CN207287120U - A kind of material recycling device of triphenylchloromethane production - Google Patents

A kind of material recycling device of triphenylchloromethane production Download PDF

Info

Publication number
CN207287120U
CN207287120U CN201721338300.6U CN201721338300U CN207287120U CN 207287120 U CN207287120 U CN 207287120U CN 201721338300 U CN201721338300 U CN 201721338300U CN 207287120 U CN207287120 U CN 207287120U
Authority
CN
China
Prior art keywords
induction chamber
reative cell
level sensor
triphenylchloromethane
feeding box
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201721338300.6U
Other languages
Chinese (zh)
Inventor
余毅
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangxi Yuankang Silicon Industry Technology Co Ltd
Original Assignee
Jiangxi Yuankang Silicon Industry Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangxi Yuankang Silicon Industry Technology Co Ltd filed Critical Jiangxi Yuankang Silicon Industry Technology Co Ltd
Priority to CN201721338300.6U priority Critical patent/CN207287120U/en
Application granted granted Critical
Publication of CN207287120U publication Critical patent/CN207287120U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The utility model provides a kind of material recycling device of triphenylchloromethane production, including babinet, and reative cell, induction chamber are divided into babinet and supplies hot cell between reative cell and induction chamber；The first feeding box and the second feeding box are equipped with above reative cell, is additionally provided with rabble in reative cell, rabble is driven by motor；Heater is equipped with for hot cell bottom, the heat-generating pipe of heater is located in heat supply room；The 3rd feeding box and wind turbine are equipped with above induction chamber；The gas outlet of wind turbine is connected by air outlet pipe with induction chamber, and the air inlet of wind turbine is connected by the first air inlet pipe with extraneous reaction kettle；Reative cell side wall is equipped with the first liquid level sensor, level sensor and temperature sensor；Induction chamber side wall is equipped with the second liquid level sensor and pH sensor；It can distinguish solid, gaseous waste processing recycling, enhance the standard of waste to property so that recycling is more thorough, substantially increases the rate of recovery of waste material.

Description

A kind of material recycling device of triphenylchloromethane production
Technical field
Technical field of pharmaceutical chemistry is the utility model is related to, more particularly to a kind of triphenylchloromethane production Material recycling device.
Background technology
In existing technology, the chemical synthesis process of triphenylchloromethane mainly with triphenylcarbinol and thionyl chloride, Chloroacetic chloride or hydrogen chloride gas chloro are prepared, this technique there is also it is larger the drawbacks of, main cause be thionyl chloride production Contain a large amount of sulfur dioxide in raw tail gas, and one of six indexs that sulfur dioxide, which is national environmental protection, strictly controls air, Processing is difficult, poisons greatly, and many unnecessary materials can be produced in the production process of triphenylchloromethane, if being exhausted directly to The external world will cause serious pollution, and the resource containing substantial amounts of recoverable is also wasted in waste, is unfavorable for Production, the life of today's society require；Therefore, it is badly in need of a kind of device that rapid efficient can be carried out to material.
Utility model content
The defects of in order to overcome the prior art, problem to be solved in the utility model are to propose a kind of triphenyl chloromethane The material recycling device of alkane production, it can give up the solid waste and gas produced in the production process of triphenylchloromethane Material distinguishes processing recycling, enhances the standard of waste to property so that recycling is more thorough, substantially increases the recycling of waste material Rate；And automated control is realized to the whole process of waste disposal, staff is reduced and is contacted with the direct of discarded object, protected Hinder employee's health.
For this purpose, the utility model uses following technical scheme：
The utility model provides a kind of material recycling device of triphenylchloromethane production, including babinet, the case Two pieces of partition plates being oppositely arranged are equipped with vivo, the babinet is divided into reative cell, for hot cell, induction chamber, institute by two pieces of partition plates State for hot cell between the reative cell and the induction chamber；The first feeding box and the second feed are equipped with above the reative cell Bucket, first feeding box and second feeding box are connected by the first pipeline and second pipe with the reative cell respectively, And first pipeline is equipped with the first solenoid valve, the second pipe is equipped with second solenoid valve, is also set in the reative cell There is rabble, the rabble is driven by motor；Described to be equipped with heater for hot cell bottom, the heat-generating pipe of the heater is located at In the heat supply room；Be equipped with the 3rd feeding box and wind turbine above the induction chamber, the 3rd feeding box by the 3rd pipeline and The induction chamber connection, and the 3rd pipeline is equipped with the 3rd solenoid valve；The gas outlet of the wind turbine passes through air outlet pipe and institute Induction chamber connection is stated, the air inlet of the wind turbine is connected by the first air inlet pipe with extraneous reaction kettle；On the reative cell side wall Equipped with the first liquid level sensor, level sensor and temperature sensor；The induction chamber side wall is equipped with the second level sensing Device and pH sensor；First liquid level sensor, the level sensor, the temperature sensor；Second liquid level Sensor, the pH sensor, first solenoid valve, the second solenoid valve, the 3rd solenoid valve, the fever Device, the motor and the wind turbine are electrically connected with controller.
In the utility model preferably technical solution, first liquid level sensor is located at the upper of the level sensor Side.
In the utility model preferably technical solution, the rabble is equipped with polylith paddle, and the paddle It is equipped with through hole.
In the utility model preferably technical solution, the second air inlet pipe, second air inlet are additionally provided with the wind turbine Pipe one end is connected with the air inlet of the wind turbine, and the other end is connected with the reative cell.
In the utility model preferably technical solution, first air inlet pipe is hose, and its free end is equipped with pipe Connector.
In the utility model preferably technical solution, the air-breathing indoor storage air-breathing solvent, the end of the air outlet pipe End is located in the air-breathing solvent.
In the utility model preferably technical solution, the air outlet pipe is equipped with check valve.
In the utility model preferably technical solution, the air-breathing chamber upper wall is equipped with relief valve.
The beneficial effects of the utility model are：
A kind of material recycling device of triphenylchloromethane production provided by the utility model, it utilizes reative cell and suction The solid waste produced in the production process of triphenylchloromethane and gaseous waste are distinguished processing recycling by gas chamber respectively, The standard of waste is enhanced to property so that recycling is more thorough, substantially increases the rate of recovery of waste material；And reative cell and induction chamber Between suitable reaction temperature can be provided for hot cell, accelerate infiltration rate, improve production efficiency；And to the whole of waste disposal A process realizes automated control, reduces staff and is contacted with the direct of discarded object, ensures employee's health.
Brief description of the drawings
Fig. 1 is the knot of the material recycling device for the triphenylchloromethane production that the utility model embodiment provides Structure schematic diagram.
In figure：
1st, babinet；11st, reative cell；111st, the first liquid level sensor；112nd, level sensor；113rd, temperature sensor；12、 For hot cell；121st, heater；122nd, heat-generating pipe；13rd, induction chamber；131st, the second liquid level sensor；132nd, pH sensor；133、 Relief valve；21st, the first feeding box；211st, the first pipeline；212nd, the first solenoid valve；22nd, the second feeding box；221st, second pipe； 222nd, second solenoid valve；23rd, the 3rd feeding box；231st, the 3rd pipeline；232nd, the 3rd solenoid valve；3rd, motor；31st, rabble； 311st, paddle；312nd, through hole；4th, wind turbine；41st, air outlet pipe；411st, check valve；42nd, the first air inlet pipe；421st, pipe fitting；43、 Second air inlet pipe；5th, controller；6th, extraneous reaction kettle.
Embodiment
Further illustrate the technical solution of the utility model below with reference to the accompanying drawings and specific embodiments.
As shown in Figure 1, a kind of material recycling device of triphenylchloromethane production is provided in the present embodiment, including case Body 1, the babinet 1 is interior to be equipped with two pieces of partition plates being oppositely arranged, and the babinet 1 is divided for reative cell 11, supplied by two pieces of partition plates Hot cell 12, induction chamber 13, it is described to supply hot cell 12 between the reative cell 11 and the induction chamber 13；On the reative cell 11 Side is equipped with the first feeding box 21 and the second feeding box 22, and first feeding box 21 and second feeding box 22 are respectively by the One pipeline 211 and second pipe 221 are connected with the reative cell 11, and first pipeline 211 is equipped with the first solenoid valve 212, the second pipe 221 is equipped with second solenoid valve 222, and rabble 31, the stirring are additionally provided with the reative cell 11 Bar 31 is driven by motor 3；Described to be equipped with heater 121 for 12 bottom of hot cell, the heat-generating pipe 122 of the heater 121 is located at institute State in hot cell 12；The top of the induction chamber 13 is equipped with the 3rd feeding box 23 and wind turbine 4, and the 3rd feeding box 23 passes through the Three pipelines 231 are connected with the induction chamber 13, and the 3rd pipeline 231 is equipped with the 3rd solenoid valve 232；The wind turbine 4 Gas outlet is connected by air outlet pipe 41 with the induction chamber 13, and the air inlet of the wind turbine 4 passes through the first air inlet pipe 42 and the external world Reaction kettle connection 6；11 side wall of reative cell is equipped with the first liquid level sensor 111, level sensor 112 and temperature sensing Device 113；13 side wall of induction chamber is equipped with the second liquid level sensor 131 and pH sensor 132；First level sensing Device 111, the level sensor 112, the temperature sensor 113；Second liquid level sensor 131, pH value sensing Device 132, first solenoid valve 212, the second solenoid valve 222, the 3rd solenoid valve 232, the heater 121, institute State motor 3 and the wind turbine 4 is electrically connected with controller 5.
The material recycling device of above-mentioned triphenylchloromethane production, wherein the processing of the reative cell 11 is that solid gives up Material, solid waste are stored in first feeding box 21, and lytic agent is stored in second feeding box 22；Carrying out solid waste During processing, first solenoid valve 212 is opened, solid waste enters the reative cell 11, until exciting the level sensor 112, first solenoid valve 212 is closed, opens the second solenoid valve 222, lytic agent enters the reative cell 11, until swashing Send out the first liquid level sensor 111 described；Then the motor 3 is started, under the stirring action of the rabble 31, solid waste Quick dissolving, reaction, the preset time of the motor 3 reach, and stop the motor 3 and solution is drained into downstream, will be molten Liquid further recycles；The exhaust gas that the induction chamber 13 is handled, it is generally in the majority with sour gas, therefore the 3rd feeding box 23 is deposited Alkaline solution is put, when carrying out exhaust-gas treatment, opens the 3rd solenoid valve 232, alkaline solution enters the induction chamber 13, directly To second liquid level sensor 131 is excited, the 3rd solenoid valve 232 is closed, it is a large amount of under the neutralization of alkaline solution Purify exhaust gas；Starting the wind turbine 4, purified exhaust gas enters the induction chamber 13 along first air inlet pipe 41,；When described When pH sensor 132 reaches preset value, the alkaline solution in the induction chamber 13 is drained into downstream, further recycling； Persistently to 13 heat supply of the reative cell 11 and the induction chamber, accelerate reaction process, promote recycling in wherein described heat supply room 12；Institute State heater 121 and suitable heating and cooling are carried out according to the temperature sensor 113, ensure to provide suitable reaction temperature.
Further, first liquid level sensor 111 is located at the top of the level sensor 112, it is ensured that offer The dissolving of the enough solid wastes of lytic agent, improves the rate of recovery, reduces and wastes, reduces cost.
Further, the rabble 31 is equipped with polylith paddle 311, and the paddle 311 is equipped with through hole 312；The rabble 31 can be stirred the solid waste in the reative cell 11, accelerate dissolving, promote reaction process；Its The paddle 311 of upper design increases the contact area with waste material, can abundant comminuting matter；And the paddle 311 Son is equipped with through hole 312, is flowed in whipping process easy to liquid, and realization comes into full contact with, promotes reaction.
Further, the second air inlet pipe 43, described second air inlet pipe, 43 one end and the wind turbine are additionally provided with the wind turbine 4 4 air inlet connection, the other end are connected with the reative cell 11；The dissolving recycling of solid waste is carried out in the reative cell 11, The process can produce exhaust gas, if exhaust gas drains into the external world and can cause environmental pollution, it is therefore desirable to what is produced in the reative cell 11 Exhaust gas is recycled；The exhaust gas produced in the reative cell 11 can be led into institute by the design of second air inlet pipe 43 Induction chamber 13 is stated to be recycled.
Further, first air inlet pipe 42 is hose, and its free end is equipped with pipe fitting 421, described first into Tracheae 42 is mainly connected with the reaction kettle of the production equipment of triphenylchloromethane, absorbs what chemical reaction in production process produced In gas to the induction chamber 13, using hose design so that first air inlet pipe 42 meet in production equipment various angles or The adjustment in direction；And its free end is equipped with the pipe fitting 421, extension easy to first air inlet pipe 42, to adapt to Equipment and operating condition.
Further, storage alkaline solution in the induction chamber 13, it is molten that the end of the air outlet pipe 41 is located at the air-breathing In agent；Why the induction chamber 13 can handle exhaust gas, mainly in the induction chamber 13 the air-breathing solvent of storage with Sour gas in exhaust gas carries out neutralization absorption, and the speed for absorbing acid waste gas can be greatly speeded up using alkaline solution and is improved The solubility of exhaust gas.
Further, the air outlet pipe 41 is equipped with check valve 411；It can prevent the suction of storage in the induction chamber 13 Gaseous solvents are back at the wind turbine 4 along the air outlet pipe 41, avoid the wind turbine 4 from contacting water and be damaged.
Further, 13 upper wall of induction chamber is equipped with relief valve 133；The induction chamber 13 is to handle to give up in whole device The core component of gas, it, which all absorbs all exhaust gas, puts together, and can suck substantial amounts of air while exhaust gas is absorbed 13 in the induction chamber, the setting of the relief valve 133 will can then arrange outside air in time, avoid because of the gas in the induction chamber 13 Press through the high damage for causing equipment.
The utility model is described with reference to the preferred embodiments, and those skilled in the art know, is not departing from this reality In the case of with new spirit and scope, various changes or equivalence replacement can be carried out to these features and embodiment.This reality It is not limited to the particular embodiment disclosed with new, other embodiments fallen into claims hereof all belong to In the scope of the utility model protection.

Claims (8)

  1. A kind of 1. material recycling device of triphenylchloromethane production, it is characterised in that：
    It is equipped with two pieces of partition plates being oppositely arranged including babinet (1), in the babinet (1), two pieces of partition plates are by the babinet (1) It is divided into reative cell (11), for hot cell (12), induction chamber (13), it is described to be located at the reative cell (11) and the suction for hot cell (12) Between gas chamber (13)；
    Be equipped with the first feeding box (21) and the second feeding box (22) above the reative cell (11), first feeding box (21) and Second feeding box (22) is connected by the first pipeline (211) and second pipe (221) with the reative cell (11) respectively, and First pipeline (211) is equipped with the first solenoid valve (212), and the second pipe (221) is equipped with second solenoid valve (222), rabble (31) is additionally provided with the reative cell (11), the rabble (31) is driven by motor (3)；
    Described to be equipped with heater (121) for hot cell (12) bottom, the heat-generating pipe (122) of the heater (121) is located at the confession In hot cell (12)；
    The 3rd feeding box (23) and wind turbine (4) are equipped with above the induction chamber (13), the 3rd feeding box (23) passes through the 3rd Pipeline (231) is connected with the induction chamber (13), and the 3rd pipeline (231) is equipped with the 3rd solenoid valve (232)；The wind The gas outlet of machine (4) is connected by air outlet pipe (41) with the induction chamber (13), the air inlet of the wind turbine (4) by first into Tracheae (42) connects (6) with extraneous reaction kettle；
    Reative cell (11) side wall is equipped with the first liquid level sensor (111), level sensor (112) and temperature sensor (113)；Induction chamber (13) side wall is equipped with the second liquid level sensor (131) and pH sensor (132)；First liquid Level sensor (111), the level sensor (112), the temperature sensor (113)；Second liquid level sensor (131), the pH sensor (132), first solenoid valve (212), the second solenoid valve (222), the 3rd electricity Magnet valve (232), the heater (121), the motor (3) and the wind turbine (4) are electrically connected with controller (5).
  2. 2. the material recycling device of triphenylchloromethane production according to claim 1, it is characterised in that：
    First liquid level sensor (111) is located at the top of the level sensor (112).
  3. 3. the material recycling device of triphenylchloromethane production according to claim 1, it is characterised in that：
    The rabble (31) is equipped with polylith paddle (311), and the paddle (311) is equipped with through hole (312).
  4. 4. the material recycling device of triphenylchloromethane production according to claim 1, it is characterised in that：
    Be additionally provided with the second air inlet pipe (43) on the wind turbine (4), described second air inlet pipe (43) one end and the wind turbine (4) into Gas port connects, and the other end is connected with the reative cell (11).
  5. 5. the material recycling device of triphenylchloromethane production according to claim 1, it is characterised in that：
    First air inlet pipe (42) is hose, and its free end is equipped with pipe fitting (421).
  6. 6. the material recycling device of triphenylchloromethane production according to claim 1, it is characterised in that：
    Storage alkaline solution in the induction chamber (13), the end of the air outlet pipe (41) is located in the air-breathing solvent.
  7. 7. the material recycling device of triphenylchloromethane production according to claim 1, it is characterised in that：
    The air outlet pipe (41) is equipped with check valve (411).
  8. 8. the material recycling device of triphenylchloromethane production according to claim 1, it is characterised in that：
    Induction chamber (13) upper wall is equipped with relief valve (133).
CN201721338300.6U 2017-10-17 2017-10-17 A kind of material recycling device of triphenylchloromethane production Expired - Fee Related CN207287120U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721338300.6U CN207287120U (en) 2017-10-17 2017-10-17 A kind of material recycling device of triphenylchloromethane production

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721338300.6U CN207287120U (en) 2017-10-17 2017-10-17 A kind of material recycling device of triphenylchloromethane production

Publications (1)

Publication Number Publication Date
CN207287120U true CN207287120U (en) 2018-05-01

Family

ID=62272656

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201721338300.6U Expired - Fee Related CN207287120U (en) 2017-10-17 2017-10-17 A kind of material recycling device of triphenylchloromethane production

Country Status (1)

Country Link
CN (1) CN207287120U (en)

Similar Documents

Publication Publication Date Title
CN107311416A (en) A kind of integrated ecological sludge treatment device
CN202447086U (en) Stainless steel reaction kettle
CN102974182B (en) Method for treating smelting flue gas containing secondary zinc oxide
CN205634922U (en) Device of nitrogen oxide waste gas recovery diamond waste product
CN207287120U (en) A kind of material recycling device of triphenylchloromethane production
CN207552063U (en) A kind of waste water treatment system
CN207276448U (en) A kind of integrated ecological sludge treatment device
CN202606055U (en) Device for preparing barium chloride solution
CN207254918U (en) A kind of soil restoring device
CN204738001U (en) System for mercury in useless mercury catalyst of high -efficient environmental protection recovery
CN207126357U (en) A kind of waste gas purification environmental protection equipment
CN206570227U (en) Calcium plaster processing unit in heat-engine plant wet desulphurization system
CN201848198U (en) Industrial waste gas treatment and salt regenerating unit
CN104089492A (en) Closed submerged arc furnace coal gas dry-process purifying and recycling system
CN209646480U (en) It is a kind of for solar energy give up chip recovery processing reaction unit
CN202346788U (en) Iron oxide slurry production system provided with high-temperature exhaust gas recovery device
CN104152684B (en) A kind of cylinder Horizontal normal pressure strengthening leaching tanks
CN202342934U (en) Device for treating isopropylbenzene oxidized tail gas
CN207294189U (en) The separation and recovery system of silicon carbide micro-powder waste material
CN205570006U (en) Digester environmental protection dust collector
CN212383676U (en) Chemical industry reation kettle device with waste gas recovery utilizes
CN202382225U (en) Steam condensate water internal circulation application device
CN207605737U (en) A kind of water purification agent reaction kettle
CN205635803U (en) Copper recovery device
CN220443514U (en) Ammonia recovery device

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180501

Termination date: 20181017

CF01 Termination of patent right due to non-payment of annual fee