CN207463176U - The adjustable reaction kettle of reaction pressure and pressure-adjustable reaction kettle system - Google Patents
The adjustable reaction kettle of reaction pressure and pressure-adjustable reaction kettle system Download PDFInfo
- Publication number
- CN207463176U CN207463176U CN201721317509.4U CN201721317509U CN207463176U CN 207463176 U CN207463176 U CN 207463176U CN 201721317509 U CN201721317509 U CN 201721317509U CN 207463176 U CN207463176 U CN 207463176U
- Authority
- CN
- China
- Prior art keywords
- cavity
- reaction
- chamber
- reaction kettle
- adjustable
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 126
- 238000005984 hydrogenation reaction Methods 0.000 claims abstract description 54
- 239000002994 raw material Substances 0.000 claims abstract description 50
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 23
- 239000001257 hydrogen Substances 0.000 claims abstract description 23
- 238000005192 partition Methods 0.000 claims abstract description 23
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000000523 sample Substances 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 20
- 238000010438 heat treatment Methods 0.000 claims description 13
- 230000008676 import Effects 0.000 claims description 6
- 239000012043 crude product Substances 0.000 claims description 5
- 239000002904 solvent Substances 0.000 abstract description 22
- 238000004519 manufacturing process Methods 0.000 abstract description 11
- 239000000047 product Substances 0.000 description 10
- 239000000463 material Substances 0.000 description 4
- 230000008859 change Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
A kind of reaction kettle of adjustable reaction pressure and pressure-adjustable pressure-adjustable reaction kettle system, belong to reaction kettle device field.The reaction kettle of the adjustable reaction pressure includes the interior autoclave body for being equipped with cavity, the partition board that cavity is separated into raw material cavity and reaction chamber is equipped in autoclave body, the convection holes of multiple connection raw material cavities and reaction chamber are offered on partition board, the regulator board for being divided into convection cavity and hydrogenating chamber is equipped in reaction chamber, multiple connection convection cavities are offered on regulator board and hydrogenate the regulator hole of chamber, regulator board is also associated with the regulation component for driving its movement to adjust convection cavity and hydrogenate cavity pressure, autoclave body is equipped with the feed inlet connected with raw material cavity and the discharge gate connected with hydrogenation chamber and hydrogen delivery tube.The reaction kettle of adjustable reaction pressure provided by the utility model can promote hydrogen to mix and react with the solvent in reaction kettle, improve production efficiency.The utility model additionally provides the pressure-adjustable reaction kettle system of the reaction kettle comprising above-mentioned adjustable reaction pressure.
Description
Technical field
The utility model is related to reaction kettle device field, in particular to a kind of reaction kettle of adjustable reaction pressure
And pressure-adjustable reaction kettle system.
Background technology
Reaction kettle is the reaction vessel for being widely used in multiple key areas such as chemical industry, medicine, food, and it is each to be commonly used to production
Kind chemical products.The reaction kettle of adjustable reaction pressure is one kind of reaction kettle, in the reaction kettle operation of adjustable reaction pressure
In the process, it is often necessary to be passed through hydrogen after adding in plurality of raw materials into autoclave body.Under certain catalyst, pressure and temperature range
It is reacted, obtains product.But the reaction kettle of existing adjustable reaction pressure hydrogen in operation is difficult to and material solution
Carry out hydrogenation is sufficiently mixed, the reaction time is not only extended, reduces production efficiency, also reduces the yield of finished product.
Therefore, it is necessary to it is a kind of can be sufficiently mixed hydrogen and reaction dissolvent, improve production efficiency and product yield it is adjustable
Save the reaction kettle of reaction pressure.
Utility model content
The purpose of this utility model is to provide a kind of reaction kettle of adjustable reaction pressure, can promote hydrogen with it is anti-
The solvent in kettle is answered to mix and is reacted, improves production efficiency.
The another object of the utility model is to provide a kind of pressure-adjustable reaction kettle system, can improve object in reaction kettle
The reaction efficiency of material improves product yield.
What the embodiment of the utility model was realized in：
A kind of reaction kettle of adjustable reaction pressure is equipped with the autoclave body of cavity including in, is equipped in autoclave body by cavity point
The partition board of raw material cavity and reaction chamber is divided into, the convection holes of multiple connection raw material cavities and reaction chamber are offered on partition board, in reaction chamber
Equipped with being divided into convection cavity and hydrogenating the regulator board of chamber, multiple connection convection cavities are offered on regulator board and hydrogenate the tune of chamber
Hole is pressed, regulator board is also associated with the regulation component for driving its movement to adjust convection cavity and hydrogenate cavity pressure, and autoclave body is set
There are the feed inlet connected with raw material cavity and the discharge gate connected with hydrogenation chamber and hydrogen delivery tube.
In the utility model preferred embodiment, above-mentioned regulation component includes at least connecting rod being connect with regulator board
And the drive component moved back and forth for drive link.
In the utility model preferred embodiment, pressure regulator valve is equipped in above-mentioned at least one regulator hole, pressure regulator valve includes
The interior valve body equipped with valve chamber, the both ends of valve chamber are connected respectively by channel with the both ends of regulator hole, and being equipped in valve chamber can be along valve chamber
Movement is connected with spring to connect or block the spool of two passes between spool and the end wall of valve chamber.
In the utility model preferred embodiment, further include and sequentially pass through raw material cavity, convection cavity and extend to hydrogenation chamber
Interior probe tube.
In the utility model preferred embodiment, above-mentioned probe tube is located at convection cavity and the part of raw material cavity is respectively equipped with
Branch pipe, two branch pipes are respectively equipped with the first solenoid valve and second solenoid valve, and the part that probe tube is located at hydrogenation intracavitary is equipped with third
Solenoid valve.
In the utility model preferred embodiment, above-mentioned raw materials intracavitary is equipped at least one rotatable raw material paddle
Piece.
In the utility model preferred embodiment, at least one rotatable convection current paddle is equipped in above-mentioned convection cavity
Piece.
In the utility model preferred embodiment, above-mentioned hydrogenation intracavitary is equipped at least one rotatable reaction paddle
Piece.
In the utility model preferred embodiment, the outer wall of above-mentioned autoclave body is additionally provided with hollow heating jacket, heating folder
It is arranged with heat medium import and Crude product input.
The utility model additionally provides a kind of pressure-adjustable reaction kettle system, including the anti-of above-mentioned adjustable reaction pressure
Answer kettle.
The advantageous effect of the utility model embodiment is：The utility model embodiment provide adjustable reaction pressure it is anti-
Kettle is answered to include the interior autoclave body for being equipped with cavity, the partition board that cavity is separated into raw material cavity and reaction chamber is equipped in autoclave body, is opened on partition board
Convection holes equipped with multiple connection raw material cavities and reaction chamber, reaction chamber is interior to be equipped with the pressure regulation for being divided into convection cavity and hydrogenating chamber
Plate offers multiple connection convection cavities on regulator board and hydrogenates the regulator holes of chamber, and regulator board is also associated with driving its movement
With the regulation component for adjusting convection cavity and hydrogenating cavity pressure, autoclave body is equipped with the feed inlet connected with raw material cavity and connects with hydrogenation chamber
Logical discharge gate and hydrogen delivery tube.The reaction kettle of adjustable reaction pressure provided by the utility model can promote hydrogen with it is anti-
The solvent in kettle is answered to mix and is reacted, improves production efficiency.The utility model is additionally provided comprising above-mentioned adjustable reaction pressure
Reaction kettle pressure-adjustable reaction kettle system, the reaction efficiency of material in reactor can be improved, improve product yield.
Description of the drawings
It, below will be to use required in embodiment in order to illustrate more clearly of the technical solution of the utility model embodiment
Attached drawing be briefly described, it should be understood that the following drawings illustrates only some embodiments of the utility model, therefore should not be by
Regard the restriction to range as, for those of ordinary skill in the art, without creative efforts, may be used also
To obtain other relevant attached drawings according to these attached drawings.
Fig. 1 is the sectional view of the reaction kettle of adjustable reaction pressure that the utility model embodiment 1 provides；
Fig. 2 is the structure diagram of the reaction kettle of adjustable reaction pressure that the utility model embodiment 1 provides；
Fig. 3 is the sectional view of pressure-adjustable reaction kettle system that the utility model embodiment 2 provides；
Fig. 4 is the partial enlarged view at A in Fig. 3；
Fig. 5 is the sectional view of the pressure regulator valve in the utility model embodiment 2.
In figure：The reaction kettle of reaction pressure is adjusted in 001-；The reaction kettle of reaction pressure is adjusted in 002-；003- pressure-adjustables
Reaction kettle system；100- autoclave bodies；101- feed inlets；102- discharge gates；103- decelerating motors；104- agitating shafts；105- pressure regulator valves；
110- cavitys；111- raw material cavities；112- reaction chambers；113- convection cavities；114- hydrogenates chamber；120- partition boards；121- convection holes；130-
Regulator board；131- regulator holes；140- hydrogen delivery tubes；150- connecting rods；151- hydraulic cylinders；160- valve bodies；161- valve chambers；162-
Spring；163- spools；164- channels；170- probe tubes；171- branch pipes；The first solenoid valves of 172-；173- second solenoid valves；174-
Third solenoid valve；180- raw material stirring blades；190- convection current stirring blades；200- reacts stirring blade；210- heating jackets；
211- heat medium imports；212- Crude product inputs；300- pedestals；310- idler wheels.
Specific embodiment
Purpose, technical scheme and advantage to make the utility model embodiment are clearer, new below in conjunction with this practicality
Attached drawing in type embodiment, the technical scheme in the utility model embodiment is clearly and completely described, it is clear that is retouched
The embodiment stated is the utility model part of the embodiment, instead of all the embodiments.Usually here described in attached drawing and
The component of the utility model embodiment shown can be configured to arrange and design with a variety of different.
Therefore, requirement is not intended to limit to the detailed description of the embodiment of the utility model provided in the accompanying drawings below
The scope of the utility model of protection, but it is merely representative of the selected embodiment of the utility model.Based in the utility model
Embodiment, those of ordinary skill in the art's all other embodiments obtained without creative efforts, all
Belong to the range of the utility model protection.
It should be noted that：Similar label and letter represents similar terms in following attached drawing, therefore, once a certain Xiang Yi
It is defined in a attached drawing, does not then need to that it is further defined and explained in subsequent attached drawing.
In the description of the present invention, it should be noted that term " " center ", " on ", " under ", it is "left", "right", " perpendicular
Directly ", the orientation of the instructions such as " level ", " interior ", " outer " or position relationship be based on orientation shown in the drawings or position relationship or
The utility model product using when the orientation usually put or position relationship, be for only for ease of description the utility model and letter
Change description rather than instruction or imply signified device or element must have specific orientation, with specific azimuth configuration and
Operation, therefore it is not intended that limitation to the utility model.In addition, term " first ", " second ", " third " etc. are only used for area
Divide description, and it is not intended that instruction or hint relative importance.
In addition, the terms such as term " level ", " vertical ", " pendency " are not offered as requiring component abswolute level or pendency, and
It is that can be slightly tilted.It is not to represent the structure if " level " only refers to that its direction is more horizontal with respect to for " vertical "
It has to fully horizontally, but can be slightly tilted.
In the description of the present invention, it should also be noted that, unless otherwise clearly defined and limited, term " is set
Put ", " installation ", " connected ", " connection " should be interpreted broadly, for example, it may be fixedly connected or be detachably connected,
Or it is integrally connected；Can be mechanical connection or electrical connection；It can be directly connected, intermediary can also be passed through
It is indirectly connected, can be the connection inside two elements.For the ordinary skill in the art, it can be managed with concrete condition
Solve concrete meaning of the above-mentioned term in the utility model.
In the utility model unless specifically defined or limited otherwise, fisrt feature second feature it " on " or it
" under " can be in direct contact including the first and second features, it is not to be in direct contact but lead to that can also include the first and second features
Cross the other characterisation contact between them.Moreover, fisrt feature second feature " on ", " top " and " above " including
One feature is right over second feature and oblique upper or is merely representative of fisrt feature level height higher than second feature.First is special
Sign second feature " under ", " lower section " and " below " including fisrt feature immediately below second feature and obliquely downward or only
Represent that fisrt feature level height is less than second feature.
Embodiment 1
Referring to Fig.1 and 2, present embodiments providing a kind of reaction kettle 001 of adjustable reaction pressure, set including in
There is the autoclave body 100 of cavity 110, the partition board 120 that cavity 110 is separated into raw material cavity 111 and reaction chamber 112 be equipped in autoclave body 100,
The convection holes 121 of multiple connection raw material cavities 111 and reaction chamber 112 are offered on partition board 120, are equipped in reaction chamber 112 by its point
It is divided into convection cavity 113 and hydrogenates the regulator board 130 of chamber 114, multiple connection convection cavities 113 and hydrogenation are offered on regulator board 130
The regulator hole 131 of chamber 114, regulator board 130 be also associated with for drive its movement with adjust convection cavity 113 and hydrogenation chamber 114 in
The regulation component of pressure, autoclave body 100 are equipped with the feed inlet 101 connected with raw material cavity 111 and the discharge gate connected with hydrogenation chamber 114
102 and hydrogen delivery tube 140.In the present embodiment, it is equipped with the partition board 120 of parallel arrangement in autoclave body 100 successively from top to bottom and adjusts
Pressing plate 130, partition board 120 are equipped with 40 convection holes 121, and regulator board 130 is equipped with 20 regulator holes 131, autoclave body 100
Top and bottom are respectively equipped with feed inlet 101 and discharge gate 102, and the top of autoclave body 100 sequentially passes through 120 He of partition board equipped with bottom end
Regulator board 130 extends to the hydrogen delivery tube 140 in hydrogenation chamber 114.
The reaction kettle 001 for the adjustable reaction pressure that the utility model embodiment provides can promote in hydrogen and reaction kettle
Solvent mix and react, accelerate the progress of hydrogenation, improve production efficiency and product yield.The adjustable reaction pressure
The cavity 110 that 001 inside of reaction kettle is set is separated into raw material cavity 111, convection cavity 113 and hydrogenation by partition board 120 and regulator board 130
Chamber 114, and raw material cavity 111 is connected with convection cavity 113 by the convection holes 121 opened up on partition board 120, convection cavity 113 and hydrogenation
Chamber 114 is connected by the regulator hole 131 opened up on regulator board 130, and raw material cavity 111 is put into from the feed inlet 101 at 100 top of autoclave body
Solvent and raw material sequentially entered in convection cavity 113 and hydrogenation chamber 114 by convection holes 121 and regulator hole 131, it is and defeated with hydrogen
The hydrogen that pipe 140 is passed through in hydrogenation chamber 114 is sent to carry out hydrogenation after mixing, regulator board 130 is driven to move by regulation component
With the volume size for adjusting convection cavity 113 and hydrogenating chamber 114, so as to adjust the pressure of the solvent in hydrogenation chamber 114, promote hydrogen
The hydrogen that delivery pipe 140 is passed through in hydrogenation chamber 114 is dissolved in solvent, promotes the progress of hydrogenation, improves product yield, instead
Reaction solution after answering is discharged by the discharge gate 102 that 100 bottom of autoclave body is set.
Regulation component includes at least connecting rod 150 being connect with regulator board 130 and is moved back and forth for drive link 150
Drive component.Regulation component in the present embodiment includes two hydraulic cylinders 151 and two connecting rods perpendicular to regulator board 130
150, one end of two connecting rods 150 is connect respectively with regulator board 130, the other end piston rod with two hydraulic cylinders 151 respectively
Connection.It is moved back and forth by two 151 controls connecting rods 150 of hydraulic cylinder, regulator board 130 can be driven to move up and down, work as pressure regulation
When plate 130 moves down, the volume of hydrogenation chamber 114 reduces, and hydrogenates the pressure increase in chamber 114, is passed through hydrogen delivery tube 140
Hydrogen in hydrogenation chamber 114 is sufficiently mixed with solvent, promotes the progress of hydrogenation, when regulator board 130 moves up, hydrogenation
The solvent of chamber 114 increases, the pressure increase in convection cavity 113.Raw material is made in convection cavity 113 to enter hydrogenation chamber 114 to be reacted,
So cycle repeatedly, can greatly improve the progress of hydrogenation, improve production efficiency and product yield.
The reaction kettle 001 of adjustable reaction pressure, which is additionally provided with, to be sequentially passed through raw material cavity 111, convection cavity 113 and extends to hydrogen
Change the probe tube 170 in chamber 114.Staff can divide the reaction solution sampling in hydrogenation chamber 114 by probe tube 170
Analysis, in order to adjust production technology in real time according to production process, to obtain best production technology.
At least one rotatable raw material stirring blade 180 is equipped in raw material cavity 111, at least one is equipped in convection cavity 113
A rotatable convection current stirring blade 190, hydrogenation chamber 114 is interior to be equipped at least one rotatable reaction stirring blade 200.This reality
It applies in example, 100 top of autoclave body is equipped with decelerating motor 103, and decelerating motor 103, which is connected with, to be through in cavity 110 and sequentially pass through
Partition board 120 and regulator board 130 extend to the agitating shaft 104 in hydrogenation chamber 114, and agitating shaft 104, which is equipped with, to be located in raw material cavity 111
A raw material stirring blade 180, a convection current stirring blade 190 in convection cavity 113, positioned at hydrogenation chamber 114 in
One reaction stirring blade 200.When staff starts decelerating motor 103, and agitating shaft 104 is driven to rotate, agitating shaft 104 is same
When raw material stirring blade 180, convection current stirring blade 190 and reaction stirring blade 200 is driven to rotate, while to raw material cavity 111, right
Stream chamber 113 and the solvent hydrogenated in chamber 114 are stirred, and stir material, ensure that stablizing for reaction carries out.
The outer wall of autoclave body 100 is additionally provided with hollow heating jacket 210, and heating jacket 210 is equipped with 211 He of heat medium import
Crude product input 212.Staff can be passed through hot steam, hot water into heating jacket 210 by heat medium import 211
Or the heat mediums such as heating oil are internally heated autoclave body 100, and the heat medium discharge in heating jacket 210 is added
Heat or replacement Posterior circle are passed through in heating jacket 210.
Embodiment 2
Fig. 3, Fig. 4 and Fig. 5 are please referred to, the present embodiment provides a kind of pressure-adjustable reaction kettle system 003, including adjustable anti-
The reaction kettle 002 of pressure and the pedestal 300 for placing the reaction kettle 002 of adjustable reaction pressure are answered, the bottom of pedestal 300 is set
There are four idler wheel 310, wherein the reaction kettle 002 of adjustable reaction pressure includes the interior autoclave body 100 for being equipped with cavity 110, autoclave body 100
It is interior to be equipped with the partition board 120 that cavity 110 is separated into raw material cavity 111 and reaction chamber 112, offer 40 connections on partition board 120
The convection holes 121 of raw material cavity 111 and reaction chamber 112, interior be equipped with of reaction chamber 112 are divided into convection cavity 113 and hydrogenation chamber 114
Regulator board 130,20 connection convection cavities 113 are offered on regulator board 130 and hydrogenate the regulator holes 131 of chamber 114, regulator board
130 are also associated with the regulation component for driving its movement to adjust convection cavity 113 and hydrogenate pressure in chamber 114, regulation component
Two hydraulic cylinders including two connecting rods 150 being connect with regulator board 130 and for two connecting rods 150 to be driven to move back and forth
151；Autoclave body 100 is equipped with the feed inlet 101 connected with raw material cavity 111 and the discharge gate 102 connected with hydrogenation chamber 114 and hydrogen is defeated
Send pipe 140.It is equipped with the partition board 120 of parallel arrangement and regulator board 130 in autoclave body 100 successively from top to bottom, partition board 120 is equipped with four
Ten convection holes 121, regulator board 130 are equipped with 20 regulator holes 131, and the top and bottom of autoclave body 100 are respectively equipped with charging
Mouth 101 and discharge gate 102, the top of autoclave body 100 sequentially passes through partition board 120 equipped with bottom end and regulator board 130 extends to hydrogenation chamber
Hydrogen delivery tube 140 in 114.The reaction kettle 001 of adjustable reaction pressure, which is additionally provided with, sequentially passes through raw material cavity 111, convection cavity
113 and extend to hydrogenation chamber 114 in probe tube 170.100 top of autoclave body is equipped with decelerating motor 103, and decelerating motor 103 connects
Have and be through in cavity 110 and sequentially pass through partition board 120 and regulator board 130 extends to agitating shaft 104 in hydrogenation chamber 114, stir
Axis 104 is mixed to stir equipped with a raw material stirring blade 180 in raw material cavity 111, a convection current in convection cavity 113
Mix blade 190, a reaction stirring blade 200 in hydrogenation chamber 114.The outer wall of autoclave body 100 is additionally provided with hollow heating
Chuck 210, heating jacket 210 are equipped with heat medium import 211 and Crude product input 212.
Pressure regulator valve 105 is equipped in each regulator hole 131, pressure regulator valve 105 includes the interior valve body 160 for being equipped with valve chamber 161, valve
The both ends of chamber 161 are connected respectively by channel 164 with the both ends of regulator hole 131, and being equipped in valve chamber 161 can move along valve chamber 161
To connect or block the spool 163 of two passes 164, spring 162 is connected between spool 163 and the end wall of valve chamber 161.It is adjusting
The pressure regulator valve 105 set in pressure hole 131 can effectively adjust the pressure of 130 both sides of regulator board, make convection cavity 113 and hydrogenation chamber
Solvent in 114 is connected in pressure change maximum generates exchange of solvent, when regulator board 130 moves up, in convection cavity 113
Pressure increase, the solvent push spool 163 in convection cavity 113 overcomes the elastic stress of spring 162 move, up to spool 163
The channel 164 that being moved to connects 161 both ends of valve chamber is interconnected, and convection cavity 113 is connected with hydrogenation chamber 114 at this time, convection cavity
Solvent in 113, which enters in hydrogenation chamber 114, is ready for hydrogenation；When regulator board 130 moves down, in convection cavity 113
Pressure reduction, the elastic stress of spring 162 pushes spool 163 to move backward, 164 phase of channel for connecting 161 both ends of valve chamber
It mutually blocks, the solvent in convection cavity 113 cannot be introduced into hydrogenation chamber 114, pass through kettle after hydrogenating the raw material hydrogenation in chamber 114
The discharge gate 102 connected with hydrogenation chamber 114 of 100 bottom of body setting is discharged.
Probe tube 170 is located at convection cavity 113 and the part of raw material cavity 111 is respectively equipped with branch pipe 171, and two branch pipes 171 divide
Not She You the first solenoid valve 172 and second solenoid valve 173, probe tube 170 be located at hydrogenation chamber 114 in part be equipped with third electromagnetism
Valve 174, wherein, the branch pipe 171 that probe tube 170 is located at 111 part of raw material cavity is equipped with the first solenoid valve 172, probe tube 170
Branch pipe 171 in 113 part of convection cavity is equipped with second solenoid valve 173.User can be as needed respectively to raw material cavity
111st, the solvent in convection cavity 113 and hydrogenation chamber 114 is sampled and chemically examines, when needs sample the solvent in hydrogenation chamber 114
During chemical examination, need to close the first solenoid valve 172 and second solenoid valve 173 and open third solenoid valve 174, it is possible to pass through sampling
The solvent sample that pipe 170 is obtained in hydrogenation chamber 114 is chemically examined；When needing to solvent sample examination in convection cavity 113, need
It closes the first solenoid valve 172 and third solenoid valve 174 and opens second solenoid valve 173, it is possible to be obtained by probe tube 170
Solvent sample in hydrogenation chamber 114 is chemically examined；When needing to solvent sample examination in raw material cavity 111, closing is needed
Two solenoid valves 173 and third solenoid valve 174 simultaneously open the first solenoid valve 172, it is possible to obtain raw material cavity by probe tube 170
Solvent sample in 111 is chemically examined.
The above descriptions are merely preferred embodiments of the present invention, is not intended to limit the utility model, for this
For the technical staff in field, various modifications and changes may be made to the present invention.It is all in the spirit and principles of the utility model
Within, any modification, equivalent replacement, improvement and so on should be included within the scope of protection of this utility model.
Claims (10)
1. a kind of reaction kettle of adjustable reaction pressure, which is characterized in that it include in be equipped with the autoclave body of cavity, in the autoclave body
Equipped with the partition board that the cavity is separated into raw material cavity and reaction chamber, offered on the partition board multiple connections raw material cavities and
The convection holes of the reaction chamber, the reaction chamber is interior to be equipped with the regulator board for being divided into convection cavity and hydrogenating chamber, the pressure regulation
The regulator hole of multiple connections convection cavity and the hydrogenation chamber is offered on plate, the regulator board is also associated with driving it
To adjust the regulation component of the convection cavity and the hydrogenation cavity pressure, the autoclave body is equipped with and is connected with the raw material cavity for movement
Feed inlet and with the discharge gate that connects of hydrogenation chamber and hydrogen delivery tube.
2. the reaction kettle of adjustable reaction pressure according to claim 1, which is characterized in that the regulation component include with
An at least connecting rod and the drive component for the connecting rod to be driven to move back and forth for the regulator board connection.
3. the reaction kettle of adjustable reaction pressure according to claim 1, which is characterized in that at least one regulator hole
Interior to be equipped with pressure regulator valve, the pressure regulator valve includes the interior valve body for being equipped with valve chamber, the both ends of the valve chamber respectively by channel with it is described
The both ends connection of regulator hole, the valve chamber is interior to be equipped with the valve that can be moved along the valve chamber to connect or block two channels
Spring is connected between the end wall of core, the spool and the valve chamber.
4. the reaction kettle of adjustable reaction pressure according to claim 1, which is characterized in that further include described in sequentially passing through
Raw material cavity, the convection cavity and the probe tube for extending to the hydrogenation intracavitary.
5. the reaction kettle of adjustable reaction pressure according to claim 4, which is characterized in that the probe tube is located at described
The part of convection cavity and the raw material cavity is respectively equipped with branch pipe, and two branch pipes are respectively equipped with the first solenoid valve and the second electromagnetism
Valve, the part that the probe tube is located at the hydrogenation intracavitary are equipped with third solenoid valve.
6. the reaction kettle of adjustable reaction pressure according to claim 5, which is characterized in that be equipped with extremely in the raw material cavity
A few rotatable raw material stirring blade.
7. the reaction kettle of adjustable reaction pressure according to claim 1, which is characterized in that be equipped with extremely in the convection cavity
A few rotatable convection current stirring blade.
8. the reaction kettle of adjustable reaction pressure according to claim 1, which is characterized in that the hydrogenation intracavitary is equipped with extremely
A few rotatable reaction stirring blade.
9. the reaction kettle of adjustable reaction pressure according to claim 1, which is characterized in that the outer wall of the autoclave body is also set
There is hollow heating jacket, the heating jacket is equipped with heat medium import and Crude product input.
10. a kind of pressure-adjustable reaction kettle system, which is characterized in that it includes adjustable as claimed in any one of claims 1-9 wherein
Save the reaction kettle of reaction pressure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721317509.4U CN207463176U (en) | 2017-10-12 | 2017-10-12 | The adjustable reaction kettle of reaction pressure and pressure-adjustable reaction kettle system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721317509.4U CN207463176U (en) | 2017-10-12 | 2017-10-12 | The adjustable reaction kettle of reaction pressure and pressure-adjustable reaction kettle system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207463176U true CN207463176U (en) | 2018-06-08 |
Family
ID=62267828
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721317509.4U Expired - Fee Related CN207463176U (en) | 2017-10-12 | 2017-10-12 | The adjustable reaction kettle of reaction pressure and pressure-adjustable reaction kettle system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207463176U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107469736A (en) * | 2017-10-12 | 2017-12-15 | 重庆农药化工（集团）有限公司 | The reactor and pressure-adjustable reactor system of adjustable reaction pressure |
-
2017
- 2017-10-12 CN CN201721317509.4U patent/CN207463176U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107469736A (en) * | 2017-10-12 | 2017-12-15 | 重庆农药化工（集团）有限公司 | The reactor and pressure-adjustable reactor system of adjustable reaction pressure |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107469736A (en) | The reactor and pressure-adjustable reactor system of adjustable reaction pressure | |
| CN207463176U (en) | The adjustable reaction kettle of reaction pressure and pressure-adjustable reaction kettle system | |
| CN107937251A (en) | Circulation batch mixing formula biology enzyme agitating device in a kind of | |
| CN208426913U (en) | A kind of mildy wash emulsifier unit | |
| CN201906483U (en) | Leaching device | |
| CN206810292U (en) | A kind of glue reactor stirred using hot-fluid | |
| CN207680595U (en) | A kind of silica gel reaction kettle of recycle stock up and down | |
| CN202762430U (en) | Defoaming agent reactor | |
| CN210496424U (en) | Stirring reaction kettle for production of bean phospholipid fertilizer | |
| CN208583348U (en) | A kind of petrochemical industry reaction kettle | |
| CN210356941U (en) | Raw material stirring equipment for production of film forming auxiliary agent | |
| CN207591770U (en) | A kind of antifoaming agent reaction kettle | |
| CN207478441U (en) | Ferment automatic milk feeder | |
| CN204275970U (en) | A kind of reactor | |
| CN209848871U (en) | Improved reaction kettle | |
| CN209005736U (en) | A kind of reaction kettle stirring structure with feed paddle | |
| CN206355982U (en) | A kind of cooling water circulation highly effective reaction kettle | |
| CN212091008U (en) | Continuous liquid-liquid extraction kettle | |
| CN211814438U (en) | Fermentation cylinder is used in production of health products raw materials | |
| CN217698836U (en) | Pharmacy is with mixing cauldron | |
| CN101480601B (en) | Intracavity stick-shaped ultrasonic cyclic flow reactor | |
| CN219722885U (en) | Biological medicine reaction kettle with built-in efficient mixing structure | |
| CN208151376U (en) | A kind of liquid fermentation tank | |
| CN215234175U (en) | Structure for producing homogeneous bacteria remover | |
| CN217490897U (en) | Multilayer formula stirring reation kettle |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180608 |