CN207237979U - A kind of fluffy ester reaction kettle of lattice - Google Patents
A kind of fluffy ester reaction kettle of lattice Download PDFInfo
- Publication number
- CN207237979U CN207237979U CN201721068439.3U CN201721068439U CN207237979U CN 207237979 U CN207237979 U CN 207237979U CN 201721068439 U CN201721068439 U CN 201721068439U CN 207237979 U CN207237979 U CN 207237979U
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- CN
- China
- Prior art keywords
- reaction kettle
- agitating paddle
- entrance
- temperature monitor
- interlayer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
The utility model discloses a kind of fluffy ester reaction kettle of lattice, including reaction kettle housing；Feed inlet is provided with the reaction kettle housing, temperature monitor entrance, discharge port and agitating paddle entrance, agitating paddle is hung with directly over the reaction kettle enclosure interior, the upper end of the agitating paddle is fixedly connected through agitating paddle entrance with retarder by shaft coupling, the retarder is fixedly connected with the rotation axis of motor, temperature monitor is installed on the temperature monitor entrance, heating layer is provided with the reaction kettle inner walls, the heating layer is arranged on the lower section of agitating paddle, interlayer is provided with the reaction kettle housing exterior walls, water inlet and water outlet are provided with outer wall on the interlayer.The reaction kettle of the utility model has good sealing performance, ensures that material smoothly, effectively carries out in reaction kettle, while control of the reaction kettle to temperature is accurate, the preparation of the very convenient fluffy ester of plaid matching.
Description
Technical field
Lipid production equipment technology is the utility model is related to, is specially a kind of fluffy ester reaction kettle of lattice.
Background technology
The fluffy ester of lattice is a kind of chemical substance, and molecular formula is C10H18O3, its appearance is colourless transparent liquid, is had strong
Fruity, slightly there is the fluffy perfume (or spice) of lattice of pineapple, and flash-point is 94 DEG C, relative density 0.9364-0.944, index of refraction 1.427-
1.433, its preparation process is using metallic sodium or sodium hydride and isoamyl alcohol as raw material, is first made isoamyl sodium alkoxide, then with monoxone
Dechlorination sodium reacts, and generates amyl glycolate, and the latter continues and propenyl is in acid system, is dehydrated and generated using dehydrating agent
The fluffy ester of lattice, its preparation process require a kind of special reaction kettle.
Utility model content
The purpose of this utility model is to provide a kind of fluffy ester reaction kettle of lattice, to solve proposed in the above background technology ask
Topic, possessed beneficial effect are；The device structure is simple and convenient to operate, and beneficial to complicated manufacturing technique requirent is adapted to, is passed through
Temperature measuring equipment in reaction kettle housing, can grasp temperature parameter in time, and the operation of heating layer is can control by control device, side
Just the temperature change in the fluffy ester preparation process of lattice, is additionally provided with recirculated water outside it, facilitates shedding for heat.
To achieve the above object, the utility model provides following technical solution：A kind of fluffy ester reaction kettle of lattice, including reaction kettle
Housing；Feed inlet, temperature monitor entrance, discharge port and agitating paddle entrance, the reaction are provided with the reaction kettle housing
Agitating paddle is hung with directly over kettle enclosure interior, the upper end of the agitating paddle passes through shaft coupling through agitating paddle entrance with retarder
It is fixedly connected, the retarder is fixedly connected with the rotation axis of motor, and temperature detection is provided with the temperature monitor entrance
Instrument, is provided with heating layer in the reaction kettle inner walls, the heating layer is arranged on the lower section of agitating paddle, the reaction still shell
It is provided with interlayer on external wall, water inlet and water outlet is provided with the outer wall on the interlayer.
Preferably, it is both provided with sealing ring on the feed inlet, temperature monitor entrance, discharge port and agitating paddle entrance.
Preferably, the top of the discharge port is provided with sampling pipe.
Preferably, the temperature monitor is connected with the control device outside reaction kettle respectively with heating layer.
Preferably, the water inlet is a altogether, is circumferentially evenly distributed in the surface of interlayer, the water outlet is a altogether, edge
Circumferential centerline is symmetrically distributed in the lower part of interlayer.
Compared with prior art, the beneficial effects of the utility model are：Equipment design is reasonable, is especially suitable for the fluffy ester of plaid matching
Preparation, its specific advantage is as described below:
（1）Device external is provided with control device, easy to control the work of heating layer, adjusts the temperature in reaction kettle, if
It is standby to be internally provided with temperature monitor, the temperature change in reaction kettle can be monitored；
（2）By setting intake-outlet, facilitate the reduction of reactor temperature, preparation efficiency is improved, to the heat given out
Amount can be used as elsewhere, contributing to the reasonable utilization of energy；
（3）The equipment good airproof performance, can check whether the fluffy ester of lattice of preparation is qualified at any time by sampling pipe.
Brief description of the drawings
Fig. 1 is the internal structure schematic diagram of the utility model；
Fig. 2 is the top view of the utility model；
Fig. 3 is the temperature heating system schematic diagram of the utility model.
In figure：1- reaction kettle housings；2- feed inlets；3- temperature monitor entrances；4- temperature monitors；5- agitating paddles；6-
Motor；7- discharge ports；8- sampling pipes；9- water outlets；10- heating layers；11- water inlets；12- retarders；13- interlayers；14- is stirred
Mix paddle entrance；15- control devices.
Embodiment
The following is a combination of the drawings in the embodiments of the present utility model, and the technical scheme in the embodiment of the utility model is carried out
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are without making creative work
All other embodiments obtained, shall fall within the protection scope of the present invention.
- 3 are please referred to Fig.1, a kind of embodiment provided by the utility model：A kind of fluffy ester reaction kettle of lattice, including reaction still shell
Body 1；Feed inlet 2, temperature monitor entrance 3, discharge port 7 and agitating paddle entrance 14 are provided with the reaction kettle housing 1, it is described
Reaction kettle housing 1 is hung with agitating paddle 5 directly over inside, and the upper end of the agitating paddle 5 passes through agitating paddle entrance 14 and retarder
12 are fixedly connected by shaft coupling, and the retarder 12 is fixedly connected with the rotation axis of motor 6, the temperature monitor entrance 3
On temperature monitor 4 is installed, heating layer 10 is provided with 1 inner wall of reaction kettle housing, the heating layer 10, which is arranged on, to be stirred
The lower section of paddle 5 is mixed, is provided with interlayer 13 on 1 outer wall of reaction kettle housing, is provided with the outer wall on the interlayer 13 into water
Mouth 11 and water outlet 9；Sealing is both provided with the feed inlet 2, temperature monitor entrance 3, discharge port 7 and agitating paddle entrance 14
Circle；The top of the discharge port 7 is provided with sampling pipe 8；The temperature monitor 4 and heating layer 10 respectively with outside reaction kettle
Control device 15 connect；The water inlet 11 totally 6, is circumferentially evenly distributed in the surface of interlayer 13, the water outlet 9
Totally 2, circumferentially center line be symmetrically distributed in the lower part of interlayer 13.
Operation principle：In use, being put into the raw material for preparing the fluffy ester of lattice from feed inlet 2, it is mixed by agitating paddle 5
It is even, control heating layer 10 to raise reactor temperature by control device 15, accelerate reaction process, see at any time in the process
Reactor temperature is examined, and then adjusts the working condition of heating layer, is judged instead to detect the index of reactant by sampling pipe 8
The degree that should be carried out, water inlet 11 and water outlet 9 then can quickly cool down reaction kettle, improve preparation efficiency.
It is obvious to a person skilled in the art that the utility model is not limited to the details of above-mentioned one exemplary embodiment, and
And in the case of the spirit or essential attributes without departing substantially from the utility model, it can realize that this practicality is new in other specific forms
Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this practicality is new
The scope of type is indicated by the appended claims rather than the foregoing description, it is intended that the equivalency fallen in claim is contained
All changes in justice and scope are embraced therein.Any reference numeral in claim should not be considered as limitation
Involved claim.
Claims (5)
1. a kind of fluffy ester reaction kettle of lattice, including reaction kettle housing（1）；It is characterized in that：The reaction kettle housing（1）On be provided with
Feed inlet（2）, temperature monitor entrance（3）, discharge port（7）With agitating paddle entrance（14）, the reaction kettle housing（1）Inside is just
Overhung has agitating paddle（5）, the agitating paddle（5）Upper end pass through agitating paddle entrance（14）With retarder（12）Pass through shaft coupling
Device is fixedly connected, the retarder（12）With motor（6）Rotation axis be fixedly connected, the temperature monitor entrance（3）Upper peace
Equipped with temperature monitor（4）, the reaction kettle housing（1）Heating layer is provided with inner wall（10）, the heating layer（10）Set
In agitating paddle（5）Lower section, the reaction kettle housing（1）Interlayer is provided with outer wall（13）, the interlayer（13）On outer wall
On be provided with water inlet（11）And water outlet（9）.
A kind of 2. fluffy ester reaction kettle of lattice according to claim 1, it is characterised in that：The feed inlet（2）, temperature monitor
Entrance（3）, discharge port（7）With agitating paddle entrance（14）On be both provided with sealing ring.
A kind of 3. fluffy ester reaction kettle of lattice according to claim 1, it is characterised in that：The discharge port（7）Top set
There is sampling pipe（8）.
A kind of 4. fluffy ester reaction kettle of lattice according to claim 1, it is characterised in that：The temperature monitor（4）With heating
Layer（10）Respectively with the control device outside reaction kettle（15）Connection.
A kind of 5. fluffy ester reaction kettle of lattice according to claim 1, it is characterised in that：The water inlet（11）Totally 6, along circle
Week is evenly distributed in interlayer（13）Surface, the water outlet（9）Totally 2, circumferentially center line is symmetrically distributed in interlayer
（13）Lower part.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721068439.3U CN207237979U (en) | 2017-08-24 | 2017-08-24 | A kind of fluffy ester reaction kettle of lattice |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721068439.3U CN207237979U (en) | 2017-08-24 | 2017-08-24 | A kind of fluffy ester reaction kettle of lattice |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207237979U true CN207237979U (en) | 2018-04-17 |
Family
ID=61882142
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721068439.3U Expired - Fee Related CN207237979U (en) | 2017-08-24 | 2017-08-24 | A kind of fluffy ester reaction kettle of lattice |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207237979U (en) |
-
2017
- 2017-08-24 CN CN201721068439.3U patent/CN207237979U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180417 Termination date: 20190824 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |