CN207516324U - A kind of kjeldahl apparatus distilling apparatus with pressure alarm - Google Patents

A kind of kjeldahl apparatus distilling apparatus with pressure alarm Download PDF

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Publication number
CN207516324U
CN207516324U CN201721564910.8U CN201721564910U CN207516324U CN 207516324 U CN207516324 U CN 207516324U CN 201721564910 U CN201721564910 U CN 201721564910U CN 207516324 U CN207516324 U CN 207516324U
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China
Prior art keywords
pressure
pipe
steam oven
disappear
boils
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CN201721564910.8U
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Chinese (zh)
Inventor
严雪伟
花建丽
黄飞
张闪烁
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Henan Grg Metrology & Test Co ltd
Radio and TV Measurement and Testing Group Co.,Ltd.
Original Assignee
Guangzhou GRG Metrology and Test Co Ltd
Guangzhou GRG Metrology and Test Technology Co Ltd
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Priority to CN201721564910.8U priority Critical patent/CN207516324U/en
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Abstract

The utility model is related to the technical field of detection, more particularly, to a kind of kjeldahl apparatus distilling apparatus with pressure alarm.A kind of kjeldahl apparatus distilling apparatus with pressure alarm, pipe, vapor conduit, steam oven are boiled including disappearing, the vapor tube at one end connection, which disappears, boils inside pipe, inside other end connection steam oven, it further includes to be fixed on to disappear and boils the sealing device of tube opening, fixed on sealing device to distillate fluid catheter, the connection of distillate tube at one end, which disappears, boils pipe, and the other end is connected to disappear and boil outside pipe;Pressure detecting and control mechanism, computer control system are further included, the pressure detecting and control mechanism, which are set on to disappear, boils pipe top, and computer control system is electrically connected respectively with pressure detecting and control mechanism, steam oven.The utility model determines that sample ensures the safety of experimentation when hypertonia sends out security alarm sound automatically and instrument is carried out forced brake in dynamic pressure monitoring process by the variation of pressure.

Description

A kind of kjeldahl apparatus distilling apparatus with pressure alarm
Technical field
The utility model is related to the technical fields of detection, have the function of the kelvin of pressure alarm more particularly, to a kind of Azotometer distilling apparatus.
Background technology
Kjeldahl apparatus is detected with kelvin method in cereal, food, feed, water, soil, mud, sediment and chemicals Ammonia, protein nitrogen content, phenol, volatile fatty acid, cyanide, sulfur dioxide, ethyl alcohol equal size;Kjeldahl's method be by containing Nitrogen organic is changed into inorganic nitrogen ammonium sulfate to be detected, and being multiplied by certain coefficient with the measured value for obtaining nitrogen content obtains albumen Matter content.General applicability, accuracy and the repeatability of Kjeldahl's method have been obtained for international be widely recognized as.It is It is confirmed as detecting the standard method of protein content in foodstuff.Therefore kjeldahl apparatus is widely used.
However, in instrumentation operational process, the high-temperature high-pressure steam continually generated enters distillation cascade, and steams Pipe is evaporated for glass material, and the reaction condition of high temperature and pressure, which certainly will exist to disappear, boils the fortuitous event generation of pipe glass fragmentation faced, triumphant at present The security setting of family name's azotometer is mainly that glass disappears to boil and is provided with plastics sliding outside pipe, and nonetheless, glass, which disappears, boils the broken of pipe It splits splashing scene to be also enough test engineer is allowed to generate psychological shade, how to prevent trouble before it happens just has before glass disappears and boils pipe fragmentation Safety alarm device simultaneously carries out forced brake as a problem to be solved.
Utility model content
The utility model is at least one defect overcome described in the above-mentioned prior art, is provided a kind of with pressure alarm work( The kjeldahl apparatus distilling apparatus of energy, disappear the occurrence of boiling pipe fragmentation to avoid high-pressure glass, ensures the safety of experimenter Experimental enviroment.
The technical solution of the utility model is:A kind of kjeldahl apparatus distilling apparatus with pressure alarm, including Disappear and boil pipe, vapor conduit, steam oven, vapor tube at one end connection, which disappears, boils inside pipe, other end connection steam oven Inside further includes to be fixed on to disappear and boils the sealing device of tube opening, fixed on sealing device to distillate fluid catheter, distillate tube at one end Connection, which disappears, boils pipe, and the other end is connected to disappear and boil outside pipe;
Wherein, pressure detecting and control mechanism, computer control system, the pressure detecting and control mechanism are further included Pipe top is boiled set on disappearing, computer control system is electrically connected respectively with pressure detecting and control mechanism, steam oven.
In the utility model, when disappearing, to boil overpressure excessively high, and pressure detecting and control mechanism receive signal and send to Computer control system is simultaneously alarmed, and the detection of simultaneous computer control system control pressure and control mechanism pressure release and steam oven stop Heating is prevented from disappearing and boils pipe and crush to reduce pressure.
Further, the pressure detecting and control mechanism include probe, pressure control device, pressure sensor, institute The probe one end stated is inserted into disappear and be boiled in pipe, and other end connection pressure sensor, pressure sensor is connected by signal transmssion line and counted Calculation machine control system;
Pressure control device one end connection sealing device, the other end connect computer by signal transmssion line and control System.
The size of probe and pressure sensor can detect pressure, it is direct that pressure control device can experience instantaneous pressure overload Pressure release is opened, is controlled under normal pressure by computer control system.
Further, the pressure sensor is ceramic pressure sensor.With high resiliency, anticorrosive, wear-resistant, anti- The characteristic of shock and vibration.Pressure sensor is arranged on to disappear and boil outside pipe, reduces acid and alkali corrosion.
Further, vapor conduit connection steam oven conducting wire, steam oven conducting wire are connected to inside steam oven.Institute The steam oven stated is connect by signal transmssion line with computer control system.In the utility model, pass through the side of signal transmssion line Formula is safe and reliable.
Compared with prior art, advantageous effect is:The utility model is for safety existing for current kjeldahl apparatus instrument Hidden danger is improved, i.e., pressure sensor is added in distillation process, distillation process pressure is monitored into Mobile state, when pressure mistake Height sends out security alarm sound and instrument is carried out forced brake automatically, passes through the variation of pressure in dynamic pressure monitoring process Determine that sample ensures the safety of experimentation.
Description of the drawings
Fig. 1 is the utility model overall structure diagram.
Specific embodiment
The attached figures are only used for illustrative purposes and cannot be understood as limitating the patent;It is attached in order to more preferably illustrate the present embodiment Scheme certain components to have omission, zoom in or out, do not represent the size of actual product;To those skilled in the art, The omitting of some known structures and their instructions in the attached drawings are understandable.Being given for example only property of position relationship described in attached drawing Explanation, it is impossible to be interpreted as the limitation to this patent.
As shown in Figure 1, a kind of kjeldahl apparatus distilling apparatus with pressure alarm, pipe 7, vapor are boiled including disappearing Conduit 5, steam oven 9, the connection of 5 one end of vapor conduit, which disappears, boils inside pipe 7, inside other end connection steam oven 9, further includes fixation In the sealing device 6 that boils the opening of pipe 7 of disappearing, on sealing device 6 fixation distillate fluid catheter 2, distillate the connection of 2 one end of fluid catheter and disappear and boil pipe 7, the other end is connected to disappear and boil outside pipe 7;
Wherein, it further includes pressure detecting and control mechanism, computer control system 1, pressure detecting and control mechanism is set on Disappear and boil 7 top of pipe, computer control system 1 is electrically connected respectively with pressure detecting and control mechanism, steam oven 9.
In the present embodiment, hypertonia in pipe 7 is boiled when disappearing, pressure detecting and control mechanism receive signal and send meter to Calculation machine control system 1 is simultaneously alarmed, and the detection of 1 control pressure of simultaneous computer control system and control mechanism pressure release and steam oven 9 stop It only heats to reduce pressure, preventing from disappearing, it is broken to boil pipe 7.
In the present embodiment, pressure detecting and control mechanism include probe 3, pressure control device 4, pressure sensor 10, visit First 3 one end is inserted into disappear and be boiled in pipe 7, and other end connection pressure sensor 10, pressure sensor 10 is connected by signal transmssion line 11 Computer control system 1;
4 one end of pressure control device connects sealing device 6, and the other end connects computer control system by signal transmssion line 11 System 1.Pressure sensor 10 is ceramic pressure sensor.
The size of probe 3 and 10 can detect pressure of pressure sensor, pressure control device 4 can experience instantaneous pressure overload Pressure release is directly opened, is controlled under normal pressure by computer control system 1.
Pressure sensor 10 is ceramic pressure sensor.With high resiliency, anticorrosive, wear-resistant, shock resistance and vibration Characteristic.Pressure sensor is arranged on to disappear and boil outside pipe, reduces acid and alkali corrosion.
Vapor conduit 5 connects steam oven conducting wire 8, and steam oven conducting wire 8 is connected to inside steam oven 9.Steam oven 9 passes through letter Number transmission line 11 is connect with computer control system 1.It is safe and reliable by way of signal transmssion line 11 in the present embodiment.
Principle:Hypertonia in pipe 7 is boiled when disappearing, pressure sensor 10 receives signal and transmitted by signal transmssion line 11 It to computer control system 1 and alarms, simultaneous computer control system 1 passes through 11 control pressure control device 4 of signal transmssion line Pressure release and steam oven 9 stop heating to reduce pressure, prevent from disappearing and boil pipe and crush.
Obviously, above-described embodiment of the utility model is only intended to clearly illustrate the utility model example, and It is not the restriction to the embodiment of the utility model.For those of ordinary skill in the art, in above description On the basis of can also make other variations or changes in different ways.There is no need and unable to give all embodiments It is exhaustive.All any modification, equivalent and improvement made within the spirit and principles of the present invention etc., should be included in Within the protection domain of the utility model claims.

Claims (5)

1. a kind of kjeldahl apparatus distilling apparatus with pressure alarm, pipe is boiled including disappearing(7), vapor conduit(5), steam Vapour stove(9), the vapor conduit(5)One end connection, which disappears, boils pipe(7)Inside, other end connection steam oven(9)Inside is also wrapped It includes to be fixed on to disappear and boils pipe(7)The sealing device of opening(6), sealing device(6)Upper fixation distillates fluid catheter(2), distillate fluid catheter (2)One end connection, which disappears, boils pipe(7), the other end, which is connected to disappear, boils pipe(7)It is external;
It is characterized in that, further include pressure detecting and control mechanism, computer control system(1), the pressure detecting and control Mechanism processed, which is set on to disappear, boils pipe(7)Top, computer control system(1)Respectively with pressure detecting and control mechanism, steam oven(9)Electricity Connection.
2. a kind of kjeldahl apparatus distilling apparatus with pressure alarm according to claim 1, it is characterised in that: The pressure detecting and control mechanism include probe(3), pressure control device(4), pressure sensor(10), the probe (3)One end, which is inserted into disappear, boils pipe(7)It is interior, other end connection pressure sensor(10), pressure sensor(10)Pass through signal transmssion line (11)Connect computer control system(1);
The pressure control device(4)One end connects sealing device(6), the other end passes through signal transmssion line(11)Connection calculates Machine control system(1).
3. a kind of kjeldahl apparatus distilling apparatus with pressure alarm according to claim 2, it is characterised in that: The pressure sensor(10)For ceramic pressure sensor.
4. a kind of kjeldahl apparatus distilling apparatus with pressure alarm according to claim 3, it is characterised in that: The vapor conduit(5)Connect steam oven conducting wire(8), steam oven conducting wire(8)It is connected to steam oven(9)It is internal.
5. a kind of kjeldahl apparatus distilling apparatus with pressure alarm according to claim 3, it is characterised in that: The steam oven(9)Pass through signal transmssion line(11)With computer control system(1)Connection.
CN201721564910.8U 2017-11-21 2017-11-21 A kind of kjeldahl apparatus distilling apparatus with pressure alarm Active CN207516324U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721564910.8U CN207516324U (en) 2017-11-21 2017-11-21 A kind of kjeldahl apparatus distilling apparatus with pressure alarm

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721564910.8U CN207516324U (en) 2017-11-21 2017-11-21 A kind of kjeldahl apparatus distilling apparatus with pressure alarm

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CN207516324U true CN207516324U (en) 2018-06-19

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115090345A (en) * 2022-05-23 2022-09-23 刘全生 Universal distillation instrument based on pressure dynamic monitoring and automatic alarm

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115090345A (en) * 2022-05-23 2022-09-23 刘全生 Universal distillation instrument based on pressure dynamic monitoring and automatic alarm

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Address after: 450001 No.1, floor 1, unit 1, building 12, No.11, Changchun Road, high tech Zone, Zhengzhou City, Henan Province

Patentee after: HENAN GRG METROLOGY & TEST CO.,LTD.

Patentee after: Radio and TV Measurement and Testing Group Co.,Ltd.

Address before: 450001 No.1, floor 1, unit 1, building 12, No.11, Changchun Road, high tech Zone, Zhengzhou City, Henan Province

Patentee before: HENAN GRG METROLOGY & TEST CO.,LTD.

Patentee before: GUANGZHOU GRG METROLOGY & TEST Co.,Ltd.

CP01 Change in the name or title of a patent holder