CN207204076U - A kind of alkali soluble inorganic sample decomposition reactor - Google Patents
A kind of alkali soluble inorganic sample decomposition reactor Download PDFInfo
- Publication number
- CN207204076U CN207204076U CN201720919722.6U CN201720919722U CN207204076U CN 207204076 U CN207204076 U CN 207204076U CN 201720919722 U CN201720919722 U CN 201720919722U CN 207204076 U CN207204076 U CN 207204076U
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- Prior art keywords
- kettle
- soluble inorganic
- alkali soluble
- decomposition reactor
- water
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Abstract
The utility model discloses a kind of alkali soluble inorganic sample decomposition reactor,Including stirring motor,Kettle and the kettle cover being connected with kettle flange,The stirring motor is connected with kettle cover,The output end of the stirring motor is extended into kettle,The output end of the stirring motor and stirring axis connection,The agitating shaft is connected with multipair stirring vane,The left side of the kettle cover is provided with charging aperture,The right side of the kettle cover is provided with input duct,The end of the input duct is provided with inlet,The lateral wall of the kettle is provided with multiple bearings,The outer surface of the kettle is provided with heat-insulation layer,The inner side of the heat-insulation layer is provided with circulation water layer,High temperature resistant alkali prevention layer in device,Provide a stable reaction environment,Whole course of reaction is controllable to various different temperatures,Feeding device can be directly connected to the liquid charging stock of outside,By in liquid charging stock feeder,Avoid the injury that strong alkaline liquid may be brought to worker.
Description
Technical field
Reactor technical field is the utility model is related to, specific field is a kind of alkali soluble inorganic sample decomposition reactor.
Background technology
Alkali solution technique is the wet method for decomposing inorganic sample, by insoluble substance and sodium hydroxide（Generally analyze pure, this is all
Product decompose complete）Heat fusing altogether, makes some components therein be changed into solable matter, therefrom extracts metal, in the production of industry
Middle to need a container to carry out above-mentioned chemical reaction, reactor is a selection well as the container of alkali solution technique, and
Reactor needs to be designed according to the different functional requirement of different operating environment, and alkali solution technique causes work due to adding sodium hydroxide
Highly basic state is constantly in as environment, it is miscellaneous that existing reactor may produce the introducing of corrosion reacting kettle material after highly basic is added
Matter, influence the extraction to metal, it is impossible to for performing alkali soluble technique.
Utility model content
The purpose of this utility model is to provide a kind of alkali soluble inorganic sample decomposition reactor, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the utility model provides following technical scheme：A kind of alkali soluble inorganic sample decomposition reaction
Kettle, including stirring motor, kettle and the kettle cover being connected with kettle flange, the stirring motor are connected with kettle cover, the stirring electricity
The output end of machine is extended into kettle, and output end and stirring axis connection, the agitating shaft of the stirring motor stir with multipair
Blade connection is mixed, is inter-connected via a bolt joint between stirring vane described in each pair, the left side of the kettle cover is provided with charging aperture, described
Feed cap is connected with charging aperture, the right side of the kettle cover is provided with input duct, and input duct is extended into kettle, described
The end of input duct is provided with inlet, and the input duct is provided with feed liquor gate valve, and the lateral wall of the kettle is provided with more
Individual bearing, the outer surface of the kettle are provided with heat-insulation layer, and the inner side of the heat-insulation layer is provided with circulation water layer, the outside of the kettle
Be provided with outlet conduit connect with circulation water layer at the top of wall, the end of the outlet conduit is provided with delivery port, the kettle outside
Sidewall bottom be provided with the inlet channel that connects of circulation water layer, from a left side to by being sequentially provided with into water non-return on the inlet channel
Valve, water inlet water pump and water inlet gate valve, the end of the inlet channel are provided with water inlet, and the bottom of the kettle is provided with and recirculated water
The drainage pipeline of layer connection, the drainage pipeline are provided with water discharging valve, and the end of the drainage pipeline is provided with discharge outlet, described
The bottom of kettle is communicated with blow-off line, and the outlet end flange of the blow-off line is connected with sewage draining valve, the bottom of the kettle
Portion is provided with multiple heating chambers, and heating rod is provided with the heating chamber.
Preferably, the inlet is provided with flowmeter.
Preferably, screen pack is provided between the blow-off line and sewage draining valve.
Preferably, the bottom of the kettle is provided with the temperature sensor extended into inside kettle.
Preferably, the bottom of the temperature sensor is provided with temperature indicating meter.
Preferably, the bottom of the kettle is provided with the soda acid sensor extended into inside kettle.
Preferably, the bottom of the soda acid sensor is provided with soda acid dial gauge.
Preferably, it is equipped with high temperature resistant alkali prevention layer on the madial wall of the kettle and the lateral wall of agitating shaft.
Compared with prior art, the beneficial effects of the utility model are：A kind of alkali soluble inorganic sample decomposition reactor, lead to
The high temperature resistant alkali prevention layer crossed in kettle, there is provided a stable reaction environment, it also avoid reagent corrosion kettle and introduce impurity,
Output effect is influenceed, the heater in heating chamber can be to improve the temperature in device, and the current circulated in water layer can lower
Temperature in device, realizes demand of the whole course of reaction to various different temperatures, and feeding device can be directly connected to outside
Liquid charging stock, the injury that strong alkaline liquid may be brought to worker, temperature sensor in liquid charging stock feeder, will be avoided
Monitor the temperature in reactor and real time temperature is shown on temperature indicating meter, the soda acid journey in soda acid Sensor monitoring reactor
Spend and real-time acid-base value is shown on temperature indicating meter, so as to monitor the real-time status of whole reaction environment, blow-off line and row
Screen pack between dirty valve first can discharge the liquid in kettle, then remove screen pack and discharge solid.
Brief description of the drawings
Fig. 1 is agent structure schematic diagram of the present utility model.
In figure：1- stirring motors, 2- kettlies, 3- kettle covers, 4- agitating shafts, 5- stirring vanes, 6- charging apertures, 7- feed caps,
8- input ducts, 9- inlets, 10- feed liquors gate valve, 11- bearings, 12- heat-insulation layers, 13- circulations water layer, 14- outlet conduits, 15-
Delivery port, 16- inlet channels, 17- enter Water Check Valve, 18- water inlets water pump, 19- water inlets gate valve, 20- water inlets, 21- drainpipes
Road, 22- water discharging valves, 23- discharge outlet, 24- blow-off lines, 25- sewage draining valves, 26- heating chambers, 27- heating rods, 28- flows
Table, 29- temperature sensors, 30- temperature indicating meters, 31- soda acids sensor, 32- soda acids dial gauge, 33- high temperature resistant alkali prevention layers.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out
Clearly and completely describing, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made
The every other embodiment obtained, belong to the scope of the utility model protection.
Referring to Fig. 1, the utility model provides a kind of technical scheme：A kind of alkali soluble inorganic sample decomposition reactor, bag
Include stirring motor 1, kettle 2 and the kettle cover 3 being connected with kettle flange, the stirring motor to be connected with kettle cover, the stirring motor
Output end extend into kettle, the output end of the stirring motor is connected with agitating shaft 4, motor output end rotate drive stir
Axle rotation is mixed, the agitating shaft is connected with multipair stirring vane 5, is inter-connected via a bolt joint between stirring vane described in each pair,
The junction of stirring vane and agitating shaft is half slot, and two half slots clamp agitating shaft, and clamp agitating shaft, root by bolt
Multipair stirring vane can be installed according to demand, the left side of the kettle cover is provided with charging aperture 6, feed cap 7 is connected with the charging aperture,
Open feed cap to be put into solid material in device from charging aperture, charging, which finishes, closes feed cap to be reacted, the kettle
The right side of lid is provided with input duct 8, and input duct is extended into kettle, and input duct is used for that people will be endangered very big strong
Akaline liquid is imported into device, and the end of the input duct is provided with inlet 9, is easy to be connected with external equipment, it is described enter
Liquid pipe road is provided with feed liquor gate valve 10, and switch feed liquor gate valve is set with controlling the entrance of outside liquid on the lateral wall of the kettle
There are multiple bearings 11, for securing the device to outside support, the kettle is provided with bladder layer 12 and heat-insulation layer 12, heat-insulation layer
Reaction environment temperature can be prevented by external influence, while also avoid personnel during internal high temperature from touching the scald that device band is come, institute
The inner side for stating heat-insulation layer is provided with circulation water layer 13, and current flow through in circulation water layer makes device cool, the lateral wall of the kettle
Top is provided with the outlet conduit 14 connected with circulation water layer, and the end of the outlet conduit is provided with delivery port 15, the kettle
Lateral wall bottom is provided with the inlet channel 16 connected with circulation water layer, stops on the inlet channel from a left side to by being sequentially provided with into water
Go back to valve 17, water inlet water pump 18 and water inlet gate valve 19, the end of the inlet channel and be provided with water inlet 20, external water source, which connects, to be in
The water inlet of autoclave body bottom, water inlet water pump is opened, then open water inlet gate valve and enter Water Check Valve, current are imported from inlet channel
To circulation water layer, water is gradually added into when the water surface for circulating water layer is higher than outlet conduit, current flow out from outlet conduit, delivery port
Connection external pipe realizes the circulation of current, and so as to the function of realization device current cooling, the bottom of the kettle is provided with following
The drainage pipeline 21 of ring water layer connection, the drainage pipeline are provided with water discharging valve 22, and the end of the drainage pipeline is provided with row
The mouth of a river 23, when completing to cool, it is necessary to which the water circulated in water layer is discharged, close into Water Check Valve, water inlet water pump and intake gate
Valve, stop intaking and ensure that the infringement that water pump is not flowed back, then open water discharging valve, the water circulated in water layer is whole
Discharge, the bottom of the kettle are communicated with blow-off line 24, for the material in kettle to be discharged, the outlet of the blow-off line
End flanges are connected with sewage draining valve 25, open sewage draining valve discharge material, the bottom of the kettle is provided with multiple heating chambers 26, institute
State in heating chamber and be provided with heating rod 27, heating rod is loaded in heating chamber, heating is device and provides heat.
Specifically, the inlet is provided with flowmeter 28, and monitoring is added to the flow of the liquid in kettle, accurately
Metering intact could chemically react.
Specifically, screen pack is provided between the blow-off line and sewage draining valve, when discharging the material in kettle, can be incited somebody to action
Solid is first stayed in kettle, and liquid is all discharged, and after liquid discharge, is removed screen pack and is discharged solid material.
Specifically, the bottom of the kettle is provided with the temperature sensor 29 extended into inside kettle, monitors in kettle
Temperature.
Specifically, the bottom of the temperature sensor is provided with temperature indicating meter 30, is easy to the temperature observed in kettle, temperature
Degree has a great impact to chemical reaction, it is ensured that kettle is in suitable reaction temperature.
Specifically, the bottom of the kettle is provided with the soda acid sensor 31 extended into inside kettle, monitors the acid of kettle
Basicity.
Specifically, the bottom of the soda acid sensor is provided with soda acid dial gauge 32, is easy to the acid-base value observed in kettle,
Acid-base value has a great impact to chemical reaction, and because chemical reaction can consume alkali ion, acid-base value can reduce, it is ensured that kettle
Interior acid-base value can carry out reaction.
Specifically, high temperature resistant alkali prevention layer 33 is equipped with the madial wall of the kettle and the lateral wall of agitating shaft, prevented
Device is corroded by highly basic liquid, adds impurities in reaction, while also can guarantee that normal work in high temperature.
Operation principle：Suitable position is mounted a device onto using bearing, and the heater in heating chamber can be to improve dress
Interior temperature is put, the climbing speed of the quantity increase temperature of heating chamber is increased or decreased, when the power and the power of loss of heating
Realized when equal to the temperature control of device, external water source connects the water inlet in autoclave body bottom, opens water inlet water pump, then open into
Water gate valve and enter Water Check Valve, current are directed into circulation water layer from inlet channel, be gradually added into water when the water surface of circulation water layer
During higher than outlet conduit, current flow out from outlet conduit, and delivery port connection external pipe realizes the circulation of current, so as to realize dress
The function of current cooling is put, when completing to cool, it is necessary to which the water circulated in water layer is discharged, is closed into Water Check Valve, water inlet water
Pump and water inlet gate valve, stop intaking and ensure that the infringement that water pump is not flowed back, then open water discharging valve, will circulate water layer
Interior water is all discharged, and realizes demand of the whole course of reaction to various different temperatures, temperature sensor and temperature indicator are just
It is monitored in temperature, solid material is put into kettle from charging aperture, and fluent material imports from inlet through input duct
Into kettle, motor driven stirring vane rotates the homogeneity for ensureing liquid in kettle, and acidity-basicity sensor and acid-base value are shown
Device is easy to be monitored acid-base value, it is ensured that the steady progress of chemical reaction, after completion of the reaction, sewage draining valve is opened, due to mistake
Liquid is discharged in the presence kettle of filter screen, and solid is stayed in kettle, after liquid discharge, removes screen pack by solid material
Discharge.
Although embodiment of the present utility model has been shown and described in road, for one of ordinary skill in the art
Speech, it is possible to understand that can carry out a variety of changes to these embodiments in the case where not departing from principle of the present utility model and spirit
Change, change, replacing and modification, the scope of the utility model are defined by the appended claims and the equivalents thereof.
Claims (8)
1. a kind of alkali soluble inorganic sample decomposition reactor, including stirring motor（1）, kettle（2）With with kettle（2）Flange connects
Kettle cover（3）, it is characterised in that：The stirring motor（1）With kettle cover（3）Connection, the stirring motor（1）Output end extension
Into kettle（2）It is interior, the stirring motor（1）Output end and agitating shaft（4）Connection, the agitating shaft（4）With multipair stirring
Blade（5）Connection, stirring vane described in each pair（5）Between be inter-connected via a bolt joint, the kettle cover（3）Left side be provided with charging
Mouthful（6）, the charging aperture（6）On be connected with feed cap（7）, the kettle cover（3）Right side be provided with input duct（8）, and feed liquor
Pipeline（8）Extend into kettle（2）It is interior, the input duct（8）End be provided with inlet（9）, the input duct（8）On
Provided with feed liquor gate valve（10）, the kettle（2）Lateral wall be provided with multiple bearings（11）, the outer surface of the kettle, which is provided with, to be protected
Warm layer（12）, the heat-insulation layer（12）Inner side be provided with circulation water layer（13）, the kettle（2）Lateral wall at the top of be provided with following
Ring water layer（13）The outlet conduit of connection（14）, the outlet conduit（14）End be provided with delivery port（15）, the kettle（2）
Lateral wall bottom be provided with and circulation water layer（13）The inlet channel of connection（16）, the inlet channel（16）On from a left side to by according to
It is secondary to be provided with into Water Check Valve（17）, water inlet water pump（18）With water inlet gate valve（19）, the inlet channel（16）End be provided with into
The mouth of a river（20）, the kettle（2）Bottom be provided with and circulation water layer（13）The drainage pipeline of connection（21）, the drainage pipeline
（21）It is provided with water discharging valve（22）, the drainage pipeline（21）End be provided with discharge outlet（23）, the kettle（2）Bottom
It is communicated with blow-off line（24）, the blow-off line（24）Outlet end flange be connected with sewage draining valve（25）, the kettle（2）
Bottom be provided with multiple heating chambers（26）, the heating chamber（26）It is interior to be provided with heating rod（27）.
A kind of 2. alkali soluble inorganic sample decomposition reactor according to claim 1, it is characterised in that：The inlet
（9）It is provided with flowmeter（28）.
A kind of 3. alkali soluble inorganic sample decomposition reactor according to claim 1, it is characterised in that：The blow-off line
（24）With sewage draining valve（25）Between be provided with screen pack.
A kind of 4. alkali soluble inorganic sample decomposition reactor according to claim 1, it is characterised in that：The kettle（2）
Bottom be provided with extend into kettle（2）Internal temperature sensor（29）.
A kind of 5. alkali soluble inorganic sample decomposition reactor according to claim 4, it is characterised in that：The TEMP
Device（29）Bottom be provided with temperature indicating meter（30）.
A kind of 6. alkali soluble inorganic sample decomposition reactor according to claim 1, it is characterised in that：The kettle（2）
Bottom be provided with extend into kettle（2）Internal soda acid sensor（31）.
A kind of 7. alkali soluble inorganic sample decomposition reactor according to claim 6, it is characterised in that：The soda acid sensing
Device（31）Bottom be provided with soda acid dial gauge（32）.
A kind of 8. alkali soluble inorganic sample decomposition reactor according to claim 1, it is characterised in that：The kettle（2）
Madial wall and agitating shaft（4）Lateral wall on be equipped with high temperature resistant alkali prevention layer（33）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720919722.6U CN207204076U (en) | 2017-07-26 | 2017-07-26 | A kind of alkali soluble inorganic sample decomposition reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720919722.6U CN207204076U (en) | 2017-07-26 | 2017-07-26 | A kind of alkali soluble inorganic sample decomposition reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207204076U true CN207204076U (en) | 2018-04-10 |
Family
ID=61814125
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720919722.6U Active CN207204076U (en) | 2017-07-26 | 2017-07-26 | A kind of alkali soluble inorganic sample decomposition reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207204076U (en) |
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2017
- 2017-07-26 CN CN201720919722.6U patent/CN207204076U/en active Active
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