CN207335800U - A kind of fluidized-bed reactor solids flux measurement and effect inspection apparatus - Google Patents

A kind of fluidized-bed reactor solids flux measurement and effect inspection apparatus Download PDF

Info

Publication number
CN207335800U
CN207335800U CN201721508552.9U CN201721508552U CN207335800U CN 207335800 U CN207335800 U CN 207335800U CN 201721508552 U CN201721508552 U CN 201721508552U CN 207335800 U CN207335800 U CN 207335800U
Authority
CN
China
Prior art keywords
effect
inspection apparatus
settler
control valve
solids flux
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201721508552.9U
Other languages
Chinese (zh)
Inventor
田洪芹
王广亮
张正阳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Luoyang Kai Meisheng Petrochemical Equipment Co Ltd
Original Assignee
Luoyang Kai Meisheng Petrochemical Equipment Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Luoyang Kai Meisheng Petrochemical Equipment Co Ltd filed Critical Luoyang Kai Meisheng Petrochemical Equipment Co Ltd
Priority to CN201721508552.9U priority Critical patent/CN207335800U/en
Application granted granted Critical
Publication of CN207335800U publication Critical patent/CN207335800U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

Abstract

The utility model discloses a kind of measurement of fluidized-bed reactor solids flux and effect inspection apparatus, including two reaction tube control valves, effect settler, effect standpipe and two effect control valves, two reaction tube control valves are arranged on riser reactor upstream or catalyst transport, effect settler is arranged between two reaction tube control valves and is connected with riser reactor or catalyst transport, effect settler bottom is connected with effect standpipe, effect riser bottom is provided with solid outlet, and metering scale is provided with the effect standpipe;The effect control valve on top is arranged on effect settler, and the effect control valve of lower part is arranged at the upper end of effect standpipe lower part solid outlet.The utility model can carry out effect to the measurement result of solids flux measuring instrument, to implement to obtain accurate measurement data, also replace solids flux measuring instrument and carry out solids flux measurement, have multiple functions, very useful.

Description

A kind of fluidized-bed reactor solids flux measurement and effect inspection apparatus
Technical field
Measurement technical field is the utility model is related to, more particularly to a kind of fluidized-bed reactor solids flux Measurement and effect inspection apparatus.
Background technology
Circulating fluid bed reactor is widely used in the process industrials such as petroleum refining, chemical industry, metallurgy, electric power, in state's people's livelihood Great function is produced in production.Basin only residing for accurate judgement reactor flow field system, could be effectively to reactor Mass-and heat-transfer is adjusted, so as to improve the whole efficiency of reactor.In numerous parameters of reflection recirculating fluidized bed operating status In, solids flux is to determine the most important parameter in basin residing for system.Solids flux, also known as solid circulation flow rate, refer to unit By the solid masses of reactor unit cross-sectional area in time, circulating fluidization is most active field in contemporary fluidization research One of, it is the pass for realizing recirculating fluidized bed stable operation to efficiently control and adjust the granule organics in recirculating fluidized bed Key.The granular mass flux operating parameter basic as one, there is important influence for two phase flow.
Recirculating fluidized bed solids flux how is measured, there is many methods, the side of existing measure particle mass flux at present Method all respectively has shortcoming.Measured in recent years in multiphase flow the relatively advanced method of particle mass flux have nuclear magnetic resonance technique, CT into A variety of e measurement technologies such as picture, microwave method, gamma-rays, but the accuracy of these e measurement technologies how, can not but judge.
Chinese patent 201110449257.1 discloses a kind of recirculating fluidized bed solids flux measuring method and measuring system, The solid section average external volume point rate of the measuring surface is continuously measured within a period of time using fan-beam ray, is cut by two solids The correlation function of the function of time of face average external volume point rate calculates the solids flux of recirculating fluidized bed, and this method is without interference with anti- Answer the flow field in device, will not cause artificial gap operating, measurement result it is true and reliable, but how to confirm its measurement result It is true and reliable, do not refer to but.
Chinese patent 201110104058.7 discloses a kind of measuring device and method of solid circulation flow rate, and device is by valve The component composition such as door, height level switch, time set, material metering section and balance pipe, passes through height level switch and detects thing Discharge position, passes the signal along to time set, shows the solid accumulation time, avoids manual time-keeping error, and it is accurate to significantly improve measurement True property.The material metering section of the device directly chooses one section in dipleg, simple in structure, easy to operate.Balance pipe is set, can be subtracted Few interference of the measurement process to system operation, is particularly suitable for the survey of the solid circulation flow rate to high solid circulation flow-rate device Amount, moreover it can be used to measure solid circulation flow rate under pressurized conditions, also without it is open how effect its measurement result.
The content of the invention
The defects of present invention is in order to overcome the prior art, it is proposed that a kind of fluidized-bed reactor solids flux measurement and effect Device, the device can accurately measure fluidized-bed reactor solids flux, be reacted with effect prior art recirculating fluidized bed The order of accuarcy of device solids flux measuring method, can also be directly used in the solids flux for measuring fluidized-bed reactor.
The object of the invention to solve the technical problems is realized using following technical scheme.Itd is proposed according to the present invention A kind of measurement of fluidized-bed reactor solids flux and effect inspection apparatus, the fluidized-bed reactor include riser reactor 7, it is heavy Drop regenerator 2, stripping section 4, catalyst transport 10, wherein, described 7 one end of riser reactor is connected with sedimentation regenerator 2, The other end is connected with catalyst transport 10, and 2 bottom of sedimentation regenerator is connected with one end of stripping section 4,4 other end of stripping section with Catalyst transport 10 connects;Raw material and steam inlet 13, catalyst inlet 15 are provided with the riser reactor 7, is consolidated Body flux measurement instrument 8, stripping pars infrasegmentalis are provided with catalyst outlet 14, and reacting product outlet 1 is arranged at the top of sedimentation regenerator 2 Portion;
Solids flux effect inspection apparatus is additionally provided with the fluidized-bed reactor, which is additionally operable to flow The solids flux measurement of fluidized bed reactor, the solids flux effect inspection apparatus are arranged at upstream or the setting of riser reactor 7 In on catalyst transport 10;
The solids flux effect inspection apparatus includes reaction tube control valve 3, effect settler 5, effect standpipe 6 and effect control Valve 12, the reaction tube control valve 3 have two, and effect settler 5 is arranged between two reaction tube control valves 3, effect sedimentation 5 bottom of device is connected with effect standpipe 6, and 6 bottom of effect standpipe is provided with solid outlet 11, and metering is provided with the effect standpipe 6 Scale;
The effect control valve 12 has two, and the effect control valve on top is arranged on effect settler 5, the effect of lower part Test the upper end that control valve is arranged at 6 lower part solid outlet 11 of effect standpipe.
The object of the invention to solve the technical problems can be also applied to the following technical measures to achieve further.
Foregoing fluidized-bed reactor solids flux measurement and effect inspection apparatus, wherein, described two reaction tube control valves 3 are equal It is arranged at the upstream of riser reactor 7;Effect settler 5 is arranged between two reaction tube control valves 3 and anti-with riser Device 7 is answered to connect;
The effect control valve on top is arranged on the pipeline that effect settler 5 is connected with riser reactor 7.
Foregoing fluidized-bed reactor solids flux measurement and effect inspection apparatus, wherein, two reaction tube control valves 3 are respectively provided with In on catalyst transport 10;Effect settler 5 is arranged between two reaction tube control valves 3 and connects with catalyst transport 10 It is logical;
The effect control valve on top is arranged on the pipeline that effect settler 5 is connected with catalyst transport 10.
Foregoing fluidized-bed reactor solids flux measurement and effect inspection apparatus, wherein, the solids flux effect inspection apparatus is also Including effect return duct 9, which is connected with solid outlet 11, and the other end with riser reactor 7 with connecting It is logical.
Foregoing fluidized-bed reactor solids flux measurement and effect inspection apparatus, wherein, the solids flux effect inspection apparatus is also Including effect return duct 9, which is connected with solid outlet 11, and the other end with catalyst transport 10 with connecting It is logical.
Advantages of the present invention and effect are:
The utility model can accurately measure the solids flux of fluidized-bed reactor, with effect prior art recycle stream The order of accuarcy of fluidized bed reactor solids flux measuring method, can also be directly used in and measure the solid of fluidized-bed reactor and lead to Amount.Compared with prior art, the utility model has solids flux measurement accurately, and simple and practicable, function is more, highly practical spy Point.
Described above is only the general introduction of technical solution of the present invention, in order to better understand the technological means of the present invention, And can be practiced according to the content of specification, and in order to allow the present invention above-mentioned advantage and other purposes, feature and advantage It can become apparent, below especially exemplified by preferred embodiment, and with reference to attached drawing, describe in detail as follows.
Brief description of the drawings
Fig. 1 is the schematic diagram that solids flux measurement and effect inspection apparatus are arranged at riser reactor upstream;
Fig. 2 is the schematic device for increasing effect return duct on the basis of Fig. 1;
Fig. 3 is the schematic diagram that solids flux measurement and effect inspection apparatus are arranged at catalyst transport;
Fig. 4 is the schematic device for increasing effect return duct on the basis of Fig. 3.
Wherein:
1:Reacting product outlet 2:Sedimentation regenerator 3:Reaction tube control valve 4:Stripping section
5:Effect settler 6:Effect standpipe 7:Riser reactor 8:Solids flux measuring instrument 9:Effect is returned Flow tube 10:Catalyst transport 11:Solid outlet 12:Effect control valve 13:Raw material and steam inlet 14:Catalysis Agent outlet 15:Catalyst inlet
Embodiment
Further to illustrate the present invention to reach the technological means and effect that predetermined goal of the invention is taken, below in conjunction with Attached drawing and preferred embodiment, to according to a kind of fluidized-bed reactor solids flux measurement proposed by the present invention and effect inspection apparatus, its Embodiment, structure, feature and its effect, describe in detail as after.
Embodiment 1
A kind of fluidized-bed reactor solids flux measurement and effect inspection apparatus, the fluidized-bed reactor include lifting tube reaction Device 7, sedimentation regenerator 2, stripping section 4, catalyst transport 10, described 7 one end of riser reactor connect with sedimentation regenerator 2 Logical, the other end is connected with catalyst transport 10, and 2 bottom of sedimentation regenerator is connected with one end of stripping section 4, and stripping section 4 is another End is connected with catalyst transport 10;Raw material and steam inlet 13, catalyst inlet are provided with the riser reactor 7 15th, solids flux measuring instrument 8, stripping pars infrasegmentalis are provided with catalyst outlet 14, and reacting product outlet 1 is arranged at sedimentation regenerator 2 top;
Solids flux effect inspection apparatus is additionally provided with the fluidized-bed reactor, which can be additionally used in The solids flux measurement of fluidized-bed reactor, specifically, solids flux effect inspection apparatus includes reaction tube control valve 3, effect settles Device 5, effect standpipe 6 and effect control valve 12, reaction tube control valve 3 have two, may be contained within the upstream of riser reactor 7, Effect settler 5 is arranged between two reaction tube control valves 3 and is connected with riser reactor 7, as shown in Figure 1, effect is sunk 5 bottom of drop device is connected with effect standpipe 6, and 6 bottom of effect standpipe is provided with solid outlet 11, and meter is provided with the effect standpipe 6 Measure scale;Effect control valve 12 has two, and the effect control valve on top is arranged at effect settler 5 and connects with riser reactor 7 On logical pipeline, the effect control valve of lower part is arranged at the upper end of 6 lower part solid outlet 11 of effect standpipe.
Embodiment 2
As shown in Fig. 2, solids flux effect inspection apparatus further includes effect return duct 9, which goes out with solid Mouth 11 connects, and the other end is connected with riser reactor 7, the other the same as in Example 1.In this way, the solid in effect settler can Catalytic reaction is participated in be back to again in riser reactor.
Embodiment 3
As shown in figure 3, two reaction tube control valves 3 may be contained within catalyst transport 10, effect settler 5 is arranged at Connected between two reaction tube control valves 3 and with catalyst transport 10.The effect control valve on top is arranged at effect settler 5 On the pipeline connected with catalyst transport 10, the other the same as in Example 1.
Embodiment 4
As shown in figure 4, solids flux effect inspection apparatus further includes effect return duct 9, which goes out with solid Mouth 11 connects, and the other end is connected with catalyst transport 10, the other the same as in Example 3.
The fluidized-bed reactor is in use, feedstock oil and steam enter reactor from entrance 13, and catalyst is from catalyst Entrance 15 enters, and steam makes catalyst be in fluidized state, and in riser reactor 7, feedstock oil and catalyst reaction, go forward side by side Enter sedimentation regenerator, product is discharged from reacting product outlet, and the catalyst after use is regenerated in sedimentation regenerator, gone forward side by side Enter stripping section, the remaining part oil gasification discharge on stripping section, catalyst, the discarded catalyst that can not be recycled is from catalyst The discharge of outlet 14, the catalyst after regeneration enters catalyst transport 10 by stripping section, subsequently into riser reactor 7 after Continuous catalytic reaction.The solids flux in reactor can be measured by solids flux measuring instrument 8 in reaction process, at this time two A reaction tube control valve 3 is in opening, and two effect control valves 12 are turned off.
When needing to carry out effect to the solids flux that solids flux measuring instrument 8 measures, solids flux measuring instrument 8 is opened, First control the solids flux of riser reactor 7 to stablize, then open effect control valve (the effect control of lower part at this time on top Valve is still in closed mode), solid enters effect settler 5, by effect settler 5 and with graduated effect standpipe 6, meter Measure the solids flux T in certain time1;And the solids flux T measured on solids flux measuring instrument 8 is calculated at the same time2, effect completion Afterwards, the effect control valve on top is closed, opens the effect control valve of lower part, by the solid in effect settler 5 and effect standpipe 6 Discharged by solid outlet 11, the effect control valve of lower part is closed after drained.Surveyed by effect settler 5 and effect standpipe 6 Fixed solids flux T1The solids flux T measured to solids flux measuring instrument 82Carry out effect.
As shown in Figure 2 and Figure 4, an effect return duct 9, the solid after effect is complete can also be connected in solid outlet 11 Returned by effect return duct 9 in fluidized-bed reactor, continue to participate in catalytic reaction.
Further, if solids flux measuring instrument 8 breaks down, measurement work can not be normally completed, can be new with this practicality Solids flux effect inspection apparatus described in type substitutes 8 fluid bedreactors of solids flux measuring instrument and carries out solids flux measurement.
The above described is only a preferred embodiment of the present invention, not doing limitation in any form to the present invention, appoint What those skilled in the art, without departing from the scope of the present invention, is made a little using above-mentioned technology contents Change or the embodiment of modification, in the range of still falling within technical solution of the present invention.

Claims (5)

1. a kind of fluidized-bed reactor solids flux measurement and effect inspection apparatus, the fluidized-bed reactor include riser reactor (7), sedimentation regenerator (2), stripping section (4), catalyst transport (10), it is characterised in that:The riser reactor (7) one End is connected with sedimentation regenerator (2), and the other end is connected with catalyst transport (10), sedimentation regenerator (2) bottom and stripping section (4) one end connection, stripping section (4) other end are connected with catalyst transport (10);Set on the riser reactor (7) There are raw material and steam inlet (13), catalyst inlet (15), solids flux measuring instrument (8), stripping pars infrasegmentalis is provided with catalyst Export (14), reacting product outlet (1) is arranged at the top of sedimentation regenerator (2);
Solids flux effect inspection apparatus is additionally provided with the fluidized-bed reactor, which is additionally operable to fluid bed The solids flux measurement of reactor, the solids flux effect inspection apparatus are arranged at the upstream of riser reactor (7) or are arranged at On catalyst transport (10);
The solids flux effect inspection apparatus includes reaction tube control valve (3), effect settler (5), effect standpipe (6) and effect control Valve (12) processed, the reaction tube control valve (3) have two, effect settler (5) be arranged at two reaction tube control valves (3) it Between, effect settler (5) bottom is connected with effect standpipe (6), and effect standpipe (6) bottom is provided with solid outlet (11), the effect Test on standpipe (6) and be provided with metering scale;
The effect control valve (12) has two, and the effect control valve on top is arranged on effect settler (5), the effect of lower part Test the upper end that control valve is arranged at effect standpipe (6) lower part solid outlet (11).
2. fluidized-bed reactor solids flux measurement as claimed in claim 1 and effect inspection apparatus, it is characterised in that described two Reaction tube control valve (3) may be contained within the upstream of riser reactor (7);Effect settler (5) is arranged at two reaction management and control Connected between valve (3) processed and with riser reactor (7);
The effect control valve on top is arranged on the pipeline that effect settler (5) is connected with riser reactor (7).
3. fluidized-bed reactor solids flux measurement as claimed in claim 1 and effect inspection apparatus, it is characterised in that two reactions Pipe control valve (3) may be contained within catalyst transport (10);Effect settler (5) is arranged at two reaction tube control valves (3) Between and connect with catalyst transport (10);
The effect control valve on top is arranged on the pipeline that effect settler (5) is connected with catalyst transport (10).
4. fluidized-bed reactor solids flux measurement as claimed in claim 2 and effect inspection apparatus, it is characterised in that the solid Flux effect inspection apparatus further includes effect return duct (9), which is connected with solid outlet (11), the other end Connected with riser reactor (7).
5. fluidized-bed reactor solids flux measurement as claimed in claim 3 and effect inspection apparatus, it is characterised in that the solid Flux effect inspection apparatus further includes effect return duct (9), which is connected with solid outlet (11), the other end Connected with catalyst transport (10).
CN201721508552.9U 2017-11-13 2017-11-13 A kind of fluidized-bed reactor solids flux measurement and effect inspection apparatus Active CN207335800U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721508552.9U CN207335800U (en) 2017-11-13 2017-11-13 A kind of fluidized-bed reactor solids flux measurement and effect inspection apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721508552.9U CN207335800U (en) 2017-11-13 2017-11-13 A kind of fluidized-bed reactor solids flux measurement and effect inspection apparatus

Publications (1)

Publication Number Publication Date
CN207335800U true CN207335800U (en) 2018-05-08

Family

ID=62427663

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201721508552.9U Active CN207335800U (en) 2017-11-13 2017-11-13 A kind of fluidized-bed reactor solids flux measurement and effect inspection apparatus

Country Status (1)

Country Link
CN (1) CN207335800U (en)

Similar Documents

Publication Publication Date Title
CN102405398B (en) There is the multi-phase flowmeter in batches separated
US6212948B1 (en) Apparatus and method to obtain representative samples of oil well production
CN107083950B (en) Calibration system and calibration method based on weighing type single well metering device
CN101382556A (en) Soft measurement method for floating fine coal ash from slurry based on data drive
CN103597325A (en) Multiphase metering
CN101441099A (en) Measuring method and device of eddy flow enriched sparseness gas and solid two-phase flow capacitance chromatography imaging
CN108316912A (en) A kind of oil field individual well metering device and metering method
CN105804720A (en) Dual-body type oil-well three-phase automatic metering device
CN204352833U (en) A kind of stirring system
CN103868560B (en) Measuring method of three-phase mixed-transportation constant volume pipe piston type oil-gas-water three-phase flow meter
CN106323394A (en) Positive displacement mass flowmeter for multiphase flows
CN106988723A (en) Weight method three-phase metering mechanism and its measuring method
CN205558891U (en) Binary formula oil well three -phase automatic measurement ware
CN207335800U (en) A kind of fluidized-bed reactor solids flux measurement and effect inspection apparatus
CN101832854B (en) Unrestrained outlet laboratory table of flow characteristic of category B granule gas-solid two-phase flow
CN102410865B (en) Continuously accumulative measuring device and method for mass of solid elements in solid-liquid incompatible fluid
CN102494731A (en) Device for measuring height of bed layer of organic silicon fluidized bed
CN211008614U (en) Measuring device for three-phase flow of oil field production well produced liquid
CN206753565U (en) Multi-functional automatic skid measuring station
CN206670758U (en) Static criteria weighing device for fluid media (medium) in high-pressure sealed system
CN213775352U (en) Oil gas water precision metering device
CN201364234Y (en) Unrestraint outlet experiment table for flow characteristic of B-class granule gas-solid two-phase flow
CN206114026U (en) Heterogeneous class of mass flow meter of positive displacement type
CN102759382B (en) Device and method for measuring solid circulation flow rate
CN102384835A (en) Device for detecting flow characteristics of hydrate slurry in pipeline

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant