CN207237985U - A kind of reaction kettle of amino acids production processing - Google Patents
A kind of reaction kettle of amino acids production processing Download PDFInfo
- Publication number
- CN207237985U CN207237985U CN201721078949.9U CN201721078949U CN207237985U CN 207237985 U CN207237985 U CN 207237985U CN 201721078949 U CN201721078949 U CN 201721078949U CN 207237985 U CN207237985 U CN 207237985U
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- CN
- China
- Prior art keywords
- heat
- water pipe
- autoclave body
- heat exchanging
- exchanging water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 29
- 150000001413 amino acids Chemical class 0.000 title claims abstract description 22
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- 238000012545 processing Methods 0.000 title claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 80
- 238000005057 refrigeration Methods 0.000 claims abstract description 19
- 230000009471 action Effects 0.000 claims abstract description 18
- 238000001816 cooling Methods 0.000 claims abstract description 13
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 13
- 229920000742 Cotton Polymers 0.000 claims description 27
- 238000004321 preservation Methods 0.000 claims description 27
- 238000011084 recovery Methods 0.000 claims description 16
- 238000009413 insulation Methods 0.000 claims description 11
- 229910052602 gypsum Inorganic materials 0.000 claims description 8
- 239000010440 gypsum Substances 0.000 claims description 8
- 239000004744 fabric Substances 0.000 claims description 6
- 239000000853 adhesive Substances 0.000 claims description 3
- 230000001070 adhesive effect Effects 0.000 claims description 3
- 238000004804 winding Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 16
- 238000002425 crystallisation Methods 0.000 abstract description 13
- 230000008025 crystallization Effects 0.000 abstract description 13
- 238000012546 transfer Methods 0.000 abstract description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- 239000000741 silica gel Substances 0.000 description 6
- 229910002027 silica gel Inorganic materials 0.000 description 6
- 238000010586 diagram Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000000178 monomer Substances 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 230000006641 stabilisation Effects 0.000 description 2
- 238000011105 stabilization Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The utility model discloses a kind of reaction kettle of amino acids production processing, including autoclave body, the autoclave body external spiral is wound with heat exchanging water pipe, the heat exchanging water pipe is connected with the refrigeration system for cooling down moisture, heat conduction silicone is filled between the heat exchanging water pipe and the autoclave body, side of the heat exchanging water pipe away from the autoclave body is enclosed with insulating layer.This programme uses new mechanical structure.The utility model has the following advantages and effect：Heat conduction silicone can be stably fitted on autoclave body and heat exchanging water pipe, rapidly absorb the heat on autoclave body, and transfer heat to heat exchanging water pipe, moisture in heat exchanging water pipe constantly circulates under the action of refrigeration system, the heat that can be more evenly absorbed in same level, autoclave body side can stablize in same level and balancedly cool down, and keep good partial crystallization speed.The setting of insulating layer is used to exchange between hot-water line and external environment to be isolated, and reduces the influence of external environment exchange hot-water line.
Description
Technical field
It the utility model is related to amino acids production process equipment, more particularly to a kind of reaction for amino acid partial crystallization process
Kettle.
Background technology
The broad understanding of reaction kettle has the container physically or chemically reacted, is matched somebody with somebody by the structure design to container with parameter
Put, realize the mixture function of the heating of technological requirement, evaporation, cooling and low high speed.
Notification number is the reaction kettle of the one kind of multiple monomer polymerization reactions of Chinese patent of CN205700534U, including reaction kettle
Body, feed inlet, discharge port, blender, reacting kettle jacketing, reacting kettle jacketing water inlet, reacting kettle jacketing water outlet；Reaction kettle
Bodies top is equipped with several feed inlets；Reaction kettle body bottom portion is equipped with a discharge port；Reaction kettle body is externally provided with reaction kettle
Chuck；External heating cooling chamber is formed between reacting kettle jacketing and reaction kettle body；The bottom of reacting kettle jacketing is equipped with reaction kettle
Chuck water inlet；The top of reacting kettle jacketing is equipped with reacting kettle jacketing water outlet；In reaction kettle body stirring is equipped with along center line
Device；Blender includes servomotor, agitating shaft and agitating paddle；Servomotor is arranged on the top of reaction kettle body；Agitating shaft with
Servomotor connects；Agitating paddle and stirring axis connection.
It can be adjusted in above-mentioned scheme from the inside and outside temperature in reaction kettle, full and uniform is scattered poly-
Monomer adduct, avoids polymer reaction monomer from being segregated.But during the mode that cold water is added into chuck realizes cooling,
Since cold water needs constantly to be circulated, and the position of water inlet and water outlet is fixed, close water inlet one end with it is close
The temperature spread of water outlet one end is larger, therefore differs for the cooling temperature of each position of body, causes partial crystallization speed to decline, shadow
Ring processing efficiency.
Utility model content
The purpose of this utility model is to provide a kind of reaction kettle of amino acids production processing, during partial crystallization is carried out,
Temperature positioned at autoclave body both sides is than more uniform, so as to lift partial crystallization effect.
The above-mentioned technical purpose of the utility model technical scheme is that：A kind of amino acids production adds
The reaction kettle of work, including autoclave body, the autoclave body external spiral are wound with heat exchanging water pipe, and the heat exchanging water pipe is connected with for cooling water
The refrigeration system divided, is filled with heat conduction silicone, the heat exchanging water pipe is away from described between the heat exchanging water pipe and the autoclave body
The side of autoclave body is enclosed with insulating layer.
By using above-mentioned technical proposal, the heat conduction silicone set between autoclave body and heat exchanging water pipe, heat conduction silicone
It can stably be fitted on autoclave body and heat exchanging water pipe, rapidly absorb the heat on autoclave body, and transfer heat to heat exchange
Water pipe, the moisture in heat exchanging water pipe constantly circulate under the action of refrigeration system, can more be evenly absorbed in same level
Heat in face, autoclave body side can stablize in same level and balancedly cool down, and keep the stability of solution, brilliant
The amino acid separated out can be precipitated stably, keep good partial crystallization speed.The setting of insulating layer is used to exchange hot water
Isolated between pipe and external environment, reduce the influence of external environment exchange hot-water line, heat exchanging water pipe can stablize and efficiently
Cool down to autoclave body.
The utility model is further arranged to：Supporting rack is provided with the autoclave body, parcel is provided with support frame as described above
In the fixed frame of heat exchanging water pipe's upper and lower ends.
By using above-mentioned technical proposal, fixed frame is wrapped in the upper and lower ends of heat exchanging water pipe, and in the work of supporting rack
The fixation being maintained under on autoclave body, realizes the supporting role of exchange hot-water line, keeps the stability of heat exchanging water pipe, can stablize
Ground carries out heat exchange, cools down to autoclave body.
The utility model is further arranged to：Support frame as described above includes horizontally disposed pull rod and is used to support the drawing
The brace of bar.
By using above-mentioned technical proposal, the pull rod on supporting rack is used to be supported fixed frame effect, and oblique
The stabilization of pull rod is kept under the action of bar, pull rod is not susceptible to bend, and effect can be stably supported to fixed frame.
The utility model is further arranged to：Grid cloth is adhesive with the side wall of the autoclave body.
By using above-mentioned technical proposal, grid cloth is pasted on the side wall of autoclave body, the roughness on grid cloth surface is higher, leads
Hot layer of silica gel is not susceptible to the offset of position, can stably carry out heat conduction.
The utility model is further arranged to：It is provided with the refrigeration system and is connected to the defeated of the heat exchanging water pipe lower end
Pipe is sent, the recovery tube for being connected to the heat exchanging water pipe upper end is provided with the refrigeration system.
By using above-mentioned technical proposal, the delivery pipe that is set in refrigeration system is used for the Water Transport through cooling to changing
In hot-water line, the moisture that heat absorption is completed is back in refrigeration system again by recovery tube and is cooled down, realize that water follows
Ring, reduces the waste of water resource.
The utility model is further arranged to：Heat-preservation cotton is both provided with outside the delivery pipe and the recovery tube.
By using above-mentioned technical proposal, the setting of heat-preservation cotton is used to reduce shadow of the external environment to delivery pipe and recovery tube
Ring, keep the temperature of both internal moistures, the moisture in delivery pipe efficiently can cool down autoclave body, in delivery pipe
Moisture can reduce the change of temperature so that refrigeration system need not significantly alter the temperature of moisture, save the energy.
The utility model is further arranged to：The section of the heat-preservation cotton is set in annular shape, the side of the heat-preservation cotton
It is useful for carrying out the opening of package action.
By using above-mentioned technical proposal, section in circular heat-preservation cotton can stably and equably to delivery pipe and
Recovery tube carries out package action, keeps good heat-insulating property.The side of heat-preservation cotton sets opening, and opening is opened can be square
Just package action is carried out, lifts the convenient degree of installation.
The utility model is further arranged to：Fastening band is wound with outside the heat-preservation cotton.
By using above-mentioned technical proposal, fastening band is wrapped in outside heat-preservation cotton, the realization pair under the action of band is fastened
The fastening effect of heat-preservation cotton, heat-preservation cotton are not susceptible to position offset, so as to stably carry out package action, lift heat-preservation cotton
Heat insulation effect.
The utility model is further arranged to：The insulating layer is built into by insulation gypsum.
By using above-mentioned technical proposal, insulation gypsum is built into insulating layer, and insulation effect is carried out for exchanging hot-water line, and
And insulation gypsum has good intensity, hot-water line can be exchanged and carry out protective effect, be not easy by extraneous physical damage, lifting
Durability degree.
In conclusion the utility model has the advantages that：Heat exchanging water pipe is spirally wound on autoclave body, in supporting rack
Fixed with holding position under the action of fixed frame, heat conduction is carried out under the action of heat conductive silica gel, can be more equably right
Autoclave body at same level cools down, and the moisture in heat exchanging water pipe connects in the effect of delivery pipe and recovery tube with refrigeration system
Connect, can constantly carry out water circulation, keep stable cooling effect, keep the stability of solution, the amino acid that partial crystallization comes out
Can stably it be precipitated, so as to lift partial crystallization effect.Insulating layer is built into by keeping the temperature gypsum, exchange hot-water line is wrapped
Wrap up in, and delivery pipe and recovery tube are wrapped up by heat-preservation cotton, the moisture in cyclic process can be reduced by external environment
Influence, keep the cooling-down effect good to autoclave body, save the energy.
Brief description of the drawings
Fig. 1 is the exterior overall structure diagram of the present embodiment；
Fig. 2 is the diagrammatic cross-section of autoclave body；
Fig. 3 is the schematic diagram of supporting rack；
Fig. 4 is the connection relationship diagram between autoclave body and heat conduction silicone；
Fig. 5 is the connection relationship diagram between both delivery pipe and recovery tube and heat-preservation cotton.
In figure：1st, autoclave body；2nd, heat exchanging water pipe；3rd, refrigeration system；4th, heat conduction silicone；5th, insulating layer；6th, supporting rack；61、
Pull rod；62nd, brace；7th, fixed frame；8th, grid cloth；9th, delivery pipe；10th, recovery tube；11st, heat-preservation cotton；12nd, it is open；13rd, fastening bag
Band.
Embodiment
The utility model is described in further detail below in conjunction with attached drawing.
A kind of reaction kettle of amino acids production processing, as shown in Figure 1, including autoclave body 1, high concentration is loaded with autoclave body 1
Freamine Ⅲ, amino acid partial crystallization by cooling down to autoclave body 1, can be come out, produce the amino acid of high-purity.
As shown in Fig. 2, 1 external spiral of autoclave body is wound with heat exchanging water pipe 2, with reference to Fig. 1, heat exchanging water pipe 2 connects with refrigeration system 3
Connect, the delivery pipe 9 for being connected to 2 one end of heat exchanging water pipe is provided with refrigeration system 3, for moisture conveying to be entered heat exchanging water pipe
In 2, the recovery tube 10 for being connected to 2 other end of heat exchanging water pipe is additionally provided with refrigeration system 3, for will be discharged in heat exchanging water pipe 2
Water Sproading enter cooling cycle carried out in refrigeration system 3, lift the utilization rate of water resource.
As shown in Fig. 2, being provided with supporting rack 6 on autoclave body 1, and it is connected with and is wrapped on heat exchanging water pipe 2 on supporting rack 6
The fixed frame 7 at lower both ends, by the combination of supporting rack 6 and fixed frame 7, realizes the fixation of exchange hot-water line 2, lifts heat exchange
The stability of water pipe 2, stably can cool down autoclave body 1.
As shown in Figures 2 and 3, supporting rack 6 by the pull rod 61 that is horizontally fixed on autoclave body 1 and is used to support pull rod 61
Brace 62 forms, and one end of brace 62 is welded on autoclave body 1, and the other end is welded on the one end of pull rod 61 away from autoclave body 1, in pull rod
The supporting role to fixed frame 7 can be kept under the action of 61, the stabilization of fixed frame 7 is kept, is realized under the action of brace 62
Supporting role to pull rod 61, pull rod 61 are not susceptible to bend, the stability of raising rod 61, so as to stably to fixation
Frame 7 is supported.
As shown in Fig. 2, being provided with heat conduction silicone 4 between heat exchanging water pipe 2 and autoclave body 1, heat conduction silicone 4 has good
Heat conduction function, can rapidly absorb the heat on autoclave body 1, and cool down under the action of heat exchanging water pipe 2, so that
Lift the efficiency of partial crystallization.Heat conduction silicone 4 is injected between heat exchanging water pipe 2 and autoclave body 1 by heat conductive silica gel and is formed, heat conduction silicone
It can stablize between 4 and heat exchanging water pipe 2 and be bonded in large area, so as to keep good thermal conducting function.
As shown in figure 4, due to the surface smoother of autoclave body 1, what heat conduction silicone 4 cannot be well adhere to, therefore
Be adhesive with grid cloth 8 on the side wall of autoclave body 1, lift roughness, heat conductive silica gel when being injected between autoclave body 1 and heat exchanging water pipe 2,
It can be stably attached between autoclave body 1, keep stable heat to conduct.
As shown in figure 5, be both provided with heat-preservation cotton 11 outside delivery pipe 9 and recovery tube 10, the moisture temperature in delivery pipe 9 compared with
It is low, and the temperature after heat exchange is carried out by heat exchanging water pipe 2 of the moisture in recovery tube 10 still keeps relatively low state,
It can be realized under the action of heat-preservation cotton 11 to the isolation between delivery pipe 9 and external environment condition, reduce external environment condition to moisture
Temperature influences, and saves the energy.
As shown in figure 5, the section of heat-preservation cotton 11 equably can carry out delivery pipe 9 or recovery tube 10 in annular shape
Package action, lifts heat-insulating property.The side of heat-preservation cotton 11 is provided with opening 12, by will be opened at opening 12, Neng Goufang
Just package action is carried out, it is easy to operate, and heat-preservation cotton 11 has good recoverability, and can be certainly after the completion of parcel
It is dynamic to restore, keep good parcel effect.
As shown in figure 5, due to the setting of opening 12, cause heat-preservation cotton 11 on parcel to delivery pipe 9 and recovery tube 10 it
Stability afterwards is relatively low, therefore in the present embodiment, fastening band 13 is wound with outside heat-preservation cotton 11, fastening work is carried out to heat-preservation cotton 11
With the stability of lifting heat-preservation cotton 11, keeps good heat insulation effect.
As shown in Fig. 2, side of the heat exchanging water pipe 2 away from autoclave body 1 is additionally provided with insulating layer 5, by heat exchanging water pipe 2 and extraneous ring
Border is completely cut off, and realizes the insulation effect of exchange hot-water line 2, reduces scattering and disappearing for energy.In the present embodiment, insulating layer 5 has insulation
Gypsum is built into, and insulation gypsum can be stablized and comprehensively be contacted with heat exchanging water pipe 2, be not easy to leave gap between the two, therefore can
Good heat insulation effect is kept, and keeps the temperature gypsum there is preferable intensity, hot-water line 2 can be exchanged and carry out protective effect, carried
Rise the durability degree of equipment.
Specific implementation process：When Freamine Ⅲ in autoclave body 1 needs to carry out cooling partial crystallization, refrigeration system 3 starts, and leads to
Delivery pipe 9 is crossed by the moisture conveying of low temperature into heat exchanging water pipe 2, and heat exchanging water pipe 2 is spirally wound on autoclave body 1, can be opposite
Temperature of the heat exchanging water pipe 2 in same level is equably kept, autoclave body 1 carries out heat transfer by heat conductive silica gel, in heat-exchanging water
Fast cooling is carried out to heat conductive silica gel under the action of pipe 2, so as to fulfill the fast cooling to autoclave body 1, and in same level
In cooling-down effect than more uniform, keep the stability of solution, the amino acid that partial crystallization comes out can be precipitated stably, can
Keep good partial crystallization efficiency.
This specific embodiment is only explanation to the utility model, it is not the limitation to the utility model, ability
Field technique personnel as needed can make the present embodiment the modification of no creative contribution after this specification is read, but
As long as all protected in the right of the utility model be subject to Patent Law.
Claims (9)
1. a kind of reaction kettle of amino acids production processing, including autoclave body (1), it is characterised in that：Autoclave body (1) the external spiral winding
There is heat exchanging water pipe (2), the heat exchanging water pipe (2) is connected with the refrigeration system (3) for cooling down moisture, the heat exchanging water pipe (2)
Heat conduction silicone (4) is filled between the autoclave body (1), side of the heat exchanging water pipe (2) away from the autoclave body (1) is wrapped up
There is insulating layer (5).
A kind of 2. reaction kettle of amino acids production processing according to claim 1, it is characterised in that：On the autoclave body (1)
Supporting rack (6) is provided with, the fixed frame for being wrapped in the heat exchanging water pipe (2) upper and lower ends is provided with support frame as described above (6)
(7)。
A kind of 3. reaction kettle of amino acids production processing according to claim 2, it is characterised in that：Support frame as described above (6)
Including horizontally disposed pull rod (61) and it is used to support the braces (62) of the pull rod (61).
A kind of 4. reaction kettle of amino acids production processing according to claim 1, it is characterised in that：The autoclave body (1)
Grid cloth (8) is adhesive with side wall.
A kind of 5. reaction kettle of amino acids production processing according to claim 1, it is characterised in that：The refrigeration system
(3) delivery pipe (9) for being connected to the heat exchanging water pipe (2) lower end is provided with, is provided with and is connected on the refrigeration system (3)
The recovery tube (10) of heat exchanging water pipe (2) upper end.
A kind of 6. reaction kettle of amino acids production processing according to claim 5, it is characterised in that：The delivery pipe (9)
And it is both provided with heat-preservation cotton (11) outside the recovery tube (10).
A kind of 7. reaction kettle of amino acids production processing according to claim 6, it is characterised in that：The heat-preservation cotton (11)
Section in annular shape, the side of the heat-preservation cotton (11) is provided with the opening (12) for carrying out package action.
A kind of 8. reaction kettle of amino acids production processing according to claim 7, it is characterised in that：The heat-preservation cotton (11)
It is outer to be wound with fastening band (13).
A kind of 9. reaction kettle of amino acids production processing according to claim 1, it is characterised in that：The insulating layer (5)
It is built into by insulation gypsum.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721078949.9U CN207237985U (en) | 2017-08-26 | 2017-08-26 | A kind of reaction kettle of amino acids production processing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721078949.9U CN207237985U (en) | 2017-08-26 | 2017-08-26 | A kind of reaction kettle of amino acids production processing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207237985U true CN207237985U (en) | 2018-04-17 |
Family
ID=61883494
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721078949.9U Expired - Fee Related CN207237985U (en) | 2017-08-26 | 2017-08-26 | A kind of reaction kettle of amino acids production processing |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207237985U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109569465A (en) * | 2018-12-31 | 2019-04-05 | 江苏百达环保科技有限公司 | A kind of heating and heat-insulating device |
-
2017
- 2017-08-26 CN CN201721078949.9U patent/CN207237985U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109569465A (en) * | 2018-12-31 | 2019-04-05 | 江苏百达环保科技有限公司 | A kind of heating and heat-insulating device |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180417 |