CN207493238U - A kind of device for detaching immiscible liquid - Google Patents
A kind of device for detaching immiscible liquid Download PDFInfo
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- CN207493238U CN207493238U CN201721527755.2U CN201721527755U CN207493238U CN 207493238 U CN207493238 U CN 207493238U CN 201721527755 U CN201721527755 U CN 201721527755U CN 207493238 U CN207493238 U CN 207493238U
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- flow container
- baffle
- solvent
- connecing
- immiscible liquid
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Abstract
The utility model provides a kind of device for detaching immiscible liquid, including connecing flow container, connect flow container is internally provided with the baffle being vertically arranged, baffle is fixed on the opposite both sides inner wall for connecing flow container, the both sides of the width direction of baffle and the two madial walls sealed connection for connecing flow container, the inner space for connecing flow container is divided into large space and small space by baffle, there are top notches and bottom notch between top and bottom respectively for the both sides of the length direction of baffle, top notch respectively connects large space with small space with bottom notch, connecing at small space is provided with refluxing opening on the side wall of flow container, connecing at large space is provided with inlet at the top of flow container.The utility model goes live liquid separation in single flash flow without people, carries out a liquid separation at the end of only needing, personnel cost is greatly saved, flow is made to become simple.
Description
Technical field
The utility model belongs to chemical technology field more particularly to a kind of device for detaching immiscible liquid.
Background technology
In Chemical Manufacture, following separation problem is frequently encountered：Certain hazardous solvent contained in separation solid material.Often
The separation method of rule is：The second harmless solvent is added in into solid, is distilled (solid product, You Hairong after mixing
Agent, harmless solvent are immiscible), two kinds of solvents boil together to be distilled out out of kettle, and is entered by condenser condensation and connect flow container,
Using two kinds of mutual exclusive properties of solvent, hazardous solvent is separated, harmless solvent is returned in kettle, and such operating method is only
Continuous operation can be realized in one cycle.
If using conventional operating method, first hazardous solvent and harmless solvent can only be distilled into one and connect liquid
After flow container layering is connect, liquid is squeezed into distillation still or will connect with delivery pump with harmless solvent by tank, hazardous solvent for harmless solvent
Tank is placed on higher position, and harmless solvent is divided into distillation still, and both of these case, which is intended to control, does not make harmless solvent enter steaming
It evaporates in kettle.Due to needing the boundary of artificial judgment liquid level and control valve, so can not achieve continuous operation.
In addition, conventional method operating process of the prior art is comparatively laborious, needs to be mostly used to a pump or liquid will be connect
Tank frame is high, frequent operation also bad control.
Utility model content
In view of this, first purpose of the utility model is to propose a kind of device for detaching immiscible liquid, to solve
Above-mentioned technical problem.
In order to achieve the above objectives, the technical solution of the utility model is realized in：
A kind of device for detaching immiscible liquid, including connecing flow container, connect flow container is internally provided with the baffle being vertically arranged,
Baffle is fixed on the opposite both sides inner wall for connecing flow container, the both sides of the width direction of baffle and the two madial walls sealing for connecing flow container
The inner space for connecing flow container is divided into large space and small space by connection, baffle, the both sides of the length direction of baffle respectively with top
There are top notch and bottom notch, top notch and bottom notch between portion and bottom respectively to connect large space and small space
Logical, connecing at small space is provided with refluxing opening on the side wall of flow container, and connecing at large space is provided with inlet at the top of flow container.
Further, the need for connecing flow container volume and being more than in a liquid separation operating process of the direct tube section at large space Internal baffle
The volume of solvent to be separated.
Further, height of the refluxing opening 12 apart from 11 bottom of baffle is (1 ÷ ρ 2 of ρ) × L；Wherein, ρ 1 is solid to be deposited in
The density of first solvent to be separated in body material, ρ 2 are the density for detaching the second solvent of the first solvent, and L is baffle 11
Total length, ρ 2 be more than ρ 1.
Further, refluxing opening and the inlet communication of distillation still, the outlet of distillation still and the import of condenser connect, condensation
The outlet of device is connected with connecing the inlet of flow container.
Further, the first bend pipe and the first observation visor, condensation are provided on the pipeline between refluxing opening and distillation still
The second bend pipe and the second observation visor are provided on pipeline between device and inlet.
Further, distillation still and connecing is connected by condenser between flow container, and condenser is located at distillation still and connects flow container
Top.
Further, condenser is obliquely installed, and the other end of condenser is higher than close to one end of the condenser of distillation still.
Further, the both sides of the length direction of baffle are respectively close to top and bottom.
The device that second purpose of the utility model is to provide any one above-mentioned separation immiscible liquid is solid in separation
Application in body material in residual solvent.
Wherein, remaining solvent is substantially hazardous solvent in solid material.
The third purpose of the utility model is to provide a kind of method for detaching residual solvent in solid material, and this method is excellent
Choosing realizes that specific separation method includes the following steps using any one above-mentioned device：
S1：The quantity of solvent detached as needed calculates the solvent size for connecing flow container 1；
S2：The solid material containing the first solvent is added in into distillation still, density is then added in into distillation still is more than the
One solvent and with immiscible second solvent of the first solvent and solid material；
S3：The second solvent is added in flow container so that the second solvent did not had bottom notch just to connecing；
S4：Start and distill, in distillation process, the condensed device of the first solvent and the mixture of the second solvent distilled out condenses
Enter large space afterwards, after the liquid level of the second solvent in small space reaches refluxing opening, the second solvent refluxing to distillation still, first
Solvent is stayed in large space, that is, realizes separation.
Relative to the prior art, the utility model has the advantage that：
(1) the utility model carries out a liquid separation without manual site's liquid separation in single flash flow at the end of only needing,
Personnel cost is greatly saved, flow is made to become simple；
(2) solvent (such as hazardous solvent) that the design of the utility model baffle effectively avoids the need for detaching is again introduced into
Into distillation still, while separation is more thorough, production efficiency higher.
Description of the drawings
The attached drawing for forming the part of the utility model is used to provide a further understanding of the present invention, this practicality is new
The illustrative embodiments and their description of type do not form the improper restriction to the utility model for explaining the utility model.
In attached drawing：
Fig. 1 is the structure diagram of the utility model embodiment；
Fig. 2 is the Distallation systm structure diagram described in the utility model embodiment；
Fig. 3 is Distallation systm structure diagram of the prior art.
Reference sign：
1st, flow container is connect；11st, baffle；12nd, refluxing opening；13rd, inlet；14th, bottom notch；15th, top notch；16th, small sky
Between；17th, large space；18th, top；19th, bottom；2nd, distillation still；3rd, condenser；4th, the first bend pipe；5th, the first observation visor；6th,
Two bend pipes；7th, the second observation visor；8th, third observation visor；9th, delivery pump.
Specific embodiment
It should be noted that in the absence of conflict, the feature in embodiment and embodiment in the utility model can
To be combined with each other.
In the description of the present invention, it is to be appreciated that term " " center ", " longitudinal direction ", " transverse direction ", " on ", " under ",
The orientation or position relationship of the instructions such as "front", "rear", "left", "right", " vertical ", " level ", " top ", " bottom ", " interior ", " outer " are
Based on orientation shown in the drawings or position relationship, it is for only for ease of description the utility model and simplifies description rather than instruction
Or imply that signified device or element there must be specific orientation, with specific azimuth configuration and operation, therefore be not understood that
For the limitation to the utility model.In addition, term " first ", " second " etc. are only used for description purpose, and it is not intended that instruction
Or imply relative importance or the implicit quantity for indicating indicated technical characteristic." first ", " second " etc. are defined as a result,
Feature can express or implicitly include one or more this feature.It is in the description of the present invention, unless another
It is described, " multiple " are meant that two or more.
In the description of the present invention, it should be noted that unless otherwise clearly defined and limited, term " is pacified
Dress ", " connected ", " connection " should be interpreted broadly, for example, it may be being fixedly connected or being detachably connected or integrally
Connection；Can be mechanical connection or electrical connection；It can be directly connected, can also be indirectly connected by intermediary,
It can be the connection inside two elements.For the ordinary skill in the art, on being understood by concrete condition
State concrete meaning of the term in the utility model.
The utility model will be described in detail below with reference to the accompanying drawings and embodiments.
As shown in Figure 1, a kind of device for detaching immiscible liquid, including connecing flow container 1, it is perpendicular to connect being internally provided with for flow container 1
The baffle 11 directly set, the both sides of the width direction of baffle 11 are separately fixed on the opposite both sides inner wall for connecing flow container 1, baffle
The both sides of 11 width direction and the two madial walls sealed connection for connecing flow container 1.The inner space for connecing flow container 1 is divided by baffle 11
Small one and large one large space 17 and small space 16.The both sides of the length direction of baffle 11 are respectively facing 18 He of top for connecing flow container 1
Bottom 19 extends and does not contact close to top 18 and bottom 19 but with top 18 and bottom 19, the both sides of the length direction of baffle 11
There are top notches 15 and bottom notch 14 between top 18 and bottom 19 respectively.Top notch 15 and bottom notch 14 are distinguished
Large space 17 is connected with small space 16.
As shown in Figure 1, refluxing opening 12 is arranged on the side wall for connecing flow container 1 at small space 16, inlet 13 is arranged on greatly
Top 18 at space 17.Connecing the volume size of flow container 1 and the specific installation site of baffle 11 needs by calculating, a liquid separation
The volume of need the first solvent to be separated in operating process should connect liquid less than the direct tube section at 17 Internal baffle 11 of large space
The volume of tank 1.The calculation formula of the mounting height of refluxing opening 12 is：The distance of best mounting height and 11 bottom of baffle=(the
The density of the solvent of the density of one solvent/second) 11 total length of * baffles.
As shown in Fig. 2, refluxing opening 12 and the inlet communication of distillation still 2, the outlet of distillation still 2 connect with the import of condenser 3
It connects, the outlet of condenser 3 is connected with connecing the inlet 13 of flow container 1.Is provided on pipeline between refluxing opening 12 and distillation still 2
One bend pipe 4 and the first observation visor 5, the first bend pipe 4 are used for anti-backflow, and the first observation visor 5 is used to observe the situation of pipeline.
The second bend pipe 6 and the second observation visor 7 are provided on pipeline between condenser 3 and inlet 13, the second bend pipe 6 is used to prevent
Reflux, the second observation visor 7 are used to observe the situation of pipeline.Condenser 3 is located at distillation still 2 and connects the top of flow container 1, condenser
3 are obliquely installed, and the import of condenser 3 is higher than the outlet of condenser 3.Bottom 19 on the pipeline of valve and reservoir by setting
There is third to observe visor 8.
As shown in figure 3, the lower end of the prior art for connecing flow container 1 passes through delivery pump 9 and the inlet communication of distillation still 2.It is existing
Operation principle in technology is：First the first solvent and the second solvent can only be distilled into one and connect flow container 1, first is molten
Second solvent after connecing flow container 1 and being layered, is squeezed into distillation still 2 or will connect flow container 1 with the second solvent with delivery pump 9 and put by agent
In higher position, the second solvent is divided into distillation still 2, two kinds of situations, which are intended to control, does not make the first solvent enter distillation still 2
It is interior.Due to needing, the artificial judgment page is demarcated and control valve is so can not achieve continuous operation.
The utility model is mentioned that a kind of separation method of immiscible liquid, includes the following steps：
S1：The quantity of solvent detached as needed calculates the size for connecing flow container 1；
S2：The solid material containing the first solvent is added in into distillation still 2, density is then added in into distillation still 2 is more than
First solvent and with immiscible second solvent of the first solvent and solid material；
S3：The second solvent is added in flow container 1 so that the second solvent did not had bottom notch 14 just to connecing；
S4：Start and distill, in distillation process, the condensed device 3 of the first solvent and the mixture of the second solvent distilled out is cold
Enter large space 17 after solidifying, after the liquid level of the second solvent in small space 16 reaches refluxing opening 12, the second solvent refluxing to steaming
Kettle 2 is evaporated, the first solvent is stayed in large space 17, that is, realizes separation.
The operation principle of the utility model：According to the volume of separation solvent, the volume size for connecing flow container 1 is calculated, is distilled
Before, a small amount of second solvent is added in toward connecing the inside of flow container 1, the liquid level of the second solvent is best not have bottom notch 14 just.
Refluxing opening 12 connects distillation still 2, and the lime set that the first solvent and the second solvent distill enters large space 17, the first solvent and second
Solvent is after connecing flow container 1 and being layered, and with the raising of liquid level, the second solvent enters distillation still 2 from 11 bottom of baffle to refluxing opening 12,
First solvent is stayed in into 11 right side of baffle.The first solvent can thus be stayed in and connect in the large space 17 of flow container 1, and the second solvent
Distillation still 2 can be flowed back into, is detached so as to fulfill by the first solvent, and can operate continuously, without manual operation, only needs one
Period finishes, and the first solvent for connecing 1 the inside of flow container is detached.
The above is only the preferred embodiment of the utility model only, is not intended to limit the utility model, all at this
Within the spirit and principle of utility model, any modification, equivalent replacement, improvement and so on should be included in the utility model
Protection domain within.
Claims (7)
1. a kind of device for detaching immiscible liquid, it is characterised in that：Including connecing flow container (1), being internally provided with for flow container (1) is connect
The baffle (11) being vertically arranged, baffle (11) are fixed on the opposite both sides inner wall for connecing flow container (1), the width side of baffle (11)
To both sides and connect two madial walls of flow container (1) and be tightly connected, the inner space for connecing flow container (1) is divided into big sky by baffle (11)
Between (17) and small space (16), there are tops between top (18) and bottom (19) respectively for the both sides of the length direction of baffle (11)
Portion's notch (15) and bottom notch (14), top notch (15) and bottom notch (14) are respectively by large space (17) and small space
(16) it connects, is provided with refluxing opening (12) on the side wall for connecing flow container (1) at small space (16), flow container is connect at large space (17)
(1) top (18) is provided with inlet (13).
2. the device of separation immiscible liquid according to claim 1, it is characterised in that：Large space (17) Internal baffle (11)
The direct tube section at place connects volume of flow container (1) volume more than the need solvent to be separated in a liquid separation operating process.
3. the device of separation immiscible liquid according to claim 1, it is characterised in that：Refluxing opening (12) is apart from baffle
(11) height of bottom is (1 ÷ ρ 2 of ρ) × L；Wherein, ρ 1 is the density for being deposited in the first solvent to be separated in solid material, ρ
2 be the density for detaching the second solvent of the first solvent, and L is the total length of baffle (11), and ρ 2 is more than ρ 1.
4. the device of separation immiscible liquid according to any one of claims 1 to 3, it is characterised in that：Refluxing opening (12)
With the inlet communication of distillation still (2), the outlet of distillation still (2) is connect with the import of condenser (3), the outlet of condenser (3) with
Connect inlet (13) connection of flow container (1).
5. the device of separation immiscible liquid according to claim 4, it is characterised in that：Refluxing opening (12) and distillation still
(2) the first bend pipe (4) and the first observation visor (5) are provided on the pipeline between；And/or condenser (3) and inlet (13)
Between pipeline on be provided with the second bend pipe (6) and second observation visor (7).
6. the device of separation immiscible liquid according to any one of claims 1 to 3, it is characterised in that：Distillation still (2) with
It connects and is connected by condenser (3) between flow container (1), condenser (3) is positioned at distillation still (2) and connects the top of flow container (1).
7. the device of separation immiscible liquid according to any one of claims 1 to 3, it is characterised in that：Baffle (11)
The both sides of length direction are respectively close to top (18) and bottom (19).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721527755.2U CN207493238U (en) | 2017-11-15 | 2017-11-15 | A kind of device for detaching immiscible liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721527755.2U CN207493238U (en) | 2017-11-15 | 2017-11-15 | A kind of device for detaching immiscible liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207493238U true CN207493238U (en) | 2018-06-15 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721527755.2U Active CN207493238U (en) | 2017-11-15 | 2017-11-15 | A kind of device for detaching immiscible liquid |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107715487A (en) * | 2017-11-15 | 2018-02-23 | 利安隆（珠海）新材料有限公司 | A kind of device and method for separating immiscible liquid |
-
2017
- 2017-11-15 CN CN201721527755.2U patent/CN207493238U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107715487A (en) * | 2017-11-15 | 2018-02-23 | 利安隆（珠海）新材料有限公司 | A kind of device and method for separating immiscible liquid |
| CN107715487B (en) * | 2017-11-15 | 2024-04-16 | 利安隆（珠海）新材料有限公司 | Device and method for separating immiscible liquids |
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