CN207552210U - Continuous washing kettle in one kind 3,4- dichloronitrobenzene preparation process - Google Patents
Continuous washing kettle in one kind 3,4- dichloronitrobenzene preparation process Download PDFInfo
- Publication number
- CN207552210U CN207552210U CN201721607163.1U CN201721607163U CN207552210U CN 207552210 U CN207552210 U CN 207552210U CN 201721607163 U CN201721607163 U CN 201721607163U CN 207552210 U CN207552210 U CN 207552210U
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- China
- Prior art keywords
- autoclave body
- discharge nozzle
- motors
- pipe
- filter screen
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Abstract
The utility model discloses one kind 3, continuous washing kettle in 4 dichloronitrobenzene preparation process, including autoclave body and Y355 motors, the top of autoclave body is equipped with cushion socket and Y355 motors, cushion socket is flat on the crown center position of autoclave body, and fit closely fixation with autoclave body, autoclave body is fixedly connected with Y355 motors by cushion socket, the bottom of Y355 motors is equipped with Y355 machine shafts, the inside for being arranged on Y355 motors is run through on the top of Y355 machine shafts, and it is connect with Y355 motor activities, it can be to 3, 4 dichloronitrobenzenes are stirred effect stirring, ensure continuous washing effect, in addition, it can be to 3 after cleaning by the first filter screen, water in 4 dichloronitrobenzenes drains, after water is drained, collect 3, 4 dichloronitrobenzenes.
Description
Technical field
The utility model is related to chemical technology fields, and in particular to continuous in one kind 3,4- dichloronitrobenzene preparation process
Washing kettle.
Background technology
It needs to apply to a large amount of washing kettle in chemical industry, in 3,4- dichloronitrobenzene preparation process, first by 3,4-
The reactant of dichloronitrobenzene is put into washing kettle, then is injected water into inside washing kettle, utilizes the agitating device inside washing kettle
Material is carried out to be sufficiently stirred washing, again separates impurity after standing.
It is found by retrieval, the utility model of patent No. CN204544200U discloses " washing kettle ", discloses a kind of water
Kettle is washed, including autoclave body, the middle part of the autoclave body is equipped with the transmission shaft by outer power drive, is equipped with from top to bottom on the transmission shaft upper
Blender and lower blender are distributed with through-hole on the blade of two blenders.However, the analysis found that, existing washing
Kettle has the following disadvantages；One：Material can not be sufficiently stirred, secondly：Stirring efficiency is low；Thirdly：It cannot be to stirring
Material afterwards is filtered processing.
Invention content
Therefore, in order to solve above-mentioned deficiency, the utility model is provided herein in one kind 3,4- dichloronitrobenzene preparation process
Continuous washing kettle.
The utility model is realized in this way：
Continuous washing kettle in one kind 3,4- dichloronitrobenzene preparation process, including autoclave body and Y355 motors, feature exists
In the top of autoclave body is equipped with cushion socket and Y355 motors, and cushion socket is flat on the crown center position of autoclave body, and close with autoclave body
Fitting is fixed, and autoclave body is fixedly connected with Y355 motors by cushion socket, and the bottom of Y355 motors is equipped with Y355 machine shafts, Y355
The inside for being arranged on Y355 motors is run through on the top of machine shaft, and is connect with Y355 motor activities, the bottom of Y355 machine shafts
Portion, which is equipped with, tilts agitating shaft, tilts agitating shaft and runs through and is arranged on the centre positions of Y355 machine shafts, and with Y355 machine shafts
Engaging, tilt agitating shaft is internally provided with six equally distributed through-holes；The side of autoclave body is equipped with rubber sleeve, rubber neck winding
The side wall in autoclave body is put, and is engaged with autoclave body, the bottom of rubber sleeve is equipped with two columns being symmetric, and column is perpendicular to be set
It puts in the bottom end of rubber sleeve, and fixation is fitted closely with rubber sleeve, the bottom end of column is equipped with pedestal, and pedestal is welded with column, kettle
The top of body is equipped with water inlet pipe and feed pipe, and water inlet pipe and feed pipe run through the top edge position for being arranged on autoclave body, and and kettle
Body penetrates through, and the bottom of autoclave body is equipped with discharge nozzle, and discharge nozzle runs through the bottom centre position for being arranged on autoclave body, and is penetrated through with autoclave body,
The bottom end of discharge nozzle is equipped with articulation piece, and articulation piece is welded with discharge nozzle；Autoclave body is internally provided with blow-off pipe, and blow-off pipe is through setting
It is penetrated through in the side bottom of autoclave body, and with autoclave body, the top of blow-off pipe is equipped with the second filter screen, and the second filter screen is inclined to set
The interior bottom of autoclave body, and engage with autoclave body, blow-off pipe is internally provided with valve, and valve is flexibly connected with blow-off pipe.
As an improvement of the above technical solution, the bottom of Y355 machine shafts is equipped with auxiliary agitating shaft, and auxiliary agitating shaft is embedding
Be set on the bottom end of Y355 machine shafts, and engage with Y355 machine shafts, staff in use, first pass through into
Water pipe will pour into water scouring water inside autoclave body, then 3,4- dichloronitrobenzenes are added to by feed pipe inside autoclave body, then will
Y355 electric motor startings, Y355 motors drive machine shaft rotation, and then drive and tilt agitating shaft and auxiliary agitating shaft rotation, reach
The effect being stirred to 3, the 4- dichloronitrobenzenes inside autoclave body and water.
As an improvement of the above technical solution, the top of discharge nozzle is equipped with closed piston, and closed piston insertion is arranged on out
The top of expects pipe, and be flexibly connected with discharge nozzle, after 3,4- dichloronitrobenzenes stir, staff opens valve,
Water scouring water inside autoclave body is discharged by blow-off pipe, while draining, second filter screen on blow-off pipe top can to 3,
4- dichloronitrobenzenes play barrier effect, after the discharge of water inside autoclave body, then by water inlet pipe toward pouring water inside autoclave body.
As an improvement of the above technical solution, the bottom of discharge nozzle is equipped with the first filter screen, and the first filter screen is perpendicular to be set
It puts in the bottom end of discharge nozzle, and the first filter screen is hinged with discharge nozzle by articulation piece.Finally closed piston is opened, rotation the
One filter screen makes to block discharging nozzle, drains the water in 3,4- dichloronitrobenzenes by the first filter screen, turns after water is drained
Dynamic first filter screen collects 3, the 4- dichloronitrobenzenes for cleaning and finishing from discharging nozzle.
The utility model has the following advantages that：The utility model provides one kind 3,4- dichloronitrobenzene systems herein by improving
Continuous washing kettle during standby, compared to the continuous washing kettle in a kind of existing 3,4- dichloronitrobenzenes preparation process, have
Following advantage：With can be stirred to 3,4- dichloronitrobenzenes, mixing effect is abundant；Can to the material after washing into
Row filtration treatment, is embodied as：
Advantage 1：The bottom of Y355 machine shafts is equipped with auxiliary agitating shaft, and auxiliary agitating shaft nesting is arranged on Y355 motors and turns
The bottom end of axis, and engage with Y355 machine shafts, in use, first passing through water inlet pipe will pour into staff inside autoclave body
Water scouring water, then 3,4- dichloronitrobenzenes are added to by feed pipe inside autoclave body, then by Y355 electric motor startings, Y355 electricity
Machine drives machine shaft rotation, and then drives and tilt agitating shaft and auxiliary agitating shaft rotation, reaches to autoclave body inside 3,4- dichloros
The effect that nitrobenzene and water are stirred.
Advantage 2：The top of discharge nozzle is equipped with closed piston, and closed piston is embedded in the top for being arranged on discharge nozzle, and with going out
Expects pipe is flexibly connected, and after 3,4- dichloronitrobenzenes stir, staff opens valve, the water scouring water inside autoclave body
It is discharged by blow-off pipe, second filter screen on blow-off pipe top can play barrier effect to 3,4- dichloronitrobenzenes, in draining
While, continuous wash is realized toward pouring water inside autoclave body by water inlet pipe, improves working efficiency.
Advantage 3：After the completion of cleaning, closed piston is opened, and the first filter screen of the bottom of discharge nozzle, which is vertical setting,
The bottom end of expects pipe, and the first filter screen is flexibly connected with discharge nozzle by articulation piece, finally opens closed piston, by first
Filter screen drains the water in 3,4- dichloronitrobenzenes, and after water is drained, 3, the 4- dichloro nitre finished is cleaned using container collection
Base benzene.
Description of the drawings
Fig. 1 is the continuous washing kettle structure diagram of the utility model；
Fig. 2 is the discharge nozzle partial enlarged view of the continuous washing kettle of the utility model；
Fig. 3 is the blow-off pipe partial enlarged view of the continuous washing kettle of the utility model.
In figure, 1, autoclave body；2nd, rubber sleeve；3rd, column；4th, pedestal；5th, closed piston；6th, water inlet pipe；7th, cushion socket；8、
Y355 motors；9th, feed pipe；10th, agitating shaft is tilted；11st, through-hole；12nd, agitating shaft is assisted；13rd, articulation piece；14th, the first filtering
Net；15th, discharge nozzle；16th, the second filter screen；17th, valve；18th, blow-off pipe；19th, Y355 motors；20th, shaft.
Specific embodiment
The utility model is described in detail below in conjunction with attached drawing 1- Fig. 3, to the skill in the utility model embodiment
Art scheme is clearly and completely described, it is clear that and the described embodiments are only a part of the embodiments of the utility model, and
The embodiment being not all of.Based on the embodiment in the utility model, those of ordinary skill in the art are not making creativeness
All other embodiments obtained under the premise of labour, shall fall within the protection scope of the present invention.
The utility model is by improving the continuous washing kettle provided herein in one kind 3,4- dichloronitrobenzene preparation process, such as
Shown in Fig. 1-Fig. 3, it can be practiced as follows；Including autoclave body 1 and Y355 motors 8, the top of autoclave body 1 is equipped with damping
Seat 7 and Y355 motors 8, cushion socket 7 are flat on the crown center position of autoclave body 1, and fit closely fixation with autoclave body 1, autoclave body 1 with
Y355 motors 8 are fixedly connected by cushion socket 7, and the bottom of Y355 motors 8 is equipped with Y355 machine shafts 19, Y355 machine shafts 19
Top run through and be arranged on the inside of Y355 motors 8, and be flexibly connected with Y355 motors 8, the bottom of Y355 machine shafts 19 is set
Have and tilt agitating shaft 10, tilt agitating shaft 10 and run through the centre position for being arranged on Y355 machine shafts 19, and turn with Y355 motors
Axis 19 engages, and tilt agitating shaft 10 is internally provided with six equally distributed through-holes 11.
The side of autoclave body 1 is equipped with rubber sleeve 2, and rubber sleeve 2 is circumferentially positioned at the side wall of autoclave body 1, and engages with autoclave body 1, rubber
The bottom of gum cover 2 is equipped with two columns 3 being symmetric, and column 3 is vertical setting in the bottom end of rubber sleeve 2, and and rubber
Set 2 fits closely fixation, and the bottom end of column 3 is equipped with pedestal 4, and pedestal 4 is welded with column 3, and the top of autoclave body 1 is equipped with water inlet pipe 6
With feed pipe 9, water inlet pipe 6 and feed pipe 9 run through the top edge position for being arranged on autoclave body 1, and penetrate through with autoclave body 1, autoclave body 1
Bottom is equipped with discharge nozzle 15, and discharge nozzle 15 runs through the bottom centre position for being arranged on autoclave body 1, and is penetrated through with autoclave body 1, discharge nozzle 15
Bottom end be equipped with articulation piece 13, articulation piece 13 welds with discharge nozzle 15.
Autoclave body 1 is internally provided with blow-off pipe 18, and blow-off pipe 18 runs through the side bottom for being arranged on autoclave body 1, and is passed through with autoclave body 1
Logical, the top of blow-off pipe 18 is equipped with the second filter screen 16, and the second filter screen 16 is inclined to set in the interior bottom of autoclave body 1, and with
Autoclave body 1 engages, and blow-off pipe 18 is internally provided with valve 17, and valve 17 is flexibly connected with blow-off pipe 18.
The bottom of Y355 machine shafts 19 is equipped with auxiliary agitating shaft 12, and auxiliary 12 nesting of agitating shaft is arranged on Y355 motors and turns
The bottom end of axis 19, and engage with Y355 machine shafts 19, staff in use, first passes through water inlet pipe 6 in autoclave body 1
Portion pours into water scouring water, then 3,4- dichloronitrobenzenes are added to by feed pipe 9 inside autoclave body 1, then opens Y355 motors 8
Dynamic, Y355 motors 8 drive machine shaft 19 to rotate, and then drive and tilt agitating shaft 10 and auxiliary agitating shaft 12 rotates, and reach pair
The effect that 1 inside 3,4- dichloronitrobenzenes of autoclave body and water are stirred.
The top of discharge nozzle 15 is equipped with closed piston 5, and closed piston 5 is embedded in the top for being arranged on discharge nozzle 15, and with going out
Expects pipe 15 is flexibly connected, and after 3,4- dichloronitrobenzenes stir, staff opens valve 17, the water inside autoclave body 1
Scouring water is discharged by blow-off pipe 18, and while draining, second filter screen 16 on 18 top of blow-off pipe can be to 3,4- dichloros
Nitrobenzene plays barrier effect, after the discharge of water inside autoclave body 1, then by water inlet pipe 6 toward pouring water inside autoclave body 1.
The bottom of discharge nozzle 15 is equipped with the first filter screen 14, and the first filter screen 14 is vertical setting at the bottom of discharge nozzle 15
End, and the first filter screen 14 is hinged by articulation piece 13 with discharge nozzle 15, finally opens closed piston 5, the first filtering of rotation
Net 14 makes to block 15 mouthfuls of discharge nozzle, drains the water in 3,4- dichloronitrobenzenes by the first filter screen 14, turns after water is drained
Dynamic first filter screen 14, from 15 mouthfuls of 3,4- dichloronitrobenzenes collected cleaning and finished of discharge nozzle.
To sum up；The utility model one kind 3, the continuous washing kettle in 4- dichloronitrobenzene preparation process, and existing a kind of 3,
Continuous washing kettle in 4- dichloronitrobenzene preparation process is compared to have and can be stirred effect to 3,4- dichloronitrobenzenes and stir
It mixes, ensures continuous washing effect, in addition, can be dripped by the first filter screen 14 to the water in 3, the 4- dichloronitrobenzenes after cleaning
It is dry, after water is drained, 3, the 4- dichloronitrobenzenes finished are cleaned using container collection.
The foregoing description of the disclosed embodiments enables professional and technical personnel in the field to realize or new using this practicality
Type.A variety of modifications of these embodiments will be apparent for those skilled in the art, determine herein
The General Principle of justice can be realized in other embodiments without departing from the spirit or scope of the present utility model.Cause
This, the utility model is not intended to be limited to the embodiments shown herein, and is to fit to and principles disclosed herein
The most wide range consistent with features of novelty.
Claims (4)
1. one kind 3, the continuous washing kettle in 4- dichloronitrobenzene preparation process, including autoclave body（1）With Y355 motors（8）, it is special
Sign is：The autoclave body（1）Top be equipped with cushion socket（7）With Y355 motors（8）, the cushion socket（7）It is flat on autoclave body（1）
Crown center position, and and autoclave body（1）Fit closely fixation, the autoclave body（1）With Y355 motors（8）Pass through cushion socket（7）
It is fixedly connected, the Y355 motors（8）Bottom be equipped with Y355 machine shafts（19）, the Y355 machine shafts（19）Top
Through being arranged on Y355 motors（8）Inside, and with Y355 motors（8）Flexible connection, the Y355 machine shafts（19）Bottom
Portion, which is equipped with, tilts agitating shaft（10）, the inclination agitating shaft（10）Through being arranged on Y355 machine shafts（19）Centre position,
And with Y355 machine shafts（19）Engaging, the inclination agitating shaft（10）Be internally provided with six equally distributed through-holes（11）；
The autoclave body（1）Side be equipped with rubber sleeve（2）, the rubber sleeve（2）It is circumferentially positioned at autoclave body（1）Side wall, and with
Autoclave body（1）Engaging, the rubber sleeve（2）Bottom be equipped with two columns being symmetric（3）, the column（3）It is perpendicular
It is arranged on rubber sleeve（2）Bottom end, and and rubber sleeve（2）Fit closely fixation, the column（3）Bottom end be equipped with pedestal（4）,
The pedestal（4）With column（3）Welding, the autoclave body（1）Top be equipped with water inlet pipe（6）And feed pipe（9）, the water inlet pipe
（6）And feed pipe（9）Through being arranged on autoclave body（1）Top edge position, and and autoclave body（1）Perforation, the autoclave body（1）Bottom
Portion is equipped with discharge nozzle（15）, the discharge nozzle（15）Through being arranged on autoclave body（1）Bottom centre position, and and autoclave body（1）It passes through
It is logical, the discharge nozzle（15）Bottom end be equipped with articulation piece（13）, the articulation piece（13）With discharge nozzle（15）Welding；
The autoclave body（1）Be internally provided with blow-off pipe（18）, the blow-off pipe（18）Through being arranged on autoclave body（1）Side bottom,
And and autoclave body（1）Perforation, the blow-off pipe（18）Top be equipped with the second filter screen（16）, second filter screen（16）In inclining
Tiltedly it is arranged on autoclave body（1）Interior bottom, and and autoclave body（1）Engaging, the blow-off pipe（18）Be internally provided with valve（17）, it is described
Valve（17）With blow-off pipe（18）Flexible connection.
2. the continuous washing kettle in one kind 3,4- dichloronitrobenzene preparation process according to claim 1, it is characterised in that：Institute
State Y355 machine shafts（19）Bottom be equipped with auxiliary agitating shaft（12）, the auxiliary agitating shaft（12）Nesting is arranged on Y355 electricity
Machine shaft（19）Bottom end, and with Y355 machine shafts（19）Engaging.
3. the continuous washing kettle in one kind 3,4- dichloronitrobenzene preparation process according to claim 1, it is characterised in that：Institute
State discharge nozzle（15）Top be equipped with closed piston（5）, the closed piston（5）Insertion is arranged on discharge nozzle（15）Top,
And and discharge nozzle（15）Flexible connection.
4. the continuous washing kettle in one kind 3,4- dichloronitrobenzene preparation process according to claim 1, it is characterised in that：Institute
State discharge nozzle（15）Bottom be equipped with the first filter screen（14）, first filter screen（14）It is vertical setting in discharge nozzle（15）
Bottom end, and first filter screen（14）With discharge nozzle（15）Pass through articulation piece（13）It is hinged.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721607163.1U CN207552210U (en) | 2017-11-27 | 2017-11-27 | Continuous washing kettle in one kind 3,4- dichloronitrobenzene preparation process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721607163.1U CN207552210U (en) | 2017-11-27 | 2017-11-27 | Continuous washing kettle in one kind 3,4- dichloronitrobenzene preparation process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207552210U true CN207552210U (en) | 2018-06-29 |
Family
ID=62677542
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721607163.1U Expired - Fee Related CN207552210U (en) | 2017-11-27 | 2017-11-27 | Continuous washing kettle in one kind 3,4- dichloronitrobenzene preparation process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207552210U (en) |
-
2017
- 2017-11-27 CN CN201721607163.1U patent/CN207552210U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180629 Termination date: 20181127 |