CN207446199U - A kind of process units of organic amine electroplating additive - Google Patents
A kind of process units of organic amine electroplating additive Download PDFInfo
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- CN207446199U CN207446199U CN201721474954.1U CN201721474954U CN207446199U CN 207446199 U CN207446199 U CN 207446199U CN 201721474954 U CN201721474954 U CN 201721474954U CN 207446199 U CN207446199 U CN 207446199U
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- reaction kettle
- kettle body
- air inlet
- inlet pipe
- frame type
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Abstract
The utility model provides a kind of process units of organic amine electroplating additive, including reaction kettle body, reaction kettle body upper end is equipped with reaction kettle cover, reaction kettle body side wall is equipped with horizontal air inlet pipe, vertical air inlet pipe is equipped in reaction kettle body, horizontal air inlet pipe connects connection with vertical air inlet pipe, multi-turn air outlet pipe is equipped in reaction kettle body from top to bottom, multi-turn air outlet pipe connects connection with vertical air inlet pipe, air outlet pipe medial surface is evenly equipped with venthole, permeable watertight film is fixed on venthole, the outlet tube of reaction kettle body lower end is detachably connected with Rose Box, Rose Box is equipped with filter screen diagonally downward, the corresponding Rose Box side wall in filter screen lower end is equipped with discharge nozzle, discharge nozzle is equipped with outlet valve；The utility model can be such that hydrogen is quickly spread in the reaction solution of reaction kettle body, so as to effectively increase reduction reaction efficiency, while reflect that completion can be directly filtered in year, collection catalyst is convenient, reduces production cost.
Description
Technical field
The utility model is related to technical field of chemical, and in particular to a kind of production dress of organic amine electroplating additive
It puts.
Background technology
The reaction process of organic amine is more complicated, and more convenient so far, clean method is that organic amine is corresponding
For nitro compound in Pd/C as catalyst, hydrogen carries out reduction reaction as reducing agent.It needs to use during the reaction
Reaction kettle, but existing reaction kettle is passed directly into reaction kettle upper end when being passed through hydrogen, therefore make the efficiency of reduction reaction big
It is big to reduce, while when to catalyst filtration, also need that reaction solution importing filtering ponds are filtered processing by the pump housing, it is very numb
It is tired, add production cost.
Utility model content
The purpose of this utility model is to provide a kind of process units of organic amine electroplating additive, and hydrogen can be made quick
It is spread in the reaction solution of reaction kettle body, so as to effectively increase reduction reaction efficiency, while reflects that completion can be carried out directly in year
Filtering, collection catalyst is convenient, reduces production cost.
To achieve the above object, the utility model provides following technical solution：
A kind of process units of organic amine electroplating additive, including reaction kettle body, air outlet pipe, Rose Box, the reaction
Autoclave body upper end is equipped with reaction kettle cover, and the reaction kettle is equipped with engine base between covering end, is installed with motor on the engine base, institute
The reaction kettle around engine base is stated to cover equipped with feeding-in solid body mouth, reagent feeds mouth, inert gas air inlet, the reaction kettle body by
Supporting rack support is fixed, and agitating device is equipped in the reaction kettle body, the agitating device is by motor-driven rotation, the reaction
Autoclave body side wall is equipped with horizontal air inlet pipe, and the transverse direction air inlet pipe is equipped with intake valve, lower end seal is equipped in the reaction kettle body
The vertical air inlet pipe closed, the transverse direction air inlet pipe connect connection with vertical air inlet pipe top, in the reaction kettle body from top to bottom
Equipped with multi-turn air outlet pipe, air outlet pipe described in multi-turn connects connection with vertical air inlet pipe, and the air outlet pipe medial surface is evenly equipped with out
Stomata, permeable watertight film is fixed on the venthole, and the reaction kettle body lower end is equipped with outlet tube, is set on the outlet tube
There is liquid valve, the outlet tube lower end is detachably connected with Rose Box, and the Rose Box is equipped with filter screen diagonally downward,
Corresponding Rose Box side wall described in the filter screen is equipped with discharge nozzle, and the discharge nozzle is equipped with outlet valve, the Rose Box
Lower end is equipped with filtrate (liquid.
Further, the agitating device includes agitating shaft, frame type stirring blade, is had on the agitating shaft from upper
Multiple frame type stirring blades, the output shaft of the motor sequentially pass through engine base, react kettle cover and pass through on shaft coupling and agitating shaft
End connection.
Further, the frame type stirring blade includes frame type stirring blade one, frame type stirring blade two, the agitating shaft
On frame type stirring blade one, frame type stirring blade two be arranged alternately from top to bottom, the frame type stirring blade one is along level side
Upward length of blade is the 1/2-2/3 of the length of blade of frame type stirring blade two.
Further, the reaction kettle body is externally provided with electric heating cover, and the reaction kettle is covered equipped with temperature detector, described
The outer upper end of reaction kettle body is equipped with controller, and the electric heating cover, temperature detector are connected with controller.
Further, the outlet tube passes through flanged joint with Rose Box upper end.
Further, the permeable watertight film includes ePTFE, ePTFE Modified Membrane or ePTFE laminating composite films.
Further, it is equipped with from top to bottom in the reaction kettle body and irises out tracheae.
The beneficial effects of the utility model are：
The process units of the utility model organic amine electroplating additive, hydrogen enter to permeable watertight by venthole
Film is entered in reaction solution, hydrogen can be made quickly to be spread in reaction solution, so as to effectively increase reduction reaction efficiency.It has reacted
Reaction solution after complete is filtered by Rose Box, and catalyst is stayed on filter screen, then again by discharge nozzle to catalyst into
Row is collected, easy to operate, reduces production cost.Further, by setting the frame type stirring blade one of different size, and hand over
For being arranged on agitating shaft, stirring efficiency can be improved to carrying out comprehensive stirring in the reaction solution in reaction kettle, so that
Reaction effect is more preferable.
Description of the drawings
It in order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment
Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only
It is some embodiments of the utility model, for those of ordinary skill in the art, in the premise not made the creative labor
Under, it can also be obtained according to these attached drawings other attached drawings.
Fig. 1 is the structure diagram of the utility model；
In figure：1st, reaction kettle body；2nd, kettle cover is reacted；3rd, motor；4th, feeding-in solid body mouth；5th, reagent feeds mouth；6th, indifferent gas
Body air inlet；7th, supporting rack；8th, air outlet pipe；9th, Rose Box；10th, horizontal air inlet pipe；11st, intake valve；12nd, vertical air inlet pipe；13、
Venthole；14th, outlet tube；15th, filter screen；16th, discharge nozzle；17th, filtrate (liquid；18th, agitating shaft；19th, frame type stirring blade
One；20th, frame type stirring blade two；21st, electric heating cover；22nd, temperature detector；23rd, controller.
Specific embodiment
It is new below in conjunction with this practicality to make the purpose, technical scheme and advantage of the utility model embodiment clearer
Attached drawing in type embodiment, the technical scheme in the utility model embodiment is clearly and completely described, it is clear that is retouched
The embodiment stated is the utility model part of the embodiment, instead of all the embodiments.Based on the implementation in the utility model
Example, those of ordinary skill in the art's all other embodiments obtained without creative efforts, belongs to
The scope of the utility model protection.
As shown in Figure 1, a kind of process units of organic amine electroplating additive, including reaction kettle body 1, air outlet pipe 8, filtering
Case 9,1 upper end of reaction kettle body are equipped with reaction kettle cover 2, engine base are equipped between 2 upper end of reaction kettle cover, motor is installed on engine base
3, the reaction kettle cover 2 around engine base is equipped with feeding-in solid body mouth 4, reagent feeds mouth 5, inert gas air inlet 6, reaction kettle body 1
Fixation is supported by supporting rack 7, is equipped with agitating device in reaction kettle body 1, agitating device drives rotation, 1 side of reaction kettle body by motor 3
Wall is equipped with horizontal air inlet pipe 10, and horizontal air inlet pipe 10 is equipped with intake valve 11, the perpendicular of lower end closed is equipped in reaction kettle body 1
To air inlet pipe 12, horizontal air inlet pipe 10 connects connection with vertical 12 top of air inlet pipe, and multi-turn is equipped with from top to bottom in reaction kettle body 1
Air outlet pipe 8, multi-turn air outlet pipe 8 connect connection with vertical air inlet pipe 12, and 8 medial surface of air outlet pipe is evenly equipped with venthole 13, outlet
Permeable watertight film is fixed on hole 13,1 lower end of reaction kettle body is equipped with outlet tube 14, and outlet tube 14 is equipped with liquid valve, goes out liquid
14 lower end of pipe is detachably connected with Rose Box 9, and Rose Box 9 is equipped with filter screen 15 diagonally downward, and filter screen 15 is corresponding
9 side wall of Rose Box is equipped with discharge nozzle 16, and discharge nozzle 16 is equipped with outlet valve, and 9 lower end of Rose Box is equipped with filtrate (liquid 17.
Wherein, agitating device includes agitating shaft 18, frame type stirring blade, has multiple frames from upper on agitating shaft 18
Stirrer paddle, the output shaft of motor 3 sequentially pass through engine base, reaction kettle cover 2 and pass through shaft coupling and be connected with 18 upper end of agitating shaft.
Wherein, frame type stirring blade includes frame type stirring blade 1, frame type stirring blade 2 20, the frame on agitating shaft 18
Formula stirrer paddle 1, frame type stirring blade 2 20 are arranged alternately from top to bottom, frame type stirring blade 1 in the horizontal direction on
Length of blade for frame type stirring blade 2 20 length of blade 1/2-2/3.
Wherein, reaction kettle body 1 is externally provided with electric heating cover 21, and reaction kettle cover 2 is equipped with temperature detector 22, reaction kettle body 1
Outer upper end is equipped with controller 23, and electric heating cover 21, temperature detector 22 are connected with controller 23.
Wherein, outlet tube 14 passes through flanged joint with 9 upper end of Rose Box.
Wherein, permeable watertight film includes ePTFE, ePTFE Modified Membrane or ePTFE laminating composite films.
Wherein, tracheae 8 is irised out equipped with 3 from top to bottom in reaction kettle body 1.
The process units of the utility model organic amine electroplating additive, hydrogen pass sequentially through horizontal air inlet pipe, vertically into
Tracheae enters in multi-turn air outlet pipe, then is entered to by the permeable watertight film that enters to of venthole in reaction solution, and hydrogen can be made fast
Speed is spread in reaction solution, so as to effectively increase reduction reaction efficiency.Reaction solution after the reaction was complete is carried out by Rose Box
Filtering, the filtrate after filtering exports and is further processed by the corresponding pump housing, and Pd/C catalyst is then stayed in filter screen
On, then catalyst is collected by discharge nozzle again, it is easy to operate, reduce production cost.
Further, by setting the frame type stirring blade one of different size, have with short, and be alternately disposed at agitating shaft
On, stirring efficiency can be improved, so that reaction effect is more preferable to carrying out comprehensive stirring in the reaction solution in reaction kettle.
Above example is only to illustrate the technical solution of the utility model, rather than its limitations；Although with reference to foregoing reality
Example is applied the utility model is described in detail, it will be understood by those of ordinary skill in the art that：It still can be to preceding
The technical solution recorded in each embodiment is stated to modify or carry out equivalent substitution to which part technical characteristic；And these
Modification is replaced, and the essence of appropriate technical solution is not made to depart from the spirit and model of various embodiments of the utility model technical solution
It encloses.
Claims (7)
1. a kind of process units of organic amine electroplating additive, including reaction kettle body (1), reaction kettle body (1) upper end is set
There is reaction kettle cover (2), be equipped with engine base between described reaction kettle cover (2) upper end, motor (3), institute are installed on the engine base
The reaction kettle cover (2) stated around engine base is equipped with feeding-in solid body mouth (4), reagent feeds mouth (5), inert gas air inlet (6), institute
State reaction kettle body (1) and supported by supporting rack (7) and fixed, be equipped with agitating device in the reaction kettle body (1), the agitating device by
Motor (3) driving rotates, it is characterised in that：Air outlet pipe (8), Rose Box (9) are further included, is set on reaction kettle body (1) side wall
There is horizontal air inlet pipe (10), the transverse direction air inlet pipe (10) is equipped with intake valve (11), lower end is equipped in the reaction kettle body (1)
The vertical air inlet pipe (12) of closing, the transverse direction air inlet pipe (10) connect connection, the reaction with vertical air inlet pipe (12) top
Multi-turn air outlet pipe (8) is equipped in autoclave body (1) from top to bottom, air outlet pipe (8) is connected with vertical air inlet pipe (12) described in multi-turn
It connects, air outlet pipe (8) medial surface is evenly equipped with venthole (13), and permeable watertight film, institute are fixed on the venthole (13)
Reaction kettle body (1) lower end is stated equipped with outlet tube (14), the outlet tube (14) is equipped with liquid valve, outlet tube (14) lower end
It is detachably connected with Rose Box (9), the Rose Box (9) is equipped with filter screen (15) diagonally downward, the filter screen
(15) the corresponding Rose Box in lower end (9) side wall is equipped with discharge nozzle (16), and the discharge nozzle (16) is equipped with outlet valve, the mistake
Filter box (9) lower end is equipped with filtrate (liquid (17).
2. the process units of organic amine electroplating additive according to claim 1, it is characterised in that：The agitating device
It is described from upper multiple frame type stirring blades that have on the agitating shaft (18) including agitating shaft (18), frame type stirring blade
The output shaft of motor (3) sequentially passes through engine base, reaction kettle cover (2) and passes through shaft coupling and be connected with agitating shaft (18) upper end.
3. the process units of organic amine electroplating additive according to claim 2, it is characterised in that：The frame type stirring
Blade includes frame type stirring blade one (19), frame type stirring blade two (20), the frame type stirring blade on the agitating shaft (18)
One (19), frame type stirring blade two (20) are arranged alternately from top to bottom, the frame type stirring blade one (19) in the horizontal direction on
Length of blade for frame type stirring blade two (20) length of blade 1/2-2/3.
4. the process units of organic amine electroplating additive according to claim 1, it is characterised in that：The reaction kettle body
(1) electric heating cover (21) is externally provided with, the reaction kettle cover (2) is equipped with temperature detector (22), and the reaction kettle body (1) is outside upper
End is equipped with controller (23), and the electric heating cover (21), temperature detector (22) are connected with controller (23).
5. the process units of organic amine electroplating additive according to claim 1, it is characterised in that：The outlet tube
(14) flanged joint is passed through with Rose Box (9) upper end.
6. the process units of organic amine electroplating additive according to claim 1, it is characterised in that：It is described ventilative impermeable
Moisture film includes ePTFE, ePTFE Modified Membrane or ePTFE laminating composite films.
7. the process units of organic amine electroplating additive according to claim 1, it is characterised in that：The reaction kettle body
(1) in tracheae (8) is irised out equipped with 3 from top to bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721474954.1U CN207446199U (en) | 2017-11-07 | 2017-11-07 | A kind of process units of organic amine electroplating additive |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721474954.1U CN207446199U (en) | 2017-11-07 | 2017-11-07 | A kind of process units of organic amine electroplating additive |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207446199U true CN207446199U (en) | 2018-06-05 |
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ID=62254400
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721474954.1U Active CN207446199U (en) | 2017-11-07 | 2017-11-07 | A kind of process units of organic amine electroplating additive |
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| Country | Link |
|---|---|
| CN (1) | CN207446199U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113509902A (en) * | 2021-05-22 | 2021-10-19 | 合肥膳之纤生物科技有限公司 | Functional plant polysaccharide receptor coupling purification system |
-
2017
- 2017-11-07 CN CN201721474954.1U patent/CN207446199U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113509902A (en) * | 2021-05-22 | 2021-10-19 | 合肥膳之纤生物科技有限公司 | Functional plant polysaccharide receptor coupling purification system |
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