CN207280538U - Sensitive liquid shifts and dispensing device - Google Patents

Sensitive liquid shifts and dispensing device Download PDF

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Publication number
CN207280538U
CN207280538U CN201721060894.9U CN201721060894U CN207280538U CN 207280538 U CN207280538 U CN 207280538U CN 201721060894 U CN201721060894 U CN 201721060894U CN 207280538 U CN207280538 U CN 207280538U
Authority
CN
China
Prior art keywords
mouth
air extraction
sensitive liquid
extraction connector
dispensing device
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201721060894.9U
Other languages
Chinese (zh)
Inventor
周中高
元洋洋
李美
谢永荣
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Gannan Normal University
Original Assignee
Gannan Normal University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Gannan Normal University filed Critical Gannan Normal University
Priority to CN201721060894.9U priority Critical patent/CN207280538U/en
Application granted granted Critical
Publication of CN207280538U publication Critical patent/CN207280538U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model provides a kind of sensitive liquid transfer and dispensing device, it includes preceding air extraction connector, two mouth flask, double ground graduated cylinders, conduit and rear air extraction connector, the preceding air extraction connector is arranged on a mouth of two mouth flask, air extraction connector is arranged on a mouth of double ground graduated cylinders after described, another mouth of the two mouth flask is equipped with thread rubber plug, another mouth of double ground graduated cylinders is equipped with thread rubber plug, and the both ends of the conduit are arranged in two thread rubber plugs respectively.The utility model sensitive liquid shifts and dispensing device not ingress of air during sensitive liquid shifts and measures, economical and practical, safe and efficient.

Description

Sensitive liquid shifts and dispensing device
Technical field
The utility model is related to the glass apparatus preparation field of sensitive compound correlation special requirement, particularly to oxygen, Sensitive liquid involved in water vapor sensitive liquid or reaction process accurately adds a kind of new accurate dress shifted and measure used Put.
Background technology
High reaction activity is generally configured with to the compound of oxygen, water vapor sensitive and possesses special performance, with chemical work The rapid development of industry, the use on chemical industry is more and more extensive, is extensively closed in pharmacy, national defence and field of scientific study Note.For the transfer and measurement of this kind of oxygen, the liquid of water vapor sensitive, general organic chemistry procedures are clearly what is do not applied to, Some special instruments and a set of cleverly operating technology must be used.At present, method the safest is full of indifferent gas Carried out in the use for laboratory vacuum glove box of atmosphere, but since use for laboratory vacuum glove box is expensive, takes up a large area and day The features such as often maintenance cost is higher, is restricted its popularity used, in the case of not satisfying the requirements in many laboratories, It is exactly using Simple hand casing using a kind of possible alternative of relatively economical, but use cost is high, and operation is cumbersome, separately It is outer, also without water, oxygen content detecting system, gas leakage easily to occur because removing water deaerating type of cycles without circulation, make oxygen in air, Steam enters, once gas leakage, sensitive liquid is chemically reacted with oxygen, steam in air, and gently then sample goes bad, heavy then possible Cause sensitive liquid spontaneous combustion or explosion, trigger security incident.In addition it is that common method is syringe transfer and amount to also have one kind Take, but syringe needle exposure is in atmosphere, is very easy to trigger the reaction of sensitive liquid and oxygen, steam in air, draws Send out security incident unnecessary.
Utility model content
The purpose of this utility model is that make up it is existing to oxygen, water vapor sensitive liquid shift and measure the prior art not Foot part, there is provided a kind of new sensitive liquid transfer and dispensing device, not only manufacture craft is simple for the device, but also sensitive liquid Convenient transfer, quick, positive effect, will not be by the oxygen in air during shifting and measuring sensitive liquid using the device Gas and water vapour brings transfering system into, can effectively avoid security incident.
The utility model is achieved through the following technical solutions:
The utility model provides a kind of transfer of sensitive liquid and dispensing device, it include preceding air extraction connector, two mouth flask, Double ground graduated cylinders, conduit and rear air extraction connector, the preceding air extraction connector are arranged on a mouth of two mouth flask, are evacuated after described Connector is arranged on a mouth of double ground graduated cylinders, another mouth of the two mouth flask is equipped with thread rubber plug, double mills Another mouth of mouth graduated cylinder is equipped with thread rubber plug, and the both ends of the conduit are arranged in two thread rubber plugs respectively.
Preferably, the both ends of the conduit are respectively provided with a double pointed syringe needle.
Compared with prior art, the utility model has following beneficial effect:
The distinguishing feature of the utility model is cheap and easy to get, safe, easy to use compared with traditional sensitive liquid transfer device, Oxygen, steam in ingress of air are not required during transfer and measurement, whole transfer process is completed in seconds, due to making It is tool scale ground graduated cylinder, whole transfer and measurement process accurately controls, and greatly facilitates the transfer of sensitive liquid And measurement;
In addition, sensitive liquid transfer and dispensing device make full use of the gas pressure of additional inert gas, can basis Difference transfer and measure object volumes number, by varying the internal diameter of double pointed syringe needle is lengthened, to control transfer and measure liquid Speed, while whether according to lengthening double pointed syringe needle one end by controlling and entering liquid, to control the double pointed syringe needle of lengthening whether residual Liquid stay, makes residual liquid enter two mouthfuls of round-bottomed flasks by the way of inert atmosphere is blown;
It is of low cost meanwhile sensitive liquid transfer and dispensing device also have reuse effect, are used multiple times.
Brief description of the drawings
Upon reading the detailed description of non-limiting embodiments with reference to the following drawings, other spies of the utility model Sign, objects and advantages will become more apparent upon:
Fig. 1 is the structure diagram of the utility model;
In figure:1st, preceding air extraction connector;2nd, two mouth flask;3rd, double ground graduated cylinders;4th, rear air extraction connector;5th, conduit;6th, screw thread Rubber plug.
Embodiment
The utility model is described in detail with reference to specific embodiment.Following embodiments will be helpful to this area Technical staff further understands the utility model, but does not limit the utility model in any form.It should be pointed out that to ability For the those of ordinary skill in domain, without departing from the concept of the premise utility, various modifications and improvements can be made. These belong to the scope of protection of the utility model.
As shown in Figure 1, a kind of sensitive liquid transfer provided by the utility model and dispensing device, it includes preceding air extraction connector 1st, two mouth flask 2, double ground graduated cylinders 3, rear air extraction connector 4 and conduit 5, preceding air extraction connector 1 are arranged at a mouth of two mouth flask 2 On, rear air extraction connector 4 is arranged on a mouth of double ground graduated cylinders 3, another mouth of two mouth flask 2 is equipped with thread rubber plug 6, a thread rubber plug 6 also is provided with another mouth of double ground graduated cylinders 3, and the both ends of conduit 5 are arranged in two screw thread glue respectively In plug 6.
For the ease of the access of conduit, the both ends of conduit 5 are respectively provided with a double pointed syringe needle.
In use, by preceding air extraction connector 1, two mouth flask 2, double ground graduated cylinders 3, rear air extraction connector 4, conduit 5 and screw thread glue Plug 6 is installed as shown in Figure 1, is sensitive liquid transfer and dispensing device.Have the preceding air extraction connector 1 and vacuum pump of glass section door It is connected, the glass section door of preceding air extraction connector 1 is opening, and rear air extraction connector 4 is connected with inert gas source, rear air extraction connector 4 Glass section door be in off state, start vacuum pump, take out 30 seconds, the glass section door of air extraction connector 1, is evacuated after unlatching before closing Connector 4 has glass section door, makes inert gas full of sensitive liquid transfer and dispensing device.Repeat this step three times, then it is described quick Inert gas is full of in the transfer of sense liquid and dispensing device, forms sensitive liquid transfer and dispensing device under inert gas shielding.
When transfer and measurement sensitive liquid, preceding air extraction connector 1 connects bubbler, and rear air extraction connector 4 is connected with inert gas source, The glass section door of air extraction connector 4 after unlatching, sensitive liquid by the pressure of inert gas, accurately shifted and measured to two mouthfuls In flask 2, specific volume is read by the scale on graduated cylinder, when reaching volume needed for transfer and measurement, is evacuated and is connect after closing First 4 glass section door.
Specific embodiment of the utility model is described above.It is to be appreciated that the utility model not office It is limited to above-mentioned particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, This has no effect on the substantive content of the utility model.

Claims (2)

1. a kind of sensitive liquid transfer and dispensing device, it is characterised in that including preceding air extraction connector, two mouth flask, double ground amounts Cylinder, conduit and rear air extraction connector, the preceding air extraction connector are arranged on a mouth of two mouth flask, and the rear air extraction connector is set In on a mouth of double ground graduated cylinders, another mouth of the two mouth flask is equipped with thread rubber plug, double ground graduated cylinders Another mouth is equipped with thread rubber plug, and the both ends of the conduit are arranged in two thread rubber plugs respectively.
2. sensitive liquid transfer as claimed in claim 1 and dispensing device, it is characterised in that the both ends of the conduit are respectively provided with One double pointed syringe needle.
CN201721060894.9U 2017-08-23 2017-08-23 Sensitive liquid shifts and dispensing device Expired - Fee Related CN207280538U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721060894.9U CN207280538U (en) 2017-08-23 2017-08-23 Sensitive liquid shifts and dispensing device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721060894.9U CN207280538U (en) 2017-08-23 2017-08-23 Sensitive liquid shifts and dispensing device

Publications (1)

Publication Number Publication Date
CN207280538U true CN207280538U (en) 2018-04-27

Family

ID=61984641

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201721060894.9U Expired - Fee Related CN207280538U (en) 2017-08-23 2017-08-23 Sensitive liquid shifts and dispensing device

Country Status (1)

Country Link
CN (1) CN207280538U (en)

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GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180427

Termination date: 20190823