CN207412819U - A kind of modularization ionic liquid rapidly purifies device - Google Patents

A kind of modularization ionic liquid rapidly purifies device Download PDF

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Publication number
CN207412819U
CN207412819U CN201820083963.6U CN201820083963U CN207412819U CN 207412819 U CN207412819 U CN 207412819U CN 201820083963 U CN201820083963 U CN 201820083963U CN 207412819 U CN207412819 U CN 207412819U
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China
Prior art keywords
housing
ionic liquid
modularization
partition plate
filler
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CN201820083963.6U
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Chinese (zh)
Inventor
任旭华
李凯明
沈珏峰
钟锡明
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ZHEJIANG LANDE ENERGY TECHNOLOGY DEVELOPMENT CO LTD
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ZHEJIANG LANDE ENERGY TECHNOLOGY DEVELOPMENT CO LTD
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Abstract

The utility model is related to ionic liquid production fields, specifically disclose a kind of modularization ionic liquid and rapidly purify device.The modularization ionic liquid rapidly purifies device, including housing and is arranged on the in vivo filler module of shell, and the housing includes the upper shell and lower housing of releasable connection each other, and the upper shell and lower housing compress filler module;The both ends of the housing are respectively equipped with material channel, and the one end of the material channel away from housing is equipped with connector, and shut-off valve is equipped between connector and housing;The filler module includes cylinder, and parallel distribution has several partition plates vertically in the cylinder, and packing layer is formed between two neighboring partition plate;It is distributed with the through hole axially through partition plate on the partition plate, the through hole stagger setting on adjacent two layers partition plate.Above-described modularization ionic liquid rapidly purifies device, simple in construction, easy to disassemble and assemble, simplifies purification step, reduces the contaminated risk of product.

Description

A kind of modularization ionic liquid rapidly purifies device
Technical field
The utility model is related to ionic liquid production fields, and in particular to a kind of modularization ionic liquid rapidly purifies dress It puts.
Background technology
Ionic liquid is a kind of low-temperature molten salt, is made of organic cation and inorganic anion.Ionic liquid external manifestation Go out a kind of physical flow, and inherent chemical property has the property of salt.Compared with traditional organic solvent, ionic liquid The advantages of body is main table has:Almost without vapour pressure;It is non-volatile, it does not burn, avoids volatile contaminant;Liquid journey is wide, liquid temperature Degree scope can reach 180-300 DEG C;Acid-base property is adjustable;Good thermal stability and chemical stability.
The production of ionic liquid includes synthesis, purifying, drying and other steps, takes off organic matter wherein being included in purification step, takes off Water, decolorization process.In existing production technology, each purification step is required to individual purification kettle, in different purification kettles Add corresponding purification media(Such as activated carbon, molecular sieve, aluminium oxide, silica gel, resin), to reach purifying purpose.The system Not only device category is various, complicated, inconvenient, and product or intermediate products are repeatedly transported between different devices, Active hydrogen on product or intermediate products is easily oxidized, meanwhile, the contact between product and pipeline and each purification kettle, Unpredictable pollution can be brought, influences the quality of final product.
The content of the invention
The technical problem to be solved by the present invention is to provide a kind of modularization ionic liquids to rapidly purify device, structure letter It is single, it is convenient for disassembly and assembly, simplify purification step, reduce the contaminated risk of product.
In order to solve the above-mentioned technical problem, the technical scheme that the utility model is provided is as follows:A kind of modularization ionic liquid Device is rapidly purified, including housing and is arranged on the in vivo filler module of shell, the housing includes the upper of releasable connection each other Housing and lower housing, the upper shell and lower housing compress filler module;The both ends of the housing are respectively equipped with material channel, The one end of the material channel away from housing is equipped with connector, and shut-off valve is equipped between connector and housing;Described fills out Expect that module includes cylinder, parallel distribution there are several partition plates vertically in the cylinder, and filler is formed between two neighboring partition plate Layer;It is distributed with the through hole axially through partition plate on the partition plate, the through hole stagger setting on adjacent two layers partition plate.
Preferably, the connector is quick union.
Preferably, the position that the filler module ends are contacted with upper shell is equipped with gasket.
Preferably, the end face of the cylinder is higher than the end face of partition plate, and groove is formed at the both ends of filler module.
Preferably, the filler in described filler layer is one kind in activated carbon, molecular sieve, aluminium oxide, silica gel and resin Or several mixing.
It is had the advantages that using above-mentioned technical proposal:
Releasable connection between upper shell and lower housing described in 1., and the upper shell and lower housing compress filler mould Block, the installation of filler are divided equally conveniently with replacing.Due to the multiple purification steps of equipment collection and one, for filling out for each purification step Doses is limited, so need periodically to be replaced, therefore the convenience of replacement has great practical value.
2. multiple packing layers are distributed in filler module, filler not of the same race, which can classify, fills to different packing layers, It realizes the removal of impurity not of the same race, not only reduces the quantity of equipment, simplify purification procedures.It is and original pure due to reducing The connecting pipeline of number of devices and equipment room in change system reduces the risk that ionic liquid is aoxidized.The device be applicable in The production environment of small lot, such as product trial production or laboratory use.
3. the purification devices are attached by the connector at both ends with relevant device, connector can be arranged to connect soon Head, the disassembling, assembling and replacing of purification devices is convenient, modularized production and use convenient for purification devices.
4. the position that filler module ends are contacted with upper shell is equipped with gasket, effectively avoid liquid from filler module and Gap between housing is by influencing purification effect.
Description of the drawings
Fig. 1 is the structure diagram that the present embodiment modularization ionic liquid rapidly purifies device;
Fig. 2 is the partial enlarged view at A in Fig. 1;
Fig. 3 is the structure diagram that the present embodiment modularization ionic liquid rapidly purifies filler module in device.
Specific embodiment
In order to make the purpose of the utility model, technical solutions and advantages more clearly understood, below in conjunction with attached drawing and implementation Example, is further elaborated the utility model.It should be appreciated that specific embodiment described herein is only used to explain The utility model is not used to limit the utility model.
Embodiment
As shown in Figure 1, a kind of modularization ionic liquid rapidly purifies device, including housing and the in vivo filler of shell is arranged on Module 1, the housing is including the upper shell 4 of releasable connection and lower housing 5, the upper shell 4 and lower housing 5 compress each other Filler module 1.Releasable connection between the upper shell 4 and lower housing 5, and the upper shell 4 and lower housing 5 compress filler Module 1, the installation of filler are divided equally conveniently with replacing.Due to the multiple purification steps of equipment collection and one, for each purification step Amount of filler it is limited, so needing periodically to be replaced, therefore the convenience of replacement has great practical value.
As shown in Figure 1, the both ends of the housing are respectively equipped with material channel, the one end of the material channel away from housing is set There is connector 3, the connector 3 is preferably quick union.Shut-off valve 2 is equipped between connector 3 and housing.The purification devices It is attached by the connector 3 at both ends with relevant device, connector 3 can be arranged to quick union, the dismounting of purification devices It is convenient to replace, modularized production and use convenient for purification devices.
As shown in Figures 2 and 3, the filler module 1 includes cylinder 11, parallel distribution vertically in the cylinder 11 There are several partition plates 14, packing layer 6 is formed between two neighboring partition plate 14.It is distributed on the partition plate 14 axially through partition plate 14 through hole 13,13 stagger setting of through hole on adjacent two layers partition plate 14.Multiple packing layers 6 are distributed in filler module 1, it is different The filler of kind can classify filling to different packing layers 6, realize the removal of impurity not of the same race, not only reduce the number of equipment Amount, simplifies purification procedures.And due to the connecting pipeline for reducing number of devices and equipment room in original purification system, drop The risk that low ionic liquid is aoxidized.The device is applicable in the production environment with small lot, such as product trial production or laboratory It uses.The position that 1 end of filler module is contacted with upper shell 4 is equipped with gasket 12.The end face of the cylinder 11 be higher than every The end face of plate 14, and form groove 15 at the both ends of filler module 1.1 end of filler module is equipped with the position that upper shell 4 contacts Gasket 12 effectively avoids liquid from the gap between filler module 1 and housing by influencing purification effect.The filler Filler in layer 6 is the mixing of one or more of activated carbon, molecular sieve, aluminium oxide, silica gel and resin.
Above-described modularization ionic liquid rapidly purifies device, simple in construction, easy to disassemble and assemble, simplifies purification step, Reduce the contaminated risk of product.
In short, the above is only the preferred embodiment of the utility model only, it is not intended to limit the utility model, it is all All any modification, equivalent and improvement made within spirit of the present utility model and principle etc., should be included in this practicality Within new protection domain.

Claims (5)

1. a kind of modularization ionic liquid rapidly purifies device, it is characterised in that:Including housing and it is arranged on the in vivo filler of shell Module(1), the housing includes the upper shell of releasable connection each other(4)And lower housing(5), the upper shell(4)With under Housing(5)Compress filler module(1);The both ends of the housing are respectively equipped with material channel, and the material channel is away from housing One end is equipped with connector(3), and in connector(3)Shut-off valve is equipped between housing(2);The filler module(1)Including Cylinder(11), the cylinder(11)Inside parallel distribution has several partition plates vertically(14), two neighboring partition plate(14)Between shape Into packing layer(6);The partition plate(14)On be distributed with axially through partition plate(14)Through hole(13), adjacent two layers partition plate (14)On through hole(13)Stagger setting.
2. modularization ionic liquid according to claim 1 rapidly purifies device, it is characterised in that:The connector (3)For quick union.
3. modularization ionic liquid according to claim 1 or 2 rapidly purifies device, it is characterised in that:The filler mould Block(1)End and upper shell(4)The position of contact is equipped with gasket(12).
4. modularization ionic liquid according to claim 3 rapidly purifies device, it is characterised in that:The cylinder(11)'s End face is higher than partition plate(14)End face, and in filler module(1)Both ends formed groove(15).
5. the modularization ionic liquid according to claim 1 or 2 or 4 rapidly purifies device, it is characterised in that:The filler Layer(6)Interior filler is the mixing of one or more of activated carbon, molecular sieve, aluminium oxide, silica gel and resin.
CN201820083963.6U 2018-01-18 2018-01-18 A kind of modularization ionic liquid rapidly purifies device Active CN207412819U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820083963.6U CN207412819U (en) 2018-01-18 2018-01-18 A kind of modularization ionic liquid rapidly purifies device

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Application Number Priority Date Filing Date Title
CN201820083963.6U CN207412819U (en) 2018-01-18 2018-01-18 A kind of modularization ionic liquid rapidly purifies device

Publications (1)

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CN207412819U true CN207412819U (en) 2018-05-29

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109499076A (en) * 2018-11-12 2019-03-22 徐州工程学院 A kind of ionic liquid purification devices

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109499076A (en) * 2018-11-12 2019-03-22 徐州工程学院 A kind of ionic liquid purification devices
CN109499076B (en) * 2018-11-12 2020-09-29 徐州工程学院 Ionic liquid purification device

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GR01 Patent grant
GR01 Patent grant
CB03 Change of inventor or designer information

Inventor after: Ren Xuhua

Inventor after: Shen Juefeng

Inventor after: Zhong Ximing

Inventor before: Ren Xuhua

Inventor before: Li Kaiming

Inventor before: Shen Juefeng

Inventor before: Zhong Ximing

CB03 Change of inventor or designer information