CN207342682U - It is used to prepare the glassed steel reaction vessels of aminotrimethylenephosphonic acid - Google Patents
It is used to prepare the glassed steel reaction vessels of aminotrimethylenephosphonic acid Download PDFInfo
- Publication number
- CN207342682U CN207342682U CN201720483855.3U CN201720483855U CN207342682U CN 207342682 U CN207342682 U CN 207342682U CN 201720483855 U CN201720483855 U CN 201720483855U CN 207342682 U CN207342682 U CN 207342682U
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- CN
- China
- Prior art keywords
- bearing
- autoclave body
- hollow shaft
- cavity
- hollow
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- Physical Or Chemical Processes And Apparatus (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model discloses a kind of glassed steel reaction vessels for being used to prepare aminotrimethylenephosphonic acid,Autoclave body is equipped with inlet port and outlet port,The rabbling mechanism includes bearing,Motor,Hollow shaft and hollow blade,Bearing is equipped with cavity,After one end of bearing is fixed on autoclave body,Autoclave body encloses the accent of the bearing upper plenum one end,Motor is fixed on the other end of bearing,One end that the accent of the output terminal of motor from the bearing upper plenum other end is extend into cavity with the hollow shaft is fixedly connected,The other end of hollow shaft extend into autoclave body inner cavity after passing through the axis hole set on autoclave body and is connected with hollow blade,The part that hollow shaft is located in bearing cavity is equipped with input port,The part that hollow shaft is located in autoclave body inner cavity is equipped with multiple delivery outlets,The inner cavity of hollow blade is corresponding with the delivery outlet in hollow shaft,Hollow blade is equipped with fumarole；Gas supply mechanism is further included, the output terminal of the gas supply mechanism is connected with bearing.The utility model improves material mixing efficiency.
Description
Technical field
It the utility model is related to a kind of glassed steel reaction vessels for being used to prepare aminotrimethylenephosphonic acid.
Background technology
Glassed steel reaction vessels are by the glass containing high silicon dioxide, the inner surface in steel vessel are served as a contrast, through high temperature sintering
Adherence is in becoming composite product securely on metal surface.Therefore, glassed steel reaction vessels had both had the mechanical performance of steel,
There is the resistance to chemical corrosion of glass again, be a kind of excellent corrosion resistant apparatus.It is widely used in chemical field, but due to
The corrosivity of medium, reaction condition be sometimes hot and sometimes cold, transport, using, it is artificial the problems such as, such-and-such enamel layer damage always occurs
It is bad, cause unnecessary production to stop, wherein, the cleaning of existing glassed steel reaction vessels be all by by water pipe from the outlet of lower end
Be passed into what is carried out in glassed steel reaction vessels, and due to needing all to clean within one week side wall, thus in cleaning process, it is necessary to
Cleaning pipes are rotated, this easily to collide between Cleaning pipes and the opening of outlet, the opening of outlet is caused brokenly
Damage.
The utility model patent of Publication No. CN204522944U discloses a kind of glassed steel reaction vessels, it include cylinder,
Inlet port and outlet port, inlet port and outlet port are respectively and fixedly installed to the top and bottom of cylinder, set in the discharge port
There is rubber stopper, the through hole passed through for Cleaning pipes is provided with the rubber stopper.Rubber stopper, cleaning pipe are set in discharge port
When road is passed into cleaning in cylinder, Cleaning pipes are contacted with rubber stopper, will not touch the madial wall of discharge port, avoid cleaning
Discharge port is damaged in journey.However, above-mentioned glassed steel reaction vessels are in material stirring, reaction process, for including solid material
Reaction paste tend not to it is rapid sufficiently crush, stirring, have impact on slurry mixed effect, cause the reaction time to be grown, react
Yield is relatively low.
The content of the invention
The purpose of this utility model is to provide a kind of aminotrimethylenephosphonic acid that is used to prepare of improving material mixing efficiency
Glassed steel reaction vessels.
The technical solution for solving above-mentioned technical problem is as follows：
The glassed steel reaction vessels of aminotrimethylenephosphonic acid, including autoclave body, rabbling mechanism are used to prepare, autoclave body is equipped with charging
Mouth and discharge port, the rabbling mechanism include bearing, motor, hollow shaft and hollow blade, and bearing is equipped with cavity, bearing
After one end is fixed on autoclave body, autoclave body encloses the accent of the bearing upper plenum one end, and motor is fixed on the other end of bearing, electricity
One end that the accent of the output terminal of machine from the bearing upper plenum other end is extend into cavity with the hollow shaft is fixedly connected, hollow
The other end of axis extend into autoclave body inner cavity after passing through the axis hole set on autoclave body and is connected with hollow blade, and hollow shaft is positioned at branch
Part in seat cavity is equipped with input port, and the part that hollow shaft is located in autoclave body inner cavity is equipped with multiple delivery outlets, hollow blade
Inner cavity is corresponding with the delivery outlet in hollow shaft, and hollow blade is equipped with fumarole；Further include gas supply mechanism, the gas supply mechanism it is defeated
Outlet is connected with bearing.
The guide sleeve being arranged in autoclave body upper shaft hole is further included, the outside wall surface of guide sleeve is fixedly connected with autoclave body, and hollow shaft passes through
Guide sleeve, hollow shaft and guide sleeve clearance fit.
The internal face of guide sleeve is equipped with annular groove, and sealing ring is embedded with the annular groove.
The advantages of the utility model is：By setting gas supply mechanism, bearing and hollow shaft and hollow blade, pass through supply
The gases at high pressure of mechanism output, after gases at high pressure are entered in the cavity of bearing, the gas in cavity can only be from hollow shaft
Input port is entered in the inner cavity of hollow shaft, then is exported from the delivery outlet of hollow shaft, the gas exported from the delivery outlet of hollow shaft
Enter in the inner cavity of hollow blade, finally sprayed from fumarole, gas forms Cavitation effect in material, compressed air
Cavitation effect significantly improves the batch mixing efficiency of feed liquid, shortens the reaction time, has not only saved energy consumption, but also improves production
Efficiency.
Brief description of the drawings
Fig. 1 is the structure diagram for the glassed steel reaction vessels for being used to prepare aminotrimethylenephosphonic acid.
Embodiment
As shown in Figure 1, the glassed steel reaction vessels for being used to prepare aminotrimethylenephosphonic acid of the utility model, including autoclave body 1,
Rabbling mechanism, autoclave body 1 are equipped with feed inlet 1a and discharge port 1b, and the autoclave body 1 in present embodiment is by containing high silicon dioxide
Glass lined steel vessel inner surface, through high temperature sintering securely adherence in becoming composite product on metal surface.
The rabbling mechanism includes bearing 2, motor 3, hollow shaft 4 and hollow blade 5, and bearing 2 is equipped with cavity 2a, and the one of bearing 2
After end is fixed on autoclave body 1, autoclave body 1 encloses the accent of the 2 upper plenum one end of bearing, and motor 3 is fixed on the another of bearing 2
End, one end that the accent of output terminal from the 2 upper plenum other end of bearing of motor 3 is extend into cavity 2a with the hollow shaft 4 is consolidated
Fixed connection, is equipped with sealing structure, in this way, two of the cavity 2a on bearing 2 between the output terminal of motor 3 and the accent of bearing 2
End accent is closed, and becomes a closed cavity.The other end of hollow shaft 4 stretches into after passing through the axis hole set on autoclave body
It is connected into 1 inner cavity of autoclave body and with hollow blade 5, guide sleeve 6, outside wall surface and the autoclave body 1 of guide sleeve is provided with the axis hole on autoclave body 1
It is fixedly connected, hollow shaft 4 passes through guide sleeve 6, hollow shaft 4 and 6 clearance fit of guide sleeve.The internal face of guide sleeve 6 is equipped with annular groove, should
Sealing ring is embedded with annular groove.The part that hollow shaft 4 is located in 2 cavity 2a of bearing is equipped with input port, and hollow shaft 4 is located at autoclave body 1
Part in inner cavity is equipped with multiple delivery outlets, since cavity 2a is closed cavity, it is input to when there is gas in cavity 2a
After, the gas in cavity 2a can only be entered in the inner cavity of hollow shaft 4 from the input port in hollow shaft 4, then from hollow shaft 4
Delivery outlet exports.The inner cavity of hollow blade 5 is corresponding with the delivery outlet in hollow shaft, and hollow blade 5 is equipped with fumarole, from hollow
The gas of the delivery outlet output of axis 4 is entered in the inner cavity of hollow blade 5, is finally sprayed from fumarole, is pointed to autoclave body inner cavity
In material impacted and make material dispersion.Gas supply mechanism 7 is further included, the output terminal of the gas supply mechanism 7 is connected with bearing 2,
Gas supply mechanism 7 is made of negative pressure pump and pipeline, and through hole is equipped with the side wall of bearing 2, and the pipeline output terminal of gas supply mechanism is stretched
Enter into the through hole.
Claims (3)
1. the glassed steel reaction vessels of aminotrimethylenephosphonic acid are used to prepare, including autoclave body, rabbling mechanism, autoclave body are equipped with feed inlet
And discharge port, it is characterised in that：Autoclave body is made of steel vessel and the glass lined being arranged on the steel vessel inner surface, institute
Stating rabbling mechanism includes bearing, motor, hollow shaft and hollow blade, and bearing is equipped with cavity, and one end of bearing is fixed on kettle
After on body, autoclave body encloses the accent of the bearing upper plenum one end, and motor is fixed on the other end of bearing, the output terminal of motor from
One end that the accent of the bearing upper plenum other end is extend into cavity with the hollow shaft is fixedly connected, and the other end of hollow shaft is worn
It extend into autoclave body inner cavity after crossing the axis hole set on autoclave body and is connected with hollow blade, hollow shaft is located at the portion in bearing cavity
Input port is arranged with, the part that hollow shaft is located in autoclave body inner cavity is equipped with multiple delivery outlets, the inner cavity of hollow blade and hollow shaft
On delivery outlet correspond to, hollow blade is equipped with fumarole；Gas supply mechanism is further included, output terminal and the bearing of the gas supply mechanism connect
Connect.
2. the glassed steel reaction vessels according to claim 1 for being used to prepare aminotrimethylenephosphonic acid, it is characterised in that：Also wrap
Include the guide sleeve being arranged in autoclave body upper shaft hole, the outside wall surface of guide sleeve is fixedly connected with autoclave body, and hollow shaft passes through guide sleeve, hollow shaft with
Guide sleeve clearance fit.
3. the glassed steel reaction vessels according to claim 2 for being used to prepare aminotrimethylenephosphonic acid, it is characterised in that：Guide sleeve
Internal face be equipped with annular groove, be embedded with sealing ring in the annular groove.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720483855.3U CN207342682U (en) | 2017-05-03 | 2017-05-03 | It is used to prepare the glassed steel reaction vessels of aminotrimethylenephosphonic acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720483855.3U CN207342682U (en) | 2017-05-03 | 2017-05-03 | It is used to prepare the glassed steel reaction vessels of aminotrimethylenephosphonic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207342682U true CN207342682U (en) | 2018-05-11 |
Family
ID=62361256
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720483855.3U Expired - Fee Related CN207342682U (en) | 2017-05-03 | 2017-05-03 | It is used to prepare the glassed steel reaction vessels of aminotrimethylenephosphonic acid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207342682U (en) |
-
2017
- 2017-05-03 CN CN201720483855.3U patent/CN207342682U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180511 Termination date: 20190503 |