CN207324788U - A kind of polymeric kettle for being used to produce carboxylic styrene butadiene latex - Google Patents

A kind of polymeric kettle for being used to produce carboxylic styrene butadiene latex Download PDF

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Publication number
CN207324788U
CN207324788U CN201720775576.4U CN201720775576U CN207324788U CN 207324788 U CN207324788 U CN 207324788U CN 201720775576 U CN201720775576 U CN 201720775576U CN 207324788 U CN207324788 U CN 207324788U
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CN
China
Prior art keywords
autoclave body
water
styrene butadiene
butadiene latex
rotor
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Expired - Fee Related
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CN201720775576.4U
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Chinese (zh)
Inventor
高兴
耿学锋
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Xiangyang Fuyuan Prosperity Technology Co Ltd
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Xiangyang Fuyuan Prosperity Technology Co Ltd
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Priority to CN201720775576.4U priority Critical patent/CN207324788U/en
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Abstract

The utility model embodiment discloses a kind of polymeric kettle for being used to produce carboxylic styrene butadiene latex, including autoclave body;Mixing component, including motor and agitating shaft, the one end of agitating shaft away from motor are stretched into autoclave body, are provided with rotor thereon, and the both sides and bottom of rotor are both provided with bristle;Sample and manage, including the high sampling pipe that bottom is interconnected is managed with low sample, the top of height sampling pipe is connected with autoclave body side wall upper part, and the low top for sampling pipe is connected with autoclave body lower sidewall;Outer cooling system, including water tank, water pump, lower water pond and the water-filling chuck for being wrapped in the setting of autoclave body outer wall of circulating water pipe connection are passed sequentially through, the bottom of water-filling chuck is connected by circulating water pipe with water tank.The utility model sets rotor bristle for producing in the polymeric kettle of carboxylic styrene butadiene latex, it can prevent that raw material is adhered on inner wall of kettle during polymerization, the outer cooling system of peripheral hardware can fast and effective cooling autoclave body, directly sampled during reaction by sampling box, it is accurate, quick and conveniently.

Description

A kind of polymeric kettle for being used to produce carboxylic styrene butadiene latex
Technical field
A kind of polymerization reaction kettle of chemical industry production is the utility model is related to, more particularly to it is a kind of for producing carboxyl The polymeric kettle of styrene-butadiene latex.
Background technology
Carboxylic styrene butadiene latex, is to add a small amount of carboxylic acid and other auxiliary agents with butadiene, styrene, is generated by emulsion polymerization Copolymer, is a kind of milky aqueous dispersion with bluish violet gloss.Carboxylic styrene butadiene latex is coated with for paper and cardboard Complete series latex needed for industry, suitable for decorating base paper, abrasion-proof paper, medium-to-high grade art paper, white board, paperboard, boxboard etc. Face, primary coat cloth and bonding.
, it is necessary to which the raw material of oil phase and water phase is disposably added to polymeric kettle in the production process of carboxylic styrene butadiene latex In, it is stirred at a certain temperature, then cooling down, the stirring of polymeric kettle is uneven, and cooling can not influence rapidly to produce Quality and production efficiency, in the course of the polymerization process, it is also necessary to detection is sampled to mixed liquor, is usually sampled in a point, As a result it is inaccurate, it can also influence product quality.
Utility model content
The technical problem to be solved by the embodiment of the utility model is, for the production process in carboxylic styrene butadiene latex In, the stirring of polymeric kettle is uneven, and cooling can not influence rapidly product quality and production efficiency, and samples detection, usually The problem of being sampled in a point, as a result inaccuracy, also influencing product quality, it is proposed that one kind is used to produce carboxylic styrene butadiene latex Polymeric kettle.
In order to solve the above-mentioned technical problem, the utility model embodiment provides a kind of for producing carboxylic styrene butadiene latex Polymeric kettle, the polymeric kettle for being used to produce carboxylic styrene butadiene latex include:Autoclave body, its top and bottom be respectively arranged with feed inlet and Discharge port;Mixing component, including motor and the agitating shaft that is connected with motor, motor are arranged at the top of autoclave body, and agitating shaft is away from electricity One end of machine is stretched into autoclave body, is provided with rotor thereon, and the both sides and bottom of rotor are both provided with bristle, bristle and autoclave body it is interior Wall contact is set;Sample and manage, including the high sampling pipe that bottom is interconnected is managed with low sample, the top and autoclave body side of height sampling pipe Wall top connects, and is provided with the first valve and the first form, and the top of low sampling pipe is connected with autoclave body lower sidewall, thereon The second valve and the second form are provided with, height sampling pipe is inserted into sampling box with one end that low sampling pipe connects;Outer cooling system, Water tank, water pump, lower water pond and the water-filling chuck for being wrapped in the setting of autoclave body outer wall including passing sequentially through circulating water pipe connection, under Water pond is sheathed at the top of autoclave body, its bottom shelf is arranged on the top of water-filling chuck, offers multiple drainage holes thereon, water-filling chuck Bottom is connected by circulating water pipe with water tank.
Wherein, rotor is rectangle, and the one end of agitating shaft away from motor is inserted into rotor and fixed.
Wherein, the both sides of rotor and bottom are both provided with folder, and bristle is installed in folder.
Wherein, water inlet pipe is connected with water tank, water inlet pipe is connected with water source.
Wherein, electric heating system is installed on autoclave body, electric heating system includes electric heating tube, temperature measurer and thermostat, Electric heating tube and temperature measurer are installed in autoclave body, and thermostat is installed on outside autoclave body, temperature and feedback in temperature measurer measurement autoclave body To thermostat, thermostat is used for the temperature for adjusting electric heating tube.
Implement the utility model embodiment, have the advantages that:The utility model be used for produce carboxy styrene-butadiene rubber Rotor bristle is set in the polymeric kettle of breast, can prevent that raw material is adhered on inner wall of kettle during polymerization, the outer cooling system of peripheral hardware can be quick Effectively cooling autoclave body, when reaction, are directly sampled by sampling box, accurate, quick and conveniently.
Brief description of the drawings
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, drawings in the following description are only It is some embodiments of the utility model, for those of ordinary skill in the art, in the premise not made the creative labor Under, other attached drawings can also be obtained according to these attached drawings.
Fig. 1 is the structure diagram of the polymeric kettle provided by the utility model for being used to produce carboxylic styrene butadiene latex.
Embodiment
The following is a combination of the drawings in the embodiments of the present utility model, and the technical scheme in the embodiment of the utility model is carried out Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are without making creative work All other embodiments obtained, shall fall within the protection scope of the present invention.
The utility model provides a kind of polymeric kettle for being used to produce carboxylic styrene butadiene latex, refers to Fig. 1, Fig. 1 is this reality With the structure diagram for being used to produce the polymeric kettle of carboxylic styrene butadiene latex of new offer.This is used to produce carboxylic styrene butadiene latex Polymeric kettle includes:Autoclave body 10, feed inlet 11, discharge port 12, mixing component 20, motor 21, agitating shaft 22, rotor 23, bristle 24, Folder 25, sampling pipe 30, high sampling pipe 31, low sampling pipe 32, the first valve 33, the first form 34, the second valve 35, second regard Window 36, sampling box 37, outer cooling system 40, circulating water pipe 41, water tank 42, water pump 43, lower water pond 44, water-filling chuck 45 and into Water pipe 46.
The top and bottom of autoclave body 10 are respectively arranged with feed inlet 11 and discharge port 12.
Mixing component 20 includes motor 21 and the agitating shaft 22 being connected with motor 21, and motor 21 is arranged at the top of autoclave body 10, The one end of agitating shaft 22 away from motor 21 is stretched into autoclave body 10, is provided with rotor 23 thereon, and rotor 23 is rectangle, agitating shaft 22 In one end insertion rotor 23 away from motor 21 and fixed, the both sides and bottom of rotor 23 are both provided with folder 25, and bristle 24 is pacified Loaded in folder 25, bristle 24 contacts setting with the inner wall of autoclave body 10.
Sampling pipe 30 includes high sampling pipe 31 and the low sampling pipe 32 that bottom is interconnected, the top of height sampling pipe 31 and kettle 10 side wall upper part of body connects, and is provided with the first valve 33 and the first form 34, the top and 10 side of autoclave body of low sampling pipe 32 Wall lower part connects, and is provided with the second valve 35 and the second form 36, one end that height sampling pipe 31 is connected with low sampling pipe 32 It is inserted into sampling box 37.
Outer cooling system 40 includes passing sequentially through the water tank 42 of the connection of circulating water pipe 41, water pump 43, lower water pond 44 and bag The water-filling chuck 45 of 10 outer wall of autoclave body setting is wrapped in, lower water pond 44 is sheathed on the top of autoclave body 10, its bottom shelf is arranged on water-filling chuck 45 top, offers multiple drainage holes (not shown) thereon, and the bottom of water-filling chuck 45 passes through circulating water pipe 41 and water tank 42 Connection.Water inlet pipe 46 is connected with water tank 42, water inlet pipe 46 is connected with water source.
Electric heating system (not shown) is installed, electric heating system includes electric heating tube, temperature measurer and control on autoclave body 10 Warm device, electric heating tube and temperature measurer are installed in autoclave body, and thermostat is installed on outside autoclave body, and the temperature in temperature measurer measurement autoclave body is simultaneously Thermostat is fed back to, thermostat is used for the temperature for adjusting electric heating tube.
When the raw material to oil phase and water phase polymerize, first raw material is disposably all poured into autoclave body 10, opens electricity Heating system, opens mixing component 20, rotates rotor 23, with the rotation of rotor 23, bristle 24 can brush off 10 inner wall of autoclave body On raw material;After specified time is stirred to, analysis is sampled, i.e., successively opens the first valve 33 and the second valve 35, and The liquid outlet quantity from the first form 34 and the second form 36 respectively, extracts the sample liquid on upper strata in autoclave body 10 in high pipe 31 of sampling, The sample liquid of lower floor in autoclave body 10 is taken in low sampling pipe 32, when all up to standard, closes electric heating system, the outer cooling system of unlatching System, cools down autoclave body.
Implement the utility model embodiment, have the advantages that:The utility model be used for produce carboxy styrene-butadiene rubber Rotor bristle is set in the polymeric kettle of breast, can prevent that raw material is adhered on inner wall of kettle during polymerization, the outer cooling system of peripheral hardware can be quick Effectively cooling autoclave body, when reaction, are directly sampled by sampling box, accurate, quick and conveniently.
The above is only the preferred embodiment of the utility model only, is not intended to limit the utility model, all at this Within the spirit and principle of utility model, any modification, equivalent replacement, improvement and so on, should be included in the utility model Protection domain within.

Claims (5)

1. a kind of polymeric kettle for being used to produce carboxylic styrene butadiene latex, it is characterised in that described to be used to produce carboxylic styrene butadiene latex Polymeric kettle includes:
Autoclave body, its top and bottom are respectively arranged with inlet port and outlet port;
Mixing component, including motor and the agitating shaft that is connected with the motor, the motor is arranged at the top of the autoclave body, described The one end of agitating shaft away from the motor is stretched into the autoclave body, is provided with rotor thereon, and the both sides and bottom of the rotor are equal Bristle is provided with, the bristle contacts setting with the inner wall of the autoclave body;
Sampling pipe, including the height sampling pipe and low sampling pipe, the top of the high sampling pipe and the autoclave body that bottom is interconnected Side wall upper part connects, and is provided with the first valve and the first form, the top of the low sampling pipe with the autoclave body side wall Portion connects, and is provided with the second valve and the second form, one end insertion that the high sampling pipe is connected with the low sampling pipe In sampling box;
Outer cooling system, including pass sequentially through the water tank of circulating water pipe connection, water pump, lower water pond and be wrapped in outside the autoclave body The water-filling chuck that wall is set, the lower water pond are sheathed at the top of the autoclave body, its bottom shelf is arranged on the top of the water-filling chuck, Multiple drainage holes are offered thereon, and the bottom of the water-filling chuck is connected by the circulating water pipe with the water tank.
2. the polymeric kettle according to claim 1 for being used to produce carboxylic styrene butadiene latex, it is characterised in that the rotor is length Square, the one end of the agitating shaft away from the motor is inserted into the rotor and fixed.
3. the polymeric kettle according to claim 2 for being used to produce carboxylic styrene butadiene latex, it is characterised in that the two of the rotor Side and bottom are both provided with folder, and the bristle is installed in the folder.
4. the polymeric kettle according to claim 1 for being used to produce carboxylic styrene butadiene latex, it is characterised in that connect on the water tank Water inlet pipe is connected to, the water inlet pipe is connected with water source.
5. the polymeric kettle according to claim 1 for being used to produce carboxylic styrene butadiene latex, it is characterised in that pacify on the autoclave body Equipped with electric heating system, the electric heating system includes electric heating tube, temperature measurer and thermostat, the electric heating tube and described Temperature measurer is installed in the autoclave body, and the thermostat is installed on outside the autoclave body, and the temperature measurer is measured in the autoclave body Temperature simultaneously feeds back to the thermostat, and the thermostat is used for the temperature for adjusting the electric heating tube.
CN201720775576.4U 2017-06-29 2017-06-29 A kind of polymeric kettle for being used to produce carboxylic styrene butadiene latex Expired - Fee Related CN207324788U (en)

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CN201720775576.4U CN207324788U (en) 2017-06-29 2017-06-29 A kind of polymeric kettle for being used to produce carboxylic styrene butadiene latex

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Application Number Priority Date Filing Date Title
CN201720775576.4U CN207324788U (en) 2017-06-29 2017-06-29 A kind of polymeric kettle for being used to produce carboxylic styrene butadiene latex

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112965338A (en) * 2021-02-01 2021-06-15 深圳市德贝尔光电材料有限公司 Special epoxy acrylic resin composition for LDI photoresist and preparation method thereof
CN114100557A (en) * 2021-12-14 2022-03-01 枣阳市军合胜塑化科技有限公司 Polymerization facility is used in butyronitrile latex production

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112965338A (en) * 2021-02-01 2021-06-15 深圳市德贝尔光电材料有限公司 Special epoxy acrylic resin composition for LDI photoresist and preparation method thereof
CN112965338B (en) * 2021-02-01 2021-10-08 深圳市德贝尔光电材料有限公司 Special epoxy acrylic resin composition for LDI photoresist and preparation method thereof
CN114100557A (en) * 2021-12-14 2022-03-01 枣阳市军合胜塑化科技有限公司 Polymerization facility is used in butyronitrile latex production

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Granted publication date: 20180508

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