, ceramic film component, plate and frame filter press, the first exchange resin tower and
Second exchange resin tower.
2. device as described in claim 1, which is characterized in that specific connection relation is as follows：
The raw sugar dissolving case juice opening case that decolourizes in advance with activated carbon is connect into juice mouth, and activated carbon decolourizes case juice opening and ceramic membrane group in advance
Part is connected into juice mouth, and ceramic film component trapped fluid outlet connection is back to activated carbon and decolourizes in advance case, ceramic film component juice opening with
Plate and frame filter press into juice mouth connect, plate and frame filter press juice outlet connect with the first exchange resin tower into juice mouth, first from
Sub-exchange resin tower juice opening is connect with the second exchange resin tower into juice mouth, and the second exchange resin tower juice opening connects
It is connected to evaporative crystallization workshop section.
3. device as described in claim 1, which is characterized in that described raw sugar dissolving case 2 and activated carbon decolourize the equal band of case in advance
There is agitating device.
4. device as described in claim 1, which is characterized in that first exchange resin tower is goes out in lower charging
Material.
5. device as described in claim 1, which is characterized in that second exchange resin tower is to go out under upper feeding
Material.
6. device as described in claim 1, which is characterized in that the average membrane pore size of the ceramic film component for 0.005~
0.05μm。
7. device as described in claim 1, which is characterized in that the operating parameter of the ceramic membrane is：Transmembrane pressure is 0.10
~0.30MPa, crossflow velocity are 4.0~5.0m/s, and filtration temperature is 80~95 DEG C.
8. device as described in claim 1, which is characterized in that first ion exchange resin for macroporous strong basic the moon from
Sub-exchange resin.
9. device as described in claim 1, which is characterized in that second ion exchange resin is handed over for highly acidic cation
Change resin or weak-acid cation-exchange resin.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721610037.1U CN207552350U (en) | 2017-11-27 | 2017-11-27 | The device of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar |
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|---|---|---|---|
| CN201721610037.1U CN207552350U (en) | 2017-11-27 | 2017-11-27 | The device of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar |
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| CN207552350U true CN207552350U (en) | 2018-06-29 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107964569A (en) * | 2017-11-27 | 2018-04-27 | 广西大学 | The device of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar |
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- 2017-11-27 CN CN201721610037.1U patent/CN207552350U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107964569A (en) * | 2017-11-27 | 2018-04-27 | 广西大学 | The device of activated carbon, ceramic membrane and ion exchange resin coupling processing and refining sugar |
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