CN207286870U - Sensitive liquid filtration apparatus - Google Patents

Sensitive liquid filtration apparatus Download PDF

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Publication number
CN207286870U
CN207286870U CN201721060881.1U CN201721060881U CN207286870U CN 207286870 U CN207286870 U CN 207286870U CN 201721060881 U CN201721060881 U CN 201721060881U CN 207286870 U CN207286870 U CN 207286870U
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China
Prior art keywords
sensitive liquid
inlet tube
filtration apparatus
liquid filtration
surge
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Expired - Fee Related
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CN201721060881.1U
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Chinese (zh)
Inventor
周中高
元洋洋
蓝倩
谢永荣
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Gannan Normal University
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Gannan Normal University
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Expired - Fee Related legal-status Critical Current
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Abstract

The utility model provides a kind of sensitive liquid filtration apparatus, it includes surge flask, inlet tube and outlet tube, the inlet tube and outlet tube are respectively arranged at the both ends of surge flask, filter plate is equipped with the middle part of the surge flask, surge flask is separated out preceding surge bunker and rear surge bunker by the filter plate, the middle part of the inlet tube is equipped with preceding air extraction connector, and the middle part of the outlet tube is equipped with rear air extraction connector, and the oral area of the inlet tube is equipped with thread rubber plug.The utility model is safe and efficient compared with sensitive liquid filtration apparatus under traditional inert gas shielding; oxygen, steam in ingress of air are not required in filter process; whole filter process can be completed in a few minutes, greatly facilitate the filtering of sensitive liquid under inert gas shielding.

Description

敏感液体过滤装置Sensitive Liquid Filters

技术领域technical field

本实用新型涉及化学实验特规类仪器制备技术领域,特别是惰性气体保护下敏感液体或反应过程中涉及敏感液体过滤所用的一种新型的过滤装置。The utility model relates to the technical field of preparation of special instruments for chemical experiments, in particular to a novel filter device used for filtering sensitive liquids under the protection of inert gas or sensitive liquids involved in the reaction process.

背景技术Background technique

化学实验中经常遇到一些物质对空气、水汽敏感,这类物质都是储存在惰性气氛中的,同时涉及这类对空气、水汽敏感的物质的化学实验通常也是在惰性气氛中进行的,通常一个化学实验会涉及到多步化学反应,并且前面的化学反应步骤会生成一些不参与后续化学反应的物质,甚至残留物或者原料会使后续的化学反应难以发生或产率低下;另外一些时候前面的化学反应用到一些原料没有反应完,不合适参与后续反应,需要经过过滤分离就可以去除,而不经过分离的话,有可能影响后续化学反应,这时候往往就非常麻烦,通常用的方法是沉积法,将反应溶液经过一定时间的沉降,用注射器或者双针尖取上层清液进行下一步化学反应,而这时将面临几大缺点:反应原料的损失;反应原料计量不准;反应原料转移过程中引入空气、水汽,甚者会导致反应体系自燃或爆炸等安全事故。In chemical experiments, it is often encountered that some substances are sensitive to air and water vapor. Such substances are stored in an inert atmosphere. At the same time, chemical experiments involving such substances sensitive to air and water vapor are usually carried out in an inert atmosphere. Usually A chemical experiment will involve multi-step chemical reactions, and the previous chemical reaction steps will generate some substances that do not participate in the subsequent chemical reactions, and even residues or raw materials will make the subsequent chemical reactions difficult to occur or the yield will be low; The chemical reaction uses some raw materials that have not been reacted and are not suitable for subsequent reactions. They need to be removed by filtration and separation. If they are not separated, they may affect the subsequent chemical reactions. This is often very troublesome. The usual method is In the deposition method, the reaction solution is settled for a certain period of time, and the supernatant is taken with a syringe or a double needle tip for the next chemical reaction. At this time, several major disadvantages will be faced: loss of reaction raw materials; inaccurate measurement of reaction raw materials; transfer of reaction raw materials The introduction of air and water vapor in the process may even lead to safety accidents such as spontaneous combustion or explosion of the reaction system.

实用新型内容Utility model content

本实用新型的目的在于弥补现有惰性气体保护下敏感液体过滤技术的不足之处,提供一种新型惰性气体保护下敏感液体过滤装置,该装置不仅制作工艺简单,使用惰性气体保护下敏感液体过滤方便、快捷、效果明显,采用该装置在过滤敏感液体流程中不会将空气中的氧气、水汽带入反应体系。The purpose of this utility model is to make up for the shortcomings of the existing sensitive liquid filtration technology under the protection of inert gas, and provide a new type of sensitive liquid filtration device under the protection of inert gas. It is convenient, quick and effective, and the device will not bring oxygen and water vapor in the air into the reaction system in the process of filtering sensitive liquids.

本实用新型是通过以下技术方案实现的:The utility model is achieved through the following technical solutions:

本实用新型提供了一种敏感液体过滤装置,其包括缓冲瓶、进液管和出液管,所述进液管和出液管分别设置于缓冲瓶的两端,所述缓冲瓶中部设有过滤板,所述过滤板将缓冲瓶分隔出前缓冲仓和后缓冲仓,所述进液管的中部设有前抽气接头,所述出液管的中部设有后抽气接头,所述进液管的口部设有螺纹胶塞。The utility model provides a sensitive liquid filtering device, which comprises a buffer bottle, a liquid inlet pipe and a liquid outlet pipe. A filter plate, the filter plate separates the buffer bottle into the front buffer chamber and the rear buffer chamber, the middle part of the liquid inlet pipe is provided with a front suction joint, the middle part of the liquid outlet pipe is provided with a rear suction joint, and the middle part of the liquid inlet pipe is provided with a rear suction joint. The mouth of the liquid pipe is provided with a threaded rubber plug.

作为优选方案,所述进液管通过导管连接有前两口瓶,所述前两口瓶的口部设有螺纹塞,所述导管的两端各设有一个双尖针头。As a preferred solution, the liquid inlet pipe is connected to the front two-neck bottles through a conduit, the mouth of the two front two-necked bottles is provided with a threaded plug, and two ends of the conduit are respectively provided with a double-pointed needle.

作为优选方案,所述出液管的口部连接有后两口瓶。As a preferred solution, the mouth of the liquid outlet pipe is connected with the rear two-necked bottles.

作为优选方案,所述过滤板为砂芯挡板。As a preferred solution, the filter plate is a sand core baffle.

作为优选方案,所述前缓冲仓和后缓冲仓可拆卸地连接。As a preferred solution, the front buffer bin and the rear buffer bin are detachably connected.

与现有技术相比,本实用新型具有如下的有益效果:Compared with the prior art, the utility model has the following beneficial effects:

1、本实用新型的显著特点与传统的惰性气体保护下敏感液体过滤装置相比安全快捷,过滤过程中在惰性气氛中完成,不需要接触空气中的氧气、水汽,整个过滤过程在几分钟内就可以完成,极大地方便了惰性气体保护下敏感液体的过滤;1. The salient features of this utility model are safer and quicker than traditional sensitive liquid filtering devices under the protection of inert gas. The filtering process is completed in an inert atmosphere without contact with oxygen and water vapor in the air. The entire filtering process is within a few minutes. It can be completed, which greatly facilitates the filtration of sensitive liquids under the protection of inert gas;

2、该惰性气体保护下敏感液体过滤装置充分利用重力作用,可以根据不同过滤对象颗粒直径大小的需求,通过改变砂芯挡板的目数,来确定过滤液体的速度;2. The sensitive liquid filtering device under the protection of inert gas makes full use of gravity, and can determine the speed of filtering liquid by changing the mesh number of the sand core baffle according to the requirements of different filter object particle diameters;

3、惰性气体保护下敏感液体过滤装置还具有重复使用效果,对同一过滤对象在使用过程中无需做任何处理,因其在惰性气氛下保存,不会影响再次使用效果,使用成本低廉。3. The sensitive liquid filter device under the protection of inert gas has the effect of repeated use, and there is no need to do any treatment for the same filter object during use, because it is stored in an inert atmosphere, it will not affect the re-use effect, and the use cost is low.

附图说明Description of drawings

通过阅读参照以下附图对非限制性实施例所作的详细描述,本实用新型的其它特征、目的和优点将会变得更明显:Other features, objects and advantages of the present invention will become more apparent by reading the detailed description of non-limiting embodiments with reference to the following drawings:

图1为本实用新型的结构示意图;Fig. 1 is the structural representation of the utility model;

图2为本实用新型中缓冲瓶部分的结构示意图;Fig. 2 is the structural representation of buffer bottle part in the utility model;

图中:1、缓冲瓶;11、前缓冲仓;12、后缓冲仓;2、进液管;21、前抽气接头;3、出液管;31、后抽气接头;4、过滤板;5、导管;6、前两口瓶;7、后两口瓶;8、螺纹胶塞。In the figure: 1. Buffer bottle; 11. Front buffer chamber; 12. Rear buffer chamber; 2. Liquid inlet pipe; 21. Front air extraction joint; 3. Liquid outlet pipe; 31. Rear air extraction joint; 4. Filter plate ; 5. Catheter; 6. Two front bottles; 7. Two back bottles; 8. Thread rubber stopper.

具体实施方式Detailed ways

下面结合具体实施例对本实用新型进行详细说明。以下实施例将有助于本领域的技术人员进一步理解本实用新型,但不以任何形式限制本实用新型。应当指出的是,对本领域的普通技术人员来说,在不脱离本实用新型构思的前提下,还可以做出若干变形和改进。这些都属于本实用新型的保护范围。The utility model is described in detail below in conjunction with specific embodiments. The following examples will help those skilled in the art to further understand the utility model, but do not limit the utility model in any form. It should be noted that those skilled in the art can make several modifications and improvements without departing from the concept of the present utility model. These all belong to the protection domain of the present utility model.

本实用新型提供了一种敏感液体过滤装置如图1和2所示,包括缓冲瓶1、进液管2和出液管3,进液管2和出液管3分别设置于缓冲瓶1的两端,缓冲瓶1中部设有过滤板4,过滤板4将缓冲瓶1分隔出前缓冲仓11和后缓冲仓12,进液管2的中部设有前抽气接头21,出液管3的中部设有后抽气接头31,进液管2的口部设有螺纹胶塞8。The utility model provides a sensitive liquid filtering device as shown in Figures 1 and 2, comprising a buffer bottle 1, a liquid inlet pipe 2 and a liquid outlet pipe 3, and the liquid inlet pipe 2 and the liquid outlet pipe 3 are respectively arranged at the bottom of the buffer bottle 1 At both ends, a filter plate 4 is provided in the middle of the buffer bottle 1, and the filter plate 4 separates the buffer bottle 1 into a front buffer chamber 11 and a rear buffer chamber 12. The middle part is provided with a rear suction joint 31, and the mouth of the liquid inlet pipe 2 is provided with a threaded rubber plug 8.

进液管1通过导管5连接有前两口瓶6,前两口瓶6的口部设有螺纹胶塞8,导管5 的两端各设有一个双尖针头。The liquid inlet pipe 1 is connected with the front two-necked bottles 6 through the conduit 5, the mouth of the front two-necked bottles 6 is provided with a threaded rubber plug 8, and the two ends of the conduit 5 are respectively provided with a double-pointed needle.

出液管3的口部连接有后两口瓶7,后两口瓶7上也设有螺纹胶塞8。The mouth of the outlet pipe 3 is connected with the rear two-necked bottles 7, and the rear two-necked bottles 7 are also provided with threaded rubber plugs 8.

过滤板4为砂芯挡板。The filter plate 4 is a sand core baffle.

为了便于过滤板4的清理和更换,前缓冲仓11和后缓冲仓12可拆卸地连接,如旋接。In order to facilitate the cleaning and replacement of the filter plate 4, the front buffer bin 11 and the rear buffer bin 12 are detachably connected, such as screwed.

以上对本实用新型的具体实施例进行了描述。需要理解的是,本实用新型并不局限于上述特定实施方式,本领域技术人员可以在权利要求的范围内做出各种变形或修改,这并不影响本实用新型的实质内容。The specific embodiments of the present utility model have been described above. It should be understood that the utility model is not limited to the above-mentioned specific embodiments, and those skilled in the art can make various changes or modifications within the scope of the claims, which does not affect the essence of the utility model.

Claims (5)

  1. A kind of 1. sensitive liquid filtration apparatus, it is characterised in that including surge flask, inlet tube and outlet tube, the inlet tube and Outlet tube is respectively arranged at the both ends of surge flask, is equipped with filter plate in the middle part of the surge flask, the filter plate separates surge flask Go out preceding surge bunker and rear surge bunker, the middle part of the inlet tube is equipped with preceding air extraction connector, and the middle part of the outlet tube is taken out after being equipped with Gas connector, the oral area of the inlet tube are equipped with thread rubber plug.
  2. 2. sensitive liquid filtration apparatus as claimed in claim 1, it is characterised in that before the inlet tube is connected with by conduit Two-mouth bottle, the oral area of the preceding two-mouth bottle are equipped with thread plug, and the both ends of the conduit are respectively provided with a double pointed syringe needle.
  3. 3. sensitive liquid filtration apparatus as claimed in claim 1, it is characterised in that the oral area of the outlet tube is connected with rear two Mouth bottle.
  4. 4. sensitive liquid filtration apparatus as claimed in claim 1, it is characterised in that the filter plate is sand core baffle.
  5. 5. the sensitive liquid filtration apparatus as described in any one in Claims 1 to 4, it is characterised in that the preceding surge bunker It is detachably connected with rear surge bunker.
CN201721060881.1U 2017-08-23 2017-08-23 Sensitive liquid filtration apparatus Expired - Fee Related CN207286870U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721060881.1U CN207286870U (en) 2017-08-23 2017-08-23 Sensitive liquid filtration apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721060881.1U CN207286870U (en) 2017-08-23 2017-08-23 Sensitive liquid filtration apparatus

Publications (1)

Publication Number Publication Date
CN207286870U true CN207286870U (en) 2018-05-01

Family

ID=62437421

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201721060881.1U Expired - Fee Related CN207286870U (en) 2017-08-23 2017-08-23 Sensitive liquid filtration apparatus

Country Status (1)

Country Link
CN (1) CN207286870U (en)

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180501

Termination date: 20190823

CF01 Termination of patent right due to non-payment of annual fee