CN207324826U - The production system of surfactant - Google Patents
The production system of surfactant Download PDFInfo
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- CN207324826U CN207324826U CN201721318569.8U CN201721318569U CN207324826U CN 207324826 U CN207324826 U CN 207324826U CN 201721318569 U CN201721318569 U CN 201721318569U CN 207324826 U CN207324826 U CN 207324826U
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- esterification
- methyl esters
- dealcoholysis
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Abstract
The utility model discloses a kind of production system of surfactant, including pretreatment unit, ester exchange reaction device, the dealcoholysis decker being sequentially arranged；Above-mentioned pretreatment unit includes sequentially connected pre-esterification reactor kettle, pre-esterification layering tank, pre-esterification pans；Above-mentioned ester exchange reaction device includes sequentially connected transesterification reactor, the thick methyl esters settling tank of containing alcohol；Above-mentioned dealcoholysis decker includes sequentially connected thick methyl esters dealcoholysis tower, the thick methyl esters layering tank of dealcoholysis, the thick methyl esters holding vessel of dealcoholysis.The beneficial effects of the utility model are, pass through more exquisite design, so that operating personnel are produced under relatively simple operation, each technological parameter can be adjusted effectively at the same time, improve operating flexibility, on the other hand the work efficiency of each device is high, reduce human cost he, while improve general safety coefficient.
Description
Technical field
It the utility model is related to the production system of a kind of production system, especially surfactant.
Background technology
Surfactant (surfactant), referring to add can make the interface state of its solution system that obvious become occur on a small quantity
The material of change.With fixed hydrophilic lipophilic group, aligned in the surface energy of solution.The molecular structure tool of surfactant
Have amphipathic：One end is hydrophilic radical, and the other end is hydrophobic grouping；Hydrophilic radical is often polar group, such as carboxylic acid, sulfonic acid, sulphur
Acid, amino or amido and its salt, hydroxyl, amide groups, ehter bond etc. can also be used as polar hydrophilic group；And hydrophobic grouping is often non-pole
Property hydrocarbon chain, such as 8 carbon atom above hydrocarbon chains.Surfactant is divided into ionic surfactant (including cation surface activating
Agent and anion surfactant), nonionic surface active agent, amphoteric surfactant, compound surfactant, other tables
Face activating agent etc..
The equipment for producing surfactant, the equipment for especially improving the quality of production and production efficiency, lives for surface
It is particularly important that production of property agent.
Utility model content
The technical problem to be solved by the present invention is to provide a kind of production system of surfactant, there is preferable use
Effect.
The utility model is achieved through the following technical solutions.
A kind of production system of surfactant, including the pretreatment unit, ester exchange reaction device, de- being sequentially arranged
Alcohol decker；
Above-mentioned pretreatment unit includes sequentially connected pre-esterification reactor kettle, pre-esterification layering tank, pre-esterification pans；
Above-mentioned pre-esterification reactor kettle include pre-esterification reactor autoclave body, pre-esterification reactor kettle shaft, pre-esterification reactor kettle motor,
Pre-esterification reactor kettle agitating paddle, above-mentioned pre-esterification reactor kettle motor is fixed on the top of above-mentioned pre-esterification reactor autoclave body, above-mentioned pre-
Reaction kettle of the esterification shaft is assemblied in above-mentioned pre-esterification reactor kettle motor, and above-mentioned pre-esterification reactor kettle shaft set is provided with fixing sleeve
Pipe, the both ends of above-mentioned fixed sleeving are both provided with a circle flange, and above-mentioned pre-esterification reactor kettle agitating paddle is sleeved on above-mentioned fixing sleeve
Manage and the top and bottom of above-mentioned pre-esterification reactor kettle agitating paddle sets recovery spring to be connected to two flanges, above-mentioned pre-esterification
Reaction kettle body bottom is provided with pre-esterification reactor autoclave body liquid outlet, and side wall sets pre-esterification reactor kettle liquid inlet；
Above-mentioned pre-esterification layering tank includes pre-esterification layering tank body, multiple partition plates, top gate, lower part gate, above-mentioned pre-
Esterification layering tank interior is vertically arranged multiple aforementioned barriers and internal flow channel for liquids is arranged to bent, above-mentioned pre-esterification point
Layer tank body is provided with pre-esterification layering tank liquid inlet and is set in the initial segment of flow channel for liquids, above-mentioned pre-esterification layering tank body on above-mentioned
Portion's gate is set with above-mentioned lower part gate in the end of flow channel for liquids, above-mentioned pre-esterification layering tank body at above-mentioned top gate
There is concentration sensor and connect above-mentioned top gate；
Above-mentioned pre-esterification pans include tank body among pre-esterification, heated shell, resistive heater, heater, temperature and pass
Sensor, above-mentioned heated shell wraps tank body among above-mentioned pre-esterification and forms a cavity for accommodating heating liquid, above-mentioned pre-
Above-mentioned temperature sensor is provided with esterification pans body, tank base sets pre-esterification pans to enter liquid among above-mentioned pre-esterification
Mouthful, side wall sets pre-esterification pans liquid outlet, and above-mentioned heater is fixed on above-mentioned heated shell and receives above-mentioned temperature sensing
New number of device, above-mentioned resistive heater are arranged in the cavity of above-mentioned heated shell and connect above-mentioned heater；
Above-mentioned ester exchange reaction device includes sequentially connected transesterification reactor, the thick methyl esters settling tank of containing alcohol；
Above-mentioned transesterification reactor include ester exchange reaction autoclave body, transesterification reactor motor, transesterification reactor shaft,
Multiple retainer plates, multiple transesterification reactor paddles, multiple partition plates, the top and bottom difference of above-mentioned ester exchange reaction autoclave body
Transesterification reactor liquid inlet and transesterification reactor liquid outlet are provided with, above-mentioned transesterification reactor motor is fixed on above-mentioned ester
Above-mentioned transesterification reactor shaft is simultaneously assembled in the top of exchange reaction autoclave body, and above-mentioned multiple partition plates are horizontally installed on above-mentioned ester exchange
In reaction kettle body and multiple interconnected spaces are divided into, the transesterification reactor shaft positioned at each space is fixed
Above-mentioned retainer plate is set with, above-mentioned retainer plate outer surface is provided with equally distributed threaded hole, above-mentioned transesterification reactor stirring
One end of leaf is provided with and the matched screw thread bar of threaded hole；
The above-mentioned thick methyl esters settling tank of containing alcohol includes the thick methyl esters sedimentation tank body of containing alcohol, the thick methyl esters settling tank motor of containing alcohol, containing alcohol
Thick methyl esters settling tank shaft, turntable, multiple rotation axis, multiple pivoting leafs, the side wall of the above-mentioned thick methyl esters sedimentation tank body of containing alcohol are set
There are the thick methyl esters settling tank liquid inlet of containing alcohol and containing alcohol glycerine liquid inlet, bottom is provided with the thick methyl esters settling tank liquid outlet of containing alcohol,
The above-mentioned thick methyl esters settling tank motor of containing alcohol is fixed on the top of the thick methyl esters sedimentation tank body of containing alcohol, and the above-mentioned thick methyl esters settling tank of containing alcohol turns
Axis is assemblied in the thick methyl esters settling tank motor of above-mentioned containing alcohol, and above-mentioned turntable is vertically fixed on the thick methyl esters settling tank shaft of containing alcohol, multiple
Rotation axis vertically penetrates above-mentioned turntable and is uniformly arranged on the marginal position of above-mentioned turntable, and each rotation axis is both provided with multiple
Above-mentioned pivoting leaf；
Above-mentioned dealcoholysis decker includes sequentially connected thick methyl esters dealcoholysis tower, the thick methyl esters layering tank of dealcoholysis, the thick first of dealcoholysis
Ester holding vessel；
Above-mentioned thick methyl esters dealcoholysis tower includes dealcoholysis tower body, warmer, fluid reservoir, spray thrower, above-mentioned dealcoholysis tower body bottom and
Side wall is respectively arranged with dealcoholysis tower liquid inlet and dealcoholysis tower liquid outlet, and above-mentioned warmer connects above-mentioned liquid storage by tube at one end
Tank, the other end connect above-mentioned spray thrower, and above-mentioned spray thrower is located at the top in above-mentioned dealcoholysis tower body, above-mentioned spray thrower bottom connection
Multiple atomizers, above-mentioned atomizer bottom are connected with spray head；
The thick methyl esters layering tank of above-mentioned dealcoholysis include the thick methyl esters layering tank body of dealcoholysis, chamber demarcation strip, the first concentration sensor,
Second concentration sensor, the first valve, the second valve, the side wall of the above-mentioned thick methyl esters layering tank body of dealcoholysis are provided with liquid inlet, on
State and be provided with vertical above-mentioned chamber demarcation strip in dealcoholysis thick methyl esters layering tank body inside is divided into the first cavity and the second chamber
Body, above-mentioned first valve are arranged on the lower part of above-mentioned chamber demarcation strip, the first concentration sensor are provided with above-mentioned first cavity
And above-mentioned first valve is connected, and above-mentioned second valve is arranged on the lower sidewall of above-mentioned dealcoholysis thick methyl esters layering tank body, and above-mentioned the
Above-mentioned second concentration sensor is set in two cavitys and connects above-mentioned second valve, the side wall of the above-mentioned thick methyl esters layering tank body of dealcoholysis
Top is provided with the first waste liquid port and the second waste liquid port, corresponds to the first cavity and the second cavity respectively；
The above-mentioned thick methyl esters holding vessel of dealcoholysis includes the thick methyl esters storage tank body of dealcoholysis, sealing cover, the above-mentioned thick methyl esters storage of dealcoholysis
Tank wall is provided with the thick methyl esters holding vessel liquid inlet of dealcoholysis, the thick methyl esters holding vessel liquid outlet of dealcoholysis, the above-mentioned thick methyl esters storage of dealcoholysis
Deposit and circular opening is provided with the top of tank body, and the bore being open from top to bottom is gradually reduced, and above-mentioned sealing cover is opened with above-mentioned
Mouthful matching, is provided with two snatches at the top of above-mentioned sealing cover, above-mentioned snatch stretch out and end downward vertically, it is above-mentioned de-
Two sockets are provided with the top of the thick methyl esters storage tank body of alcohol to be inserted into by above-mentioned snatch, the end of above-mentioned snatch has screw thread and covers
Equipped with nut.
Further, 30 ° of -60 ° of inclinations of above-mentioned pre-esterification reactor kettle agitating paddle and horizontal plane.
Further, the side wall of above-mentioned pre-esterification layering tank body is provided with observation window.
Further, it is provided with pressure sensor in above-mentioned pre-esterification pans body.
Further, aforementioned barriers are provided with two, and the transesterification reactor that retainer plate from top to bottom is assembled
The increased number of paddle.
Further, pivoting leaf of above-mentioned rotation axis or so is arranged alternately.
Further, above-mentioned spray head is arranged to column, and side wall is evenly arranged with through hole.
Further, the thick methyl esters layering tank body of above-mentioned dealcoholysis is provided with observation window.
Further, above-mentioned sealing cover periphery is provided with a circle sealing ring.
The beneficial effects of the utility model：
The utility model passes through more exquisite design so that and operating personnel are produced under relatively simple operation,
Each technological parameter can effectively be adjusted at the same time, improve the work efficiency of operating flexibility, on the other hand each device
Height, reduce human cost he, while improve general safety coefficient.
Brief description of the drawings
Fig. 1 is the overall framework figure of the production system of surfactant；
Fig. 2 is the structure diagram of pre-esterification reactor kettle；
Fig. 3 is the structure diagram that pre-esterification is layered tank；
Fig. 4 is the structure diagram of pre-esterification pans；
Fig. 5 is the structure diagram of transesterification reactor；
Fig. 6 is the structure diagram of the thick methyl esters settling tank of containing alcohol；
Fig. 7 is the structure diagram of thick methyl esters dealcoholysis tower；
Fig. 8 is the structure diagram that the thick methyl esters of dealcoholysis is layered tank；
Fig. 9 is the structure diagram of the thick methyl esters holding vessel of dealcoholysis.
Embodiment
The utility model is described in further detail below according to drawings and examples.
With reference to Fig. 1-Fig. 9, the utility model, the production system of surfactant, including the pretreatment dress being sequentially arranged
Put, ester exchange reaction device, dealcoholysis decker；
Above-mentioned pretreatment unit includes sequentially connected pre-esterification reactor kettle 1, pre-esterification layering tank 2, pre-esterification pans
3；
Above-mentioned pre-esterification reactor kettle includes pre-esterification reactor autoclave body 1-1, pre-esterification reactor kettle shaft 1-2, pre-esterification reactor
Kettle motor 1-3, pre-esterification reactor kettle agitating paddle 1-4, above-mentioned pre-esterification reactor kettle motor 1-3 are fixed on above-mentioned pre-esterification reactor kettle
The top of body 1-1, above-mentioned pre-esterification reactor kettle shaft 1-2 are assemblied in above-mentioned pre-esterification reactor kettle motor 1-3, and above-mentioned pre-esterification is anti-
The both ends that kettle shaft 1-2 suits are provided with fixed sleeving 1-5, above-mentioned fixed sleeving 1-5 are answered to be both provided with a circle flange 1-51, on
State the top that pre-esterification reactor kettle agitating paddle 1-4 is sleeved on above-mentioned fixed sleeving 1-5 and above-mentioned pre-esterification reactor kettle agitating paddle 1-4
Portion sets recovery spring 1-52 to be connected to two flange 1-51 with bottom, and above-mentioned pre-esterification reactor autoclave body 1-1 bottoms are provided with pre-
Esterification autoclave body liquid outlet 1-6, side wall set pre-esterification reactor kettle liquid inlet 1-7.
30 ° of -60 ° of inclinations of above-mentioned pre-esterification reactor kettle agitating paddle 1-4 and horizontal plane.
Pre-esterification reactor kettle agitating paddle 1-4 is provided with inclination angle, i.e., so that pre-esterification reactor kettle agitating paddle 1-4 is in whipping process
In can float upwards, while again due to flange 1-51 and the presence for recovering spring 1-52 so that pre-esterification reactor kettle agitating paddle 1-4
Up and down reciprocatingly float within the specific limits, increase mixing area, improve the effect of pre-esterification reactor.
Above-mentioned pre-esterification layering tank 2 includes pre-esterification layering tank body 2-1, multiple partition plate 2-2, top gate 2-3, lower part lock
Door 2-4, above-mentioned pre-esterification layering tank body 2-1 inner verticals set multiple aforementioned barriers 2-2 to be arranged to internal flow channel for liquids
Bent, above-mentioned pre-esterification layering tank body 2-1 are provided with pre-esterification layering tank liquid inlet 2-5 in the initial segment of flow channel for liquids, on
State pre-esterification layering tank body 2-1 and above-mentioned top gate 2-3 and above-mentioned lower part gate 2-4 is set in the end of flow channel for liquids, it is above-mentioned
Concentration sensor 2-6 is provided with above-mentioned top gate and connects above-mentioned top gate 2-3 in pre-esterification layering tank body 2-1.
The side wall of above-mentioned pre-esterification layering tank body 2-1 is provided with observation window 2-7.
Set partition plate 2-2 that internal flow channel for liquids is arranged to bent, the flow path in tank body can be increased, improve and divide
Layer efficiency, while whether the concentration sensor 2-6 set can detect the requirement of layering and reach to open top gate 2-4.
Above-mentioned pre-esterification pans 3 include tank body 3-1 among pre-esterification, heated shell 3-2, resistive heater 3-3, heating
Device 3-4, temperature sensor 3-5, above-mentioned heated shell 3-2 wrap one receiving of tank body 3-1 and formation among above-mentioned pre-esterification
Heat the cavity of liquid, be provided with above-mentioned temperature sensor 3-5 among above-mentioned pre-esterification in tank body 3-1, among above-mentioned pre-esterification
Tank body 3-1 bottoms set pre-esterification pans liquid inlet 3-6, and side wall sets pre-esterification pans liquid outlet 3-7, above-mentioned heater
3-4 is fixed on above-mentioned heated shell 3-2 and receives new number of above-mentioned temperature sensor 3-5, and above-mentioned resistive heater 3-3 is arranged on
The cavity of above-mentioned heated shell 3-2 is interior and connects above-mentioned heater 3-4.
Among above-mentioned pre-esterification pressure sensor 3-8 is provided with tank body 3-1.
The combination of the heated shell 3-2, resistive heater 3-3, heater 3-4, temperature sensor 3-5 of setting so that temperature
When degree reduces, it can be heated automatically by system, it is ensured that the temperature requirement in pans, subsequently to carry out guarantee.
Above-mentioned ester exchange reaction device includes sequentially connected transesterification reactor 4, the thick methyl esters settling tank 5 of containing alcohol；
Above-mentioned transesterification reactor 4 includes ester exchange reaction autoclave body 4-1, transesterification reactor motor 4-2, ester exchange reaction
Kettle shaft 4-3, multiple retainer plate 4-4, multiple transesterification reactor paddle 4-5, multiple partition plate 4-6, above-mentioned ester exchange reaction
The top and bottom of autoclave body 4-1 is respectively arranged with transesterification reactor liquid inlet 4-7 and transesterification reactor liquid outlet 4-8, on
State ester exchange reaction motor 4-2 and be fixed on the top of above-mentioned ester exchange reaction autoclave body 4-1 and assemble above-mentioned transesterification reactor and turn
Axis 4-3, above-mentioned multiple partition plate 4-6 are horizontally installed in above-mentioned ester exchange reaction autoclave body 4-1 and are divided into multiple phases interconnection
Logical space, the equal fixing sleeves of transesterification reactor shaft 4-3 positioned at each space are equipped with above-mentioned retainer plate 4-4, above-mentioned fixation
Circle 4-4 outer surfaces are provided with equally distributed threaded hole, and one end of above-mentioned transesterification reactor paddle 4-5 is provided with and screw thread
The matched screw thread bar in hole.
Aforementioned barriers 4-6 is provided with two, and the transesterification reactor stirring that retainer plate 4-4 from top to bottom is assembled
The increased number of leaf 4-5.
Space is divided into multiple by the partition plate 4-6 of setting, can carry out continuous ester exchange reaction, while the retainer plate 4- set
4 and assembling transesterification reactor paddle 4-5 can carry out transesterification reactor paddle 4-5's as the case may be
Arrangement, improves using flexible.
The above-mentioned thick methyl esters settling tank 5 of containing alcohol includes the thick methyl esters sedimentation tank body 5-1 of containing alcohol, the thick methyl esters settling tank motor 5- of containing alcohol
2nd, the thick methyl esters settling tank shaft 5-3 of containing alcohol, turntable 5-4, multiple rotation axis 5-5, multiple pivoting leaf 5-6, the above-mentioned thick methyl esters of containing alcohol
The side wall of sedimentation tank body 5-1 is provided with the thick methyl esters settling tank liquid inlet 5-7 of containing alcohol and containing alcohol glycerine liquid inlet 5-8, and bottom is set
It is equipped with containing alcohol thick methyl esters settling tank liquid outlet 5-9, the above-mentioned thick methyl esters settling tank motor 5-2 of containing alcohol and is fixed on the thick methyl esters sedimentation of containing alcohol
The top of tank body 5-1, the above-mentioned thick methyl esters settling tank shaft 5-3 of containing alcohol are assemblied in the thick methyl esters settling tank motor 5-2 of above-mentioned containing alcohol, on
State turntable 5-4 and be vertically fixed on containing alcohol thick methyl esters settling tank shaft 5-3, multiple rotation axis 5-5 and vertically penetrate above-mentioned turntable 5-4 simultaneously
And the marginal position of above-mentioned turntable 5-4 is uniformly arranged on, each rotation axis 5-5 is both provided with multiple above-mentioned pivoting leaf 5-6.
Pivoting leaf 5-6 of above-mentioned rotation axis or so is arranged alternately.
By setting turntable 5-4 and multiple rotation axis 5-5, it is possible to increase stirring efficiency, improves the sedimentation effect of settling tank
Fruit.
Above-mentioned dealcoholysis decker includes sequentially connected thick methyl esters dealcoholysis tower 6, the thick methyl esters of dealcoholysis is layered tank 7, dealcoholysis is thick
Methyl esters holding vessel 8；
Above-mentioned thick methyl esters dealcoholysis tower 6 includes dealcoholysis tower body 6-1, warmer 6-2, fluid reservoir 6-3, spray thrower 6-4, above-mentioned de-
Alcohol tower body 6-1 bottoms and side wall are respectively arranged with dealcoholysis tower liquid inlet 6-5 and dealcoholysis tower liquid outlet 6-6, and above-mentioned warmer 6-2 leads to
Cross tube at one end and connect above-mentioned fluid reservoir 6-3, the other end connects above-mentioned spray thrower 6-4, and above-mentioned spray thrower 6-4 is located at above-mentioned dealcoholysis
Top in tower body 6-1, above-mentioned spray thrower 6-1 bottoms connect multiple atomizer 6-7, and above-mentioned atomizer 6-7 bottoms connection is set
There is spray head 6-8.
Above-mentioned spray head 6-8 is arranged to column, and side wall is evenly arranged with through hole.
Spray thrower 6-4 is set and carries multiple atomizer 6-7 and spray head 6-8, spray area is improved, improves de-
Alcohol efficiency.
The above-mentioned thick methyl esters layering tank 7 of dealcoholysis includes the thick methyl esters layering tank body 7-1 of dealcoholysis, chamber demarcation strip 7-2, the first concentration
Sensor 7-3, the second concentration sensor 7-4, the first valve 7-5, the second valve 7-6, the above-mentioned thick methyl esters layering tank body 7-1 of dealcoholysis
Side wall be provided with liquid inlet 7-8, is provided with vertical above-mentioned chamber demarcation strip 7- in the above-mentioned thick methyl esters layering tank body 7-1 of dealcoholysis
Inside is divided into the first cavity and the second cavity by 2, and above-mentioned first valve 7-5 is arranged on the lower part of above-mentioned chamber demarcation strip 7-2,
The first concentration sensor 7-3 is provided with above-mentioned first cavity and connects above-mentioned first valve 7-5, above-mentioned second valve 7-6 is set
The lower sidewall in the thick methyl esters layering tank body 7-1 of above-mentioned dealcoholysis is put, above-mentioned second concentration sensor is set in above-mentioned second cavity
7-4 simultaneously connects above-mentioned second valve 7-6, and the side wall upper part of the above-mentioned thick methyl esters layering tank body 7-1 of dealcoholysis is provided with the first waste liquid port
7-11 and the second waste liquid port 7-12, corresponds to the first cavity and the second cavity respectively.
The above-mentioned thick methyl esters layering tank body 7-1 of dealcoholysis is provided with observation window 7-13.
Set chamber demarcation strip 7-2 that inside is divided into the first cavity and the second cavity, that is, be divided into a stage layered and two
Stage layered, and valve is opened by sensor and carries out procedure connection, that is, the effect of layering is improved, while also ensure that layering
Quality.
The above-mentioned thick methyl esters holding vessel 8 of dealcoholysis includes the thick methyl esters storage tank body 8-1 of dealcoholysis, sealing cover 8-2, the above-mentioned thick first of dealcoholysis
Ester storage tank body 8-1 side walls are provided with the thick methyl esters holding vessel liquid inlet 8-6 of dealcoholysis, the thick methyl esters holding vessel liquid outlet 8-7 of dealcoholysis, on
State and be provided with circular opening at the top of the thick methyl esters storage tank body 8-1 of dealcoholysis, and the bore being open from top to bottom is gradually reduced, on
Sealing cover 8-2 is stated to match with above-mentioned opening, be provided with the top of above-mentioned sealing cover 8-2 two snatches 8-3, above-mentioned snatch 8-3 to
Outer extension and end is downward vertically, two sockets are provided with by above-mentioned snatch at the top of the thick methyl esters storage tank body 8-1 of above-mentioned dealcoholysis
8-3 is inserted into, and the end of above-mentioned snatch 8-3 has screw thread and is set with nut 8-4.
Above-mentioned sealing cover 8-2 peripheries are provided with a circle sealing ring 8-5.
It by setting sealing cover 8-2 and relevant snatch 8-3, that is, can ensure that leakproofness, while be easy to opening and closing operations again,
The maintenance and cleaning in tank is facilitated to work, practicality is higher.
Above-described embodiment is only the technical concepts and features for illustrating the utility model, and its object is to allow be familiar with this field skill
The personage of art can understand the utility model content and be carried out, and can not limit the scope of protection of the utility model with this.
All equivalent change or modifications made according to the utility model Spirit Essence, should all cover in the scope of protection of the utility model
It is interior.
Claims (9)
1. a kind of production system of surfactant, it is characterised in that anti-including the pretreatment unit that is sequentially arranged, ester exchange
Answer device, dealcoholysis decker；
The pretreatment unit includes sequentially connected pre-esterification reactor kettle, pre-esterification layering tank, pre-esterification pans；
The pre-esterification reactor kettle includes pre-esterification reactor autoclave body, pre-esterification reactor kettle shaft, pre-esterification reactor kettle motor, pre- ester
Change reaction kettle agitating paddle, the pre-esterification reactor kettle motor is fixed on the top of the pre-esterification reactor autoclave body, the pre-esterification
Reaction kettle shaft is assemblied in the pre-esterification reactor kettle motor, and the pre-esterification reactor kettle shaft set is provided with fixed sleeving,
The both ends of the fixed sleeving are both provided with a circle flange, and the pre-esterification reactor kettle agitating paddle is sleeved on the fixed sleeving simultaneously
And the top and bottom of the pre-esterification reactor kettle agitating paddle sets recovery spring to be connected to two flanges, the pre-esterification reactor
Autoclave body bottom is provided with pre-esterification reactor autoclave body liquid outlet, and side wall sets pre-esterification reactor kettle liquid inlet；
The pre-esterification layering tank includes pre-esterification layering tank body, multiple partition plates, top gate, lower part gate, the pre-esterification
Layering tank interior is vertically arranged multiple partition plates and internal flow channel for liquids is arranged to bent, and the pre-esterification is layered tank
Body is provided with pre-esterification layering tank liquid inlet and sets the top lock in the initial segment of flow channel for liquids, the pre-esterification layering tank body
Door is dense in being provided with the end of flow channel for liquids, the pre-esterification layering tank body at the top gate with the lower part gate
Degree sensor simultaneously connects the top gate；
The pre-esterification pans include tank body, heated shell, resistive heater, heater, temperature sensor among pre-esterification,
The heated shell wraps tank body among the pre-esterification and forms a cavity for accommodating heating liquid, in the pre-esterification
Between the temperature sensor is provided with tank body, tank base sets pre-esterification pans liquid inlet, side among the pre-esterification
Wall sets pre-esterification pans liquid outlet, and the heater is fixed on the heated shell and receives the new of the temperature sensor
Number, the resistive heater is arranged in the cavity of the heated shell and connects the heater；
The ester exchange reaction device includes sequentially connected transesterification reactor, the thick methyl esters settling tank of containing alcohol；
The transesterification reactor includes ester exchange reaction autoclave body, transesterification reactor motor, transesterification reactor shaft, multiple
Retainer plate, multiple transesterification reactor paddles, multiple partition plates, the top and bottom of the ester exchange reaction autoclave body are set respectively
There are transesterification reactor liquid inlet and transesterification reactor liquid outlet, the transesterification reactor motor is fixed on the ester exchange
The transesterification reactor shaft is simultaneously assembled in the top of reaction kettle body, and the multiple partition plate is horizontally installed on the ester exchange reaction
In autoclave body and multiple interconnected spaces are divided into, the fixed suit of transesterification reactor shaft positioned at each space
There is the retainer plate, the retainer plate outer surface is provided with equally distributed threaded hole, the transesterification reactor paddle
One end is provided with and the matched screw thread bar of threaded hole；
The thick methyl esters settling tank of containing alcohol includes the thick methyl esters sedimentation tank body of containing alcohol, the thick methyl esters settling tank motor of containing alcohol, the thick first of containing alcohol
Ester settling tank shaft, turntable, multiple rotation axis, multiple pivoting leafs, the side wall of the thick methyl esters sedimentation tank body of containing alcohol, which is provided with, to be contained
The thick methyl esters settling tank liquid inlet of alcohol and containing alcohol glycerine liquid inlet, bottom is provided with the thick methyl esters settling tank liquid outlet of containing alcohol, described
The thick methyl esters settling tank motor of containing alcohol is fixed on the top of the thick methyl esters sedimentation tank body of containing alcohol, the thick methyl esters settling tank shaft dress of containing alcohol
The thick methyl esters settling tank motor of the containing alcohol is fitted over, the turntable is vertically fixed on the thick methyl esters settling tank shaft of containing alcohol, multiple rotations
Axis vertically penetrates the turntable and is uniformly arranged on the marginal position of the turntable, and each rotation axis is both provided with multiple described
Pivoting leaf；
The dealcoholysis decker includes sequentially connected thick methyl esters dealcoholysis tower, the thick methyl esters layering tank of dealcoholysis, the thick methyl esters storage of dealcoholysis
Deposit tank；
The thick methyl esters dealcoholysis tower includes dealcoholysis tower body, warmer, fluid reservoir, spray thrower, the dealcoholysis tower body bottom and side wall
Dealcoholysis tower liquid inlet and dealcoholysis tower liquid outlet are respectively arranged with, the warmer connects the fluid reservoir by tube at one end, separately
One end connects the spray thrower, and the spray thrower is located at the top in the dealcoholysis tower body, and the spray thrower bottom connection is multiple
Atomizer, the atomizer bottom are connected with spray head；
The thick methyl esters layering tank of dealcoholysis includes the thick methyl esters layering tank body of dealcoholysis, chamber demarcation strip, the first concentration sensor, second
Concentration sensor, the first valve, the second valve, the side wall of the thick methyl esters layering tank body of dealcoholysis is provided with liquid inlet, described de-
The vertical chamber demarcation strip is provided with the thick methyl esters layering tank body of alcohol, and inside is divided into the first cavity and the second cavity, institute
The lower part that the first valve is arranged on the chamber demarcation strip is stated, the first concentration sensor is provided with first cavity and connects
First valve, second valve are arranged on the lower sidewall of the thick methyl esters layering tank body of the dealcoholysis, second cavity
Interior to set second concentration sensor and connect second valve, the side wall upper part of the thick methyl esters layering tank body of dealcoholysis is set
The first waste liquid port and the second waste liquid port are equipped with, corresponds to the first cavity and the second cavity respectively；
The thick methyl esters holding vessel of dealcoholysis includes the thick methyl esters storage tank body of dealcoholysis, sealing cover, the thick methyl esters storage tank body of dealcoholysis
Side wall is provided with the thick methyl esters holding vessel liquid inlet of dealcoholysis, the thick methyl esters holding vessel liquid outlet of dealcoholysis, the thick methyl esters holding vessel of dealcoholysis
Circular opening is provided with the top of body, and the bore being open from top to bottom is gradually reduced, the sealing cover and the opening
Match somebody with somebody, be provided with two snatches at the top of the sealing cover, the snatch stretch out and end downward vertically, the dealcoholysis is thick
Two sockets are provided with the top of methyl esters storage tank body to be inserted into by the snatch, the end of the snatch has screw thread and is set with
Nut.
2. the production system of surfactant according to claim 1, it is characterised in that the pre-esterification reactor kettle stirring
30 ° of -60 ° of inclinations of paddle and horizontal plane.
3. the production system of surfactant according to claim 1, it is characterised in that the pre-esterification layering tank body
Side wall is provided with observation window.
4. the production system of surfactant according to claim 1, it is characterised in that in the pre-esterification pans body
It is provided with pressure sensor.
5. the production system of surfactant according to claim 1, it is characterised in that the partition plate is provided with two,
And the increased number for the transesterification reactor paddle that retainer plate from top to bottom is assembled.
6. the production system of surfactant according to claim 1, it is characterised in that the pivoting leaf of the rotation axis is left
The right side is arranged alternately.
7. the production system of surfactant according to claim 1, it is characterised in that the spray head is arranged to column
Shape, and side wall is evenly arranged with through hole.
8. the production system of surfactant according to claim 1, it is characterised in that the thick methyl esters layering tank of dealcoholysis
Body is provided with observation window.
9. the production system of surfactant according to claim 1, it is characterised in that the sealing cover periphery is provided with
One circle sealing ring.
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| CN201721318569.8U CN207324826U (en) | 2017-10-13 | 2017-10-13 | The production system of surfactant |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107597042A (en) * | 2017-10-13 | 2018-01-19 | 安徽天意环保科技有限公司 | The production system of surfactant |
| CN110449106A (en) * | 2019-09-06 | 2019-11-15 | 铜仁学院 | A kind of highly effective continuous reaction unit of amino acid surfactant |
-
2017
- 2017-10-13 CN CN201721318569.8U patent/CN207324826U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107597042A (en) * | 2017-10-13 | 2018-01-19 | 安徽天意环保科技有限公司 | The production system of surfactant |
| CN110449106A (en) * | 2019-09-06 | 2019-11-15 | 铜仁学院 | A kind of highly effective continuous reaction unit of amino acid surfactant |
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