CN207546497U - A kind of water soluble phenol resin reaction kettle - Google Patents
A kind of water soluble phenol resin reaction kettle Download PDFInfo
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- CN207546497U CN207546497U CN201721424993.0U CN201721424993U CN207546497U CN 207546497 U CN207546497 U CN 207546497U CN 201721424993 U CN201721424993 U CN 201721424993U CN 207546497 U CN207546497 U CN 207546497U
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- reaction kettle
- kettle body
- water soluble
- reactant
- phenol resin
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Abstract
The utility model discloses a kind of water soluble phenol resin reaction kettles, including reaction kettle body and controller, the horizontal baffle for being divided into epimere preheating autoclave body and hypomere reaction kettle body is provided in the reaction kettle body, the vertical clapboard for being divided into not connected left reaction kettle body and right reaction kettle body is provided in the hypomere reaction kettle body, the first reactant exit is provided at the center of the horizontal baffle.The water soluble phenol resin reaction kettle of the utility model realizes the continuous production of reaction, improves production efficiency, has saved production cost, has increased economic benefit.
Description
Technical field
The utility model belongs to technical field of chemical, and in particular to a kind of water soluble phenol resin reaction kettle.
Background technology
Crosslinking agent of the water soluble phenol resin as polymer, maximum feature are exactly a large amount of organic molten with water replacement
Agent can reduce or eliminate the pollution and waste of solvent, be conducive to environmental protection, and can reduce production cost, obtain wide
General application is mainly used in the industries such as anticorrosion engineering, adhesive, fire proofing manufacture.It is but existing for water-soluble phenolic
The reaction kettle of urea formaldehyde production, in reaction for intermittent reaction, influence the efficiency of production.
Utility model content
The purpose of this utility model is that：The above-mentioned problem of face provides a kind of water soluble phenol resin reaction
Kettle realizes the continuous production of reaction, improves production efficiency, saved production cost, increases economic benefit.
To achieve these goals, the technical solution adopted in the utility model is：The utility model discloses a kind of water-soluble
Property reactive modified phenolic resin kettle, including reaction kettle body and controller, is provided in the reaction kettle body and is divided into epimere still preheater
The horizontal baffle of body and hypomere reaction kettle body is provided in the hypomere reaction kettle body and is divided into not connected left reaction kettle
The vertical clapboard of body and right reaction kettle body is provided with the first reactant exit at the center of the horizontal baffle, and described first is anti-
It answers and three-way magnetic valve is provided in object outlet, in the left reaction kettle body and be both provided with reactant spray in right reaction kettle body and shine and justify
Disk, the upper surface that disk is shone in the reactant spray are provided with the first reaction-ure inlet connected with three-way magnetic valve, the reaction
The lower surface that disk is shone in object spray is provided with the reactant spray solarization hole connected with the first reaction-ure inlet；The epimere preheating autoclave body
The first electric heating body is provided in housing, cold wind import is provided on the epimere preheating autoclave body, the epimere preheating autoclave body
Top is provided with the first driving motor, first charging aperture and cold wind outlet, is additionally provided with and first in the epimere still preheater body
First stirring slurry of the output axis connection of driving motor；Fixation is both provided at the top of the left reaction kettle body and right reaction kettle body
Frame, the fixed frame are connected on the lower surface of horizontal baffle, and the second driving motor, the left side are respectively and fixedly provided on the fixed frame
The second agitating paddle with the output axis connection of the second driving motor, the left side are both provided in reaction kettle body and in right reaction kettle body
The second electric heating body is respectively provided in the housing of reaction kettle body and in the housing of right reaction kettle body, the is provided in the vertical clapboard
Three electric heating bodies, the bottom of the left reaction kettle body are provided with the second reactant exit, the bottom setting of the right reaction kettle body
There are third reactant exit, first electric heating body, the second electric heating body, three-way magnetic valve, the first driving motor and second
Driving motor is connect with controller signals.
Preferably, it is both provided with pressure sensor in the epimere preheating autoclave body, left reaction kettle body and right reaction kettle body
With temperature sensor, the pressure sensor and temperature sensor are connect with controller signals.
Preferably, the upper surface of the horizontal baffle is infundibulate.
Preferably, on the housing of the left reaction kettle body and it is both provided with the second charging on the housing of right reaction kettle body
Mouthful, it is both provided with mass flowmenter and solenoid valve in the second charging aperture, the mass flowmenter and electricity valve are and controller
Signal connects.
Preferably, first agitating paddle and the second agitating paddle are both provided with helical blade, are set on the helical blade
It is equipped with multiple through-holes.
Preferably, housing thermal-insulation coat is provided on the outer wall of the reaction kettle body, on the inner wall of the reaction kettle body
It is provided with the anti-sticking internal layer of layer of polyethylene.
By adopting the above-described technical solution, the beneficial effects of the utility model are：
Reaction kettle body is divided into epimere preheating autoclave body, left reaction kettle by the water soluble phenol resin reaction kettle of the utility model
Body and right reaction kettle body facilitate reactant linear temperature increase in epimere still preheater body to react, while preheating is reacted to certain time
Afterwards, it is entered in left reaction kettle body by triple valve, is then passed through cold wind from cold wind import, the temperature of epimere preheating autoclave body is dropped
It to default minimum temperature, then is passed through another batch reaction object and enters into epimere still preheater body, entered back into after reacting a period of time to the right side
In reaction kettle body, then into the same process of shape, after reactant reaction in just left reaction kettle body is complete, epimere is preheated into autoclave body
Interior reactant is being entered by three-way magnetic valve in left reaction kettle body, realizes that the production in entire reaction kettle is carried out continuously,
Improve production efficiency.
Description of the drawings
Fig. 1 is the structure diagram of the reaction kettle body of the water soluble phenol resin reaction kettle of the utility model；
Fig. 2 is the control block diagram of the water soluble phenol resin reaction kettle of the utility model；
Fig. 3 is the structure diagram of the horizontal baffle of the water soluble phenol resin reaction kettle of the utility model；
Fig. 4 is that the structure diagram of disk is shone in the reactant spray of the water soluble phenol resin reaction kettle of the utility model；
Reference numeral：1- epimeres preheating autoclave body, the first driving motors of 11-, 12- first charging apertures, the first agitating paddles of 13-,
The first electric heating bodies of 14-, 15- cold wind imports, 2- hypomere reaction kettle bodies, the left reaction kettle bodies of 21-, the right reaction kettle bodies of 22-, 23-
Two electric heating bodies, 24- second charging apertures, 25- fixed frames, the second driving motors of 26-, the second agitating paddles of 27-, the spray of 28- reactants
Disk is shone, hole, 3- horizontal baffles, the first reactant exits of 31-, 4- vertical clapboards, 41- third electrical heating are shone in the spray of 29- reactants
Body, 5- three-way magnetic valves, 6- controllers, 7- pressure sensors, 8- temperature sensors, 9- mass flowmenters, 10- solenoid valves.
Specific embodiment
The following describes the utility model in further detail with reference to the accompanying drawings, to enable those skilled in the art with reference to explanation
Book word can be implemented according to this.
As Figure 1-Figure 4, the utility model provides a kind of water soluble phenol resin reaction kettle, including reaction kettle body and
Controller 6 is provided with the horizontal baffle 3 for being divided into epimere preheating autoclave body 1 and hypomere reaction kettle body 2 in the reaction kettle body,
Be provided in the hypomere reaction kettle body 2 be divided into not connected left reaction kettle body 21 and right reaction kettle body 22 it is vertical every
Plate 4 is provided with the first reactant exit 31 at the center of the horizontal baffle 3, is provided in first reactant exit 31
Three-way magnetic valve 5 is both provided with reactant spray and shines disk 28 in the left reaction kettle body 21 and in right reaction kettle body 22, described anti-
The upper surface that disk 28 is shone in object spray is answered to be provided with the first reaction-ure inlet connected with three-way magnetic valve 5, the reactant spray is shone
The lower surface of disk 28 is provided with the reactant spray connected with the first reaction-ure inlet and shines hole 29；The epimere preheating autoclave body 1
The first electric heating body 14 is provided in housing, cold wind import 15, the epimere still preheater are provided on the epimere preheating autoclave body 1
The top of body 1 is provided with the first driving motor 11, first charging aperture 12 and cold wind outlet, is also set in the epimere preheating autoclave body 1
It is equipped with the first stirring slurry with the output axis connection of the first driving motor 11；The left reaction kettle body 21 and right reaction kettle body 22
Top is both provided with fixed frame 25, and the fixed frame 25 is connected on the lower surface of horizontal baffle 3, solid on the fixed frame 25
Surely there is the second driving motor 26, be both provided with and the second driving motor 26 in the interior and right reaction kettle body 22 of the left reaction kettle body 21
Output axis connection the second agitating paddle 27, be all provided in the housing of the left reaction kettle body 21 and in the housing of right reaction kettle body 22
The second electric heating body 23 is put, third electric heating body 41 is provided in the vertical clapboard 4, the bottom of the left reaction kettle body 21 is set
The second reactant exit is equipped with, the bottom of the right reaction kettle body 22 is provided with third reactant exit, first electrical heating
Body 14, the second electric heating body 23, three-way magnetic valve 5, the first driving motor 11 and the second driving motor 26 with 6 signal of controller
Connection.
The course of work of the water soluble phenol resin reaction kettle of the utility model is as follows, pre- from the first material inlet to epimere
Formaldehyde and phenol are passed through in hot autoclave body 1, is reacted, and the second electric heating body 23 is controlled linearly to be risen by controller 6
Temperature, by the pressure in pressure sensor 7 in real time monitoring autoclave body, while the first driving motor 11 drives the first agitating paddle 13, makes
The temperature uniformity in epimere preheating autoclave body 1 is obtained, when being raised to scheduled temperature, controller 6 opens three-way magnetic valve 5 so that
Reactant in epimere preheating autoclave body 1 is entered in left reaction kettle body 21, and controller 6 controls the second driving motor 26 to rotate, and stirs
The reactant in left reaction kettle body 21 is mixed, meanwhile, cold wind is passed through into epimere still preheater body 1 from cold wind import 15, is reduced in it
Temperature, temperature sensor 8 by the epimere detected preheat autoclave body 1 in temperature be transmitted to controller 6, when temperature be reduced to it is default
During value, cold wind import 15 is closed, and be passed through formaldehyde and phenol into epimere still preheater body 1 again by controller 6, is added
Heat can be detected by adding in other reaction raw materials in second charging aperture 24 to the left reaction kettle body 21 by mass flowmenter 9
The amounts of other reaction raw materials be transmitted to controller 6, controller 6 controls solenoid valve 10 so that reactant heating amount is suitable；Epimere is pre-
Raw material in hot autoclave body 1 enters reactant spray from three-way magnetic valve 5 and shines in disk 28, finally enter by same process
Into right reaction kettle body 22；Left reaction kettle body 21 and right reaction are alternately entered by the reactant in epimere preheating autoclave body 1
Subsequent reactions are carried out in autoclave body 22, realize the continuous production of whole device, improve the efficiency of production.
In another example, the upper surface of the horizontal baffle 3 is infundibulate.The namely upper surface of horizontal baffle 3
Center is low and surrounding is high, prevents bottom siltation of the reactant in epimere preheating autoclave body 1.
In another example, 13 and second agitating paddle 27 of the first agitating paddle is both provided with helical blade, the spiral shell
Vane on piece is provided with multiple through-holes.First agitating paddle 13 and the second agitating paddle 27 can drive reactant along helical blade to
Upper movement, and through-hole is set on helical blade, increase reactant molecule impact severity during stirring so that stirring
More uniformly.
In another example, housing thermal-insulation coat is provided on the outer wall of the reaction kettle body, the reaction kettle body
The anti-sticking internal layer of layer of polyethylene is provided on inner wall.Housing thermal-insulation coat plays the role of heat preservation and protection housing, and polyethylene is prevented
Viscous internal layer effectively prevents wall sticking phenomenon.
Although the embodiment of the utility model is disclosed as above, it is not restricted in specification and embodiment
Listed utilization, it can be applied to various fields suitable for the present invention completely, for those skilled in the art,
Other modification is easily implemented, therefore without departing from the general concept defined in the claims and the equivalent scope, this reality
Specific details and legend shown and described herein are not limited to novel.
Claims (6)
1. a kind of water soluble phenol resin reaction kettle, which is characterized in that including reaction kettle body and controller (6), the reaction kettle
It is provided with the horizontal baffle (3) for being divided into epimere preheating autoclave body (1) and hypomere reaction kettle body (2), the hypomere reaction in vivo
The vertical clapboard (4) for being divided into not connected left reaction kettle body (21) and right reaction kettle body (22) is provided in autoclave body (2),
The first reactant exit (31) is provided at the center of the horizontal baffle (3), is set in first reactant exit (31)
There is three-way magnetic valve (5), the left reaction kettle body (21) is interior and right reaction kettle body (22) is interior is both provided with reactant spray solarization disk
(28), the upper surface that disk (28) is shone in the reactant spray is provided with the first reaction-ure inlet connected with three-way magnetic valve (5),
The lower surface that disk (28) is shone in the reactant spray is provided with the reactant spray connected with the first reaction-ure inlet and shines hole (29)；Institute
It states and the first electric heating body (14) is provided in the housing of epimere preheating autoclave body (1), be provided on the epimere preheating autoclave body (1) cold
Wind inlet (15) is provided with the first driving motor (11), first charging aperture (12) and cold at the top of epimere preheating autoclave body (1)
Wind exports, and the first stirring with the output axis connection of the first driving motor (11) is additionally provided in the epimere preheating autoclave body (1)
Slurry；Fixed frame (25), the fixed frame (25) are both provided at the top of the left reaction kettle body (21) and right reaction kettle body (22)
It is connected on the lower surface of horizontal baffle (3), the second driving motor (26) is respectively and fixedly provided on the fixed frame (25), it is described left anti-
It answers in autoclave body (21) and is both provided in right reaction kettle body (22) and stirred with the second of the output axis connection of the second driving motor (26)
Paddle (27) is mixed, the second electric heating body is respectively provided in the interior housing with right reaction kettle body (22) of housing of the left reaction kettle body (21)
(23), it is provided with third electric heating body (41) in the vertical clapboard (4), the bottom of the left reaction kettle body (21) is provided with the
Two reactant exits, the bottom of the right reaction kettle body (22) are provided with third reactant exit, first electric heating body
(14), the second electric heating body (23), three-way magnetic valve (5), the first driving motor (11) and the second driving motor (26) with control
Device (6) signal connection processed.
2. water soluble phenol resin reaction kettle as described in claim 1, which is characterized in that the epimere preheating autoclave body (1), a left side
Pressure sensor (7) and temperature sensor (8) are both provided in reaction kettle body (21) and right reaction kettle body (22), the pressure passes
Sensor (7) and temperature sensor (8) are connect with controller (6) signal.
3. water soluble phenol resin reaction kettle as described in claim 1, which is characterized in that the upper table of the horizontal baffle (3)
Face is infundibulate.
4. water soluble phenol resin reaction kettle as described in claim 1, which is characterized in that the shell of the left reaction kettle body (21)
Second charging aperture (24) is both provided on body and on the housing of right reaction kettle body (22), is respectively provided in the second charging aperture (24)
There are mass flowmenter (9) and solenoid valve (10), the mass flowmenter (9) and electric valve are connect with controller (6) signal.
5. water soluble phenol resin reaction kettle as described in claim 1, which is characterized in that first agitating paddle (13) and
Two agitating paddles (27) are both provided with helical blade, and multiple through-holes are provided on the helical blade.
6. water soluble phenol resin reaction kettle as described in claim 1, which is characterized in that set on the outer wall of the reaction kettle body
Housing thermal-insulation coat is equipped with, the anti-sticking internal layer of layer of polyethylene is provided on the inner wall of the reaction kettle body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721424993.0U CN207546497U (en) | 2017-10-31 | 2017-10-31 | A kind of water soluble phenol resin reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721424993.0U CN207546497U (en) | 2017-10-31 | 2017-10-31 | A kind of water soluble phenol resin reaction kettle |
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| Publication Number | Publication Date |
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| CN207546497U true CN207546497U (en) | 2018-06-29 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721424993.0U Active CN207546497U (en) | 2017-10-31 | 2017-10-31 | A kind of water soluble phenol resin reaction kettle |
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| CN (1) | CN207546497U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109395673A (en) * | 2018-12-01 | 2019-03-01 | 昌邑市龙港无机硅有限公司 | A kind of continous way Liquid-phase reactor and the process using reactor production liquid sodium silicate |
| CN113694873A (en) * | 2021-09-14 | 2021-11-26 | 朱枫 | Production and processing equipment and process of polyurethane waterproof coating |
| CN114452925A (en) * | 2022-01-25 | 2022-05-10 | 宋秋晨 | High-efficient preparation facilities of phenolic resin |
-
2017
- 2017-10-31 CN CN201721424993.0U patent/CN207546497U/en active Active
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109395673A (en) * | 2018-12-01 | 2019-03-01 | 昌邑市龙港无机硅有限公司 | A kind of continous way Liquid-phase reactor and the process using reactor production liquid sodium silicate |
| CN109395673B (en) * | 2018-12-01 | 2021-08-10 | 山东龙港硅业科技有限公司 | Continuous liquid phase reactor and process method for producing liquid sodium silicate by using same |
| CN113694873A (en) * | 2021-09-14 | 2021-11-26 | 朱枫 | Production and processing equipment and process of polyurethane waterproof coating |
| CN114452925A (en) * | 2022-01-25 | 2022-05-10 | 宋秋晨 | High-efficient preparation facilities of phenolic resin |
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Legal Events
| Date | Code | Title | Description |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: 638600 Huaying Industrial Development Zone, Guang'an City, Sichuan Province Patentee after: Sichuan pavoke mineral fiber products Group Co.,Ltd. Address before: 638612 Huaying Industrial Development Zone, Guang'an City, Sichuan Province Patentee before: SICHUAN PAWOKE MINERAL FIBER PRODUCTS CO.,LTD. |
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| CP03 | Change of name, title or address |